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51. 发明申请

US20130092598A1 PRODUCTION OFLUBRICATING OIL BASESTOCKS 审中-公开
标题翻译：生产油基油
公开(公告)号：US20130092598A1
公开(公告)日：2013-04-18
申请号：US13547156
申请日：2012-07-12
申请人： Eric D. Joseck , Michael Brian Carroll , David Mentzer , Teck-Mui Hoo , Michel Daage , Ajit Bhaskar Dandekar
发明人： Eric D. Joseck , Michael Brian Carroll , David Mentzer , Teck-Mui Hoo , Michel Daage , Ajit Bhaskar Dandekar
IPC分类号： C10G65/12
CPC分类号： C10G65/12 , C10G45/60 , C10G45/62 , C10G45/64 , C10G47/14 , C10G49/22 , C10G65/14 , C10G2300/1074 , C10G2300/202 , C10G2300/301 , C10G2300/302 , C10G2300/304 , C10G2400/04 , C10G2400/10
摘要： Methods are provided for producing multiple lubricating oil basestocks from a feedstock. Prior to dewaxing, various fractions of the feedstock are exposed to hydrocracking conditions of different severity to produce a higher overall yield of basestocks. The hydrocracking conditions of different severity can represent exposing fractions of a feedstock to different processing conditions, exposing fractions of a feedstock to different amounts of hydrocracking catalyst, or a combination thereof.
摘要翻译：提供了用于从原料生产多个润滑油基础油料的方法。在脱蜡之前，原料的各种馏分暴露于不同强度的加氢裂化条件，以产生较高的基础油料总产率。不同严重程度的加氢裂化条件可以将原料暴露于不同加工条件的馏分，将原料馏分暴露于不同量的加氢裂化催化剂或其组合。

52. 发明申请

US20120209041A1 PROCESSING OF FEEDSTOCKS IN SEPARATED REACTOR VOLUMES 有权
标题翻译：分离反应器体积中的进料处理
公开(公告)号：US20120209041A1
公开(公告)日：2012-08-16
申请号：US13365328
申请日：2012-02-03
申请人： Patrick L. Hanks , Michel Daage
发明人： Patrick L. Hanks , Michel Daage
IPC分类号： C07C1/207
CPC分类号： C10G45/72 , B01J8/0214 , B01J8/0257 , B01J8/0453 , B01J8/0465 , B01J2208/00309 , B01J2208/00938 , B01J2208/025 , C10G3/42 , C10G3/50 , C10G47/36 , C10G49/002 , C10G65/02 , C10G65/14 , C10G2300/1011 , C10G2300/1044 , C10G2300/202 , C10G2300/4081 , Y02P30/20
摘要： Separated volumes can be created in a reactor using interior dividing wall or interior conduit structures. Feedstocks can be hydroprocessed in the separated volumes to allow multiple types of hydroprocessing conditions and/or feeds to be processed in a single reactor. The feedstocks can remain separate for the entire volume of the reactor, or the dividing barrier can end at some intermediate point in the reactor.
摘要翻译：可以在使用内部分隔壁或内部管道结构的反应器中产生分离体积。原料可以在分离的体积中加氢处理，以允许多种类型的加氢处理条件和/或进料在单个反应器中加工。原料可以在反应器的整个体积中保持分开，或者分隔壁可以在反应器中的某个中间点处结束。

53. 发明授权

US06800579B2 Catalyst regeneration 有权
标题翻译：催化剂再生
公开(公告)号：US06800579B2
公开(公告)日：2004-10-05
申请号：US10059926
申请日：2002-01-29
申请人： Michel Daage , Russell John Koveal , Min Chang
发明人： Michel Daage , Russell John Koveal , Min Chang
IPC分类号： B01J3812
CPC分类号： B01J23/96 , B01J23/75 , B01J23/94 , B01J38/10 , B01J38/12 , B01J38/56 , B01J38/68 , B01J2038/005 , C07C1/045 , C07C2523/75 , C10G2/331 , C10G2/332 , C10G2/333 , Y02P20/584 , C07C9/04
摘要： There is provided a process for regenerating the activity of used metal catalysts for the hydrogenation of carbon monoxide comprising decreasing the hydrocarbon content thereof, calcining under an oxidant-containing atmosphere, impregnating with a solution of at least one of a metal compound, calcining under an oxidant-containing atmosphere and activating by contacting with a hydrogen-contacting gas at elevated temperatures to form an active catalyst. The process regenerates and enhances both supported and dispersed active metal (DAM) catalysts. Used catalysts enhanced by the process are initially treated to decrease their hydrocarbon content. The treatment may be carried out in a single reactor, or by carrying out up to all steps after catalyst may be withdrawn from a reactor and returned to at least one reactor, both preferably during operation thereof. Up to all steps may be effected in a subsequent reactor, or in specialized apparatus.
摘要翻译：提供了一种用于再生用于一氧化碳氢化的所用金属催化剂的活性的方法，包括降低其含烃量，在含氧化剂的气氛下煅烧，用至少一种金属化合物的溶液浸渍，在氧化剂的气氛，并通过在高温下与接触氢的气体接触而形成活性催化剂。该方法再生并增强了负载和分散的活性金属（DAM）催化剂。首先处理通过该方法增强的使用的催化剂以降低它们的烃含量。处理可以在单个反应器中进行，或者在催化剂可以从反应器中取出并返回到至少一个反应器之后，最好在其操作期间进行到所有步骤。直到所有步骤都可以在随后的反应器中或在专门的装置中进行。

54. 发明授权

US06777451B2 Catalyst enhancement 有权
标题翻译：催化剂增强
公开(公告)号：US06777451B2
公开(公告)日：2004-08-17
申请号：US10059927
申请日：2002-01-29
申请人： Russell John Koveal , Michel Daage , Charles Harrison Mauldin , Janet Renee Clark
发明人： Russell John Koveal , Michel Daage , Charles Harrison Mauldin , Janet Renee Clark
IPC分类号： C07C2700
CPC分类号： B01J21/063 , B01J23/40 , B01J23/6567 , B01J23/70 , B01J23/75 , B01J23/8896 , B01J23/89 , B01J23/94 , B01J23/96 , B01J38/10 , B01J38/12 , B01J38/56 , B01J38/58 , B01J38/66 , C10G2/332 , C10G2/333
摘要： A process for enhancing metal catalysts for carbon monoxide hydrogenation comprising reducing the catalyst so that at least a portion is in the metallic state, impregnating under a non-oxidative atmosphere with a solution of a salt of at least one metal, optionally in combination with at least one of an ammonium salt, an alkyl ammonium salt, a weak organic acid and ammonia, oxidizing with a gaseous oxidant in the presence of the impregnating solution, and reducing to form an active catalyst. Used catalysts enhanced by the process are initially treated to decrease their hydrocarbon content. The treatment may be carried out in a single reactor, or by carrying out up to all steps after catalyst may be withdrawn from a reactor and returned to at least one reactor, both preferably during operations. Up to all steps may be effected in a subsequent reactor, or in specialized apparatus.
摘要翻译：一种用于增强用于一氧化碳氢化的金属催化剂的方法，包括将催化剂还原为至少一部分处于金属状态，在非氧化性气氛下用至少一种金属的盐溶液浸渍，任选地与至少一种铵盐，烷基铵盐，弱有机酸和氨，在浸渍溶液存在下用气态氧化剂氧化，还原形成活性催化剂。首先处理通过该方法增强的使用的催化剂以降低它们的烃含量。处理可以在单个反应器中进行，或者通过在催化剂可以从反应器中取出并返回到至少一个反应器中，两者优选在操作期间进行到所有步骤。直到所有步骤都可以在随后的反应器中或在专门的装置中进行。

55. 发明授权

US06753351B2 Supported catalyst activation 有权
标题翻译：负载催化剂活化
公开(公告)号：US06753351B2
公开(公告)日：2004-06-22
申请号：US10059918
申请日：2002-01-29
申请人： Janet Renee Clark , Michel Daage , Russell John Koveal
发明人： Janet Renee Clark , Michel Daage , Russell John Koveal
IPC分类号： C07C2700
CPC分类号： C10G2/332 , B01J23/75 , B01J37/0203 , B01J37/14 , B01J37/18 , C10G2/333
摘要： A process for activating a supported metal catalyst or catalyst precursor useful for the hydrogenation of carbon monoxide to form a mixture of hydrocarbons, comprising reducing with a hydrogen-containing gas at elevated temperature so that at least a portion is in the metallic state, impregnating under a non-oxidizing atmosphere with a solution of at least one member selected from the group consisting of ammonium salts, alkyl ammonium salts and weak organic acids, optionally further including ammonia, to the point where it has absorbed a volume of solution equal to at least about 10% of its calculated pore volume, oxidizing with a gaseous oxidant in the presence of the impregnating solution and reducing with hydrogen-containing gas at elevated temperatures to form an active catalyst. The steps beginning with the impregnation may be repeated. Optionally, the catalyst may be calcined after the oxidation step and/or passivated after activation.
摘要翻译：用于活化用于氢化一氧化碳以形成烃混合物的负载型金属催化剂或催化剂前体的方法，包括在高温下用含氢气体还原，使得至少一部分处于金属状态，浸渍在非氧化性气氛，其中选自铵盐，烷基铵盐和弱有机酸中的至少一种的溶液，任选地还包括氨，其吸收一定体积的溶液至少等于至少其计算的孔体积的约10％，在浸渍溶液存在下用气态氧化剂氧化，并在高温下用含氢气体还原形成活性催化剂。可以重复从浸渍开始的步骤。任选地，催化剂可以在氧化步骤之后煅烧和/或在活化后被钝化。

56. 发明授权

US5831138A Dispersed metal sulfide catalysts for hydroprocessing 失效
公开(公告)号：US5831138A
公开(公告)日：1998-11-03
申请号：US912895
申请日：1997-08-15
申请人： Teh Chung Ho , Stuart Leon Soled , Sabato Miseo , Gary Brice McVicker , Michel Daage , Viktor Buchholz
发明人： Teh Chung Ho , Stuart Leon Soled , Sabato Miseo , Gary Brice McVicker , Michel Daage , Viktor Buchholz
IPC分类号： B01J31/22 , B01J23/887 , B01J23/889 , B01J27/051 , B01J37/08 , B01J37/20 , C07B35/02 , C10G45/46 , C10G45/50 , C07C5/10
CPC分类号： B01J37/086 , B01J23/887 , B01J23/8878 , B01J23/8892 , B01J27/051 , B01J37/20 , C10G45/46 , C10G45/50
摘要： The present invention is directed toward a catalyst composition comprising a catalyst prepared by a process comprising: (a) impregnating an oxide precursor selected from the group consisting of rare earth oxide precursors, yttria precursors and mixtures thereof, onto an inorganic refractory oxide support; (b) drying said support at a temperature of about 100.degree. to about 120.degree. C. followed by calcining said support at a temperature of about 400.degree. to about 600.degree. C.; and (c) compositing or depositing on said support of step (b), a catalyst precursor salt represented by (ML)(Mo.sub.y W.sub.1-y O.sub.4).sub.a wherein M comprises Cr and/or one or more divalent promoter metals selected from the group consisting of Mn, Fe, Co, Ni, Cu, Zn and mixtures thereof, wherein y is any value ranging from 0 to 1, and wherein L is one or more neutral, nitrogen-containing ligands at least one of which is a chelating polydentate ligand; a=1 when chromium is not one of the promoter metals and 0.5.ltoreq.a.ltoreq.3 when Cr is one of the promoter metals. (d) sulfiding said deposited or composited supports of step (c) with an excess amount of sulfur in the form of one or more sulfur bearing compounds and at a temperature of at least about 250.degree. C. to form catalysts. In a preferred embodiment, the process will further comprise decomposing the composited or deposited supports of step (c) in a nonoxidizing atmosphere at a temperature of at least about 250.degree. C. prior to said sulfiding step (d). In a second aspect of the invention there is provided an improved aromatics hydrogenation process.

57. 发明授权

US5767037A Aromatics hydrogenation with a new class of metal oxides 失效
标题翻译：芳烃氢化与一类新型的金属氧化物
公开(公告)号：US5767037A
公开(公告)日：1998-06-16
申请号：US516890
申请日：1995-08-18
申请人： Teh Chung Ho , Charles R. Symon , Viktor Buchholz , Michel Daage
发明人： Teh Chung Ho , Charles R. Symon , Viktor Buchholz , Michel Daage
IPC分类号： B01J31/18 , B01J23/28 , B01J23/30 , B01J23/88 , B01J37/08 , B01J37/18 , C10G45/46 , C10G45/50 , C10G65/08 , B01J27/051 , C07C5/10 , C10G47/02
CPC分类号： B01J23/8898 , B01J23/28 , B01J23/30 , B01J23/88 , B01J37/086 , B01J37/18 , C10G45/46 , C10G45/50 , C10G65/08
摘要： The present invention is directed toward a highly active aromatics hydrogenation catalyst and its use. The catalyst composition is prepared by: (a) decomposing a catalyst precursor selected from the group consisting of metal amine molybdates, metal amine tungstates and mixtures thereof, wherein said metal amine catalyst precursor has the general formula ML(Mo.sub.y W.sub.1-y O.sub.4)a where M is Cr and/or one or more divalent promoter metals selected from the group consisting of Mn, Fe, Co, Ni, Cu and Zn; L is one or more neutral nitrogen containing ligands at least one of which is a chelating polydentate ligand; 0.ltoreq.y.ltoreq.1; and a=1 for non-chromium containing catalysts and wherein 0.5.ltoreq.a.ltoreq.3 for chromium containing catalysts, at a temperature of about 200.degree. to about 400.degree. C. in an inert atmosphere; and (b) reducing at a temperature of about 300.degree. to about 450.degree. C. said metal amine catalyst precursor to form a catalyst. The catalyst as prepared above may be used in an aromatics hydrogenation process. The invention is further directed to the use of such catalysts in aromatics hydrogenation processes.
摘要翻译：本发明涉及高活性芳烃氢化催化剂及其用途。催化剂组合物通过以下步骤制备：（a）分解选自钼酸金属胺，钨酸金属胺及其混合物的催化剂前体，其中所述金属胺催化剂前体具有通式ML（MoyW1-yO4）a其中M 是选自Mn，Fe，Co，Ni，Cu和Zn中的Cr和/或一种或多种二价助催化剂金属; L是一种或多种中性含氮配体，其中至少一种是螯合多齿配体; 0

58. 发明授权

US5648577A Dispersed metal sulfide catalysts for hydroprocessing (LAW105) 失效
标题翻译：用于加氢处理的分散金属硫化物催化剂（LAW105）
公开(公告)号：US5648577A
公开(公告)日：1997-07-15
申请号：US460410
申请日：1995-06-02
申请人： Teh Chung Ho , Stuart Leon Soled , Sabato Miseo , Gary Brice McVicker , Michel Daage , Viktor Buchholz
发明人： Teh Chung Ho , Stuart Leon Soled , Sabato Miseo , Gary Brice McVicker , Michel Daage , Viktor Buchholz
IPC分类号： B01J31/22 , B01J23/887 , B01J23/889 , B01J27/051 , B01J37/08 , B01J37/20 , C07B35/02 , C10G45/46 , C10G45/50 , C07C5/10
CPC分类号： B01J37/086 , B01J23/887 , B01J23/8878 , B01J23/8892 , B01J27/051 , B01J37/20 , C10G45/46 , C10G45/50
摘要： The present invention is directed toward a catalyst composition prepared by a process comprising: (a) impregnating an oxide precursor selected from the group consisting of rare earth oxide precursors, yttria precursors and mixtures thereof, onto an inorganic refractory oxide support; (b) drying said support at a temperature of about 100.degree. to about 120.degree. C. followed by calcining said support at a temperature of about 400.degree. to about 600.degree. C.; and (c) compositing or depositing on said support of step (b), a catalyst precursor salt represented by (ML)(Mo.sub.y W.sub.1-y O.sub.4).sub.a wherein M comprises Cr and/or one or more divalent promoter metals selected from the group consisting of Mn, Fe, Co, Ni, Cu, Zn and mixtures thereof, wherein y is any value ranging from 0 to 1, and wherein L is one or more neutral, nitrogen-containing ligands at least one of which is a chelating polydentate ligand; a=1 when chromium is not one of the promoter metals and 0.5.ltoreq.a.ltoreq.3 when Cr is one of the promoter metals. (d) sulfiding said deposited or composited support of step (c) with an excess amount of sulfur in the form of one or more sulfur bearing compounds and at a temperature of at least about 250.degree. C. to form catalysts. In a preferred embodiment, the the composited or deposited supports of step (c) may be decomposed in a nonoxidizing atmosphere at a temperature of at least about 250.degree. C. prior to said sulfiding step (d). In a second aspect of the invention there is provided an improved aromatics hydrogenation process.
摘要翻译：本发明涉及通过包括以下步骤的方法制备的催化剂组合物：（a）将选自稀土氧化物前体，氧化钇前体及其混合物的氧化物前体浸渍到无机难熔氧化物载体上; （b）在约100至约120℃的温度下干燥所述载体，然后在约400至约600℃的温度下煅烧所述载体; 和（c）在步骤（b）的所述载体上合成或沉积由（ML）（MoyW1-yO4）a表示的催化剂前体盐，其中M包含Cr和/或一种或多种选自以下的二价助催化剂金属： Mn，Fe，Co，Ni，Cu，Zn及其混合物，其中y是0至1的任何值，并且其中L是一种或多种中性含氮配体，其中至少一种是螯合多齿配体; 当Cr不是助催化剂金属之一时，a = 1，当Cr是助催化剂金属之一时，a = 1。（d）将步骤（c）的沉积或复合载体用一种或多种含硫化合物形式的过量的硫硫化并在至少约250℃的温度下硫化以形成催化剂。在优选的实施方案中，在所述硫化步骤（d）之前，步骤（c）的复合或沉积的载体可以在非氧化气氛中在至少约250℃的温度下分解。在本发明的第二方面，提供了一种改进的芳族化合物氢化方法。

59. 发明授权

US09598651B2 Integrated hydrocracking and dewaxing of hydrocarbons 有权
公开(公告)号：US09598651B2
公开(公告)日：2017-03-21
申请号：US14619593
申请日：2015-02-11
申请人： Krista M. Prentice , Michel Daage , Ajit B. Dandekar , Christopher G. Oliveri , Rohit Vijay , Stephen J. McCarthy , Wenyih F. Lai , Bradley R. Fingland
发明人： Krista M. Prentice , Michel Daage , Ajit B. Dandekar , Christopher G. Oliveri , Rohit Vijay , Stephen J. McCarthy , Wenyih F. Lai , Bradley R. Fingland
IPC分类号： C10G73/38 , C10G73/44 , C10G45/02 , C10G45/64 , C10G47/16 , C10G7/00 , C10G49/22 , C10G67/02 , C10G65/04 , C10G65/12 , B01J29/74 , C10L1/08 , C10M101/02 , B01J35/02
CPC分类号： C10G67/02 , B01J29/7461 , B01J35/026 , B01J2229/36 , B01J2229/42 , C10G45/64 , C10G65/043 , C10G65/12 , C10G2300/202 , C10G2300/302 , C10G2300/4018 , C10G2300/4081 , C10G2400/02 , C10G2400/04 , C10G2400/10 , C10L1/08 , C10L2200/0446 , C10L2270/026 , C10L2290/543 , C10M101/02
摘要： An integrated process for producing naphtha fuel, diesel fuel and/or lubricant base oils from feedstocks under sour conditions is provided. The ability to process feedstocks under higher sulfur and/or nitrogen conditions allows for reduced cost processing and increases the flexibility in selecting a suitable feedstock. The sour feed can be delivered to a catalytic dewaxing step without any separation of sulfur and nitrogen contaminants. The integrated process includes an initial dewaxing of a feed under sour conditions, optional hydrocracking of the dewaxed feed, and a separation to form a first diesel product and a bottoms fraction. The bottoms fraction is then exposed to additional hydrocracking and dewaxing to form a second diesel product and optionally a lubricant base oil product. Alternatively, a feedstock can be hydrotreated, fractionated, dewaxed, and then hydrocracked to form a diesel fuel and a dewaxed, hydrocracked bottoms fraction that is optionally suitable for use as a lubricant base oil.

60. 发明授权

US09499748B2 Petroleum crude oil desalting process and unit 有权
标题翻译：石油原油脱盐工艺及单位
公开(公告)号：US09499748B2
公开(公告)日：2016-11-22
申请号：US14279428
申请日：2014-05-16
申请人： Michel Daage , Magaly C. Barroeta , Brian D. Albert , Mohsen S. Yeganeh , Andrew T. Sullivan , Jose X. Simonetty , Christopher J. Wolfe
发明人： Michel Daage , Magaly C. Barroeta , Brian D. Albert , Mohsen S. Yeganeh , Andrew T. Sullivan , Jose X. Simonetty , Christopher J. Wolfe
IPC分类号： C10G21/06 , C10G21/08 , C10G53/04 , C10G31/08 , C10G33/04 , C10G53/00 , C10G75/00
CPC分类号： C10G31/08 , C10G21/08 , C10G32/02 , C10G33/04 , C10G53/04
摘要： An improved method and process unit for desalting petroleum crude oils in which a portion of the stable emulsion layer which forms in the desalter vessel is withdrawn from the desalter and diluted with a liquid diluent, typically oil or water or both to destabilize the emulsion which is then separated into separate oil and water phases.
摘要翻译：一种用于脱盐石油原油的改进的方法和方法单元，其中在脱盐器中形成的一部分稳定的乳液层从脱盐器中排出并用液体稀释剂（通常为油或水）或二者稀释以使乳液不稳定然后分离成独立的油相和水相。

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