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51. 发明授权

US4945166A Preparation of N-hydroxypyrazoles 失效
标题翻译： N-羟基吡唑的制备
公开(公告)号：US4945166A
公开(公告)日：1990-07-31
申请号：US367053
申请日：1989-06-16
申请人： Ulf Baus , Wolfgang Reuther , Rolf Fikentscher
发明人： Ulf Baus , Wolfgang Reuther , Rolf Fikentscher
IPC分类号： C07D231/12 , C07D231/16 , C07D231/54 , C07D231/56 , C07D521/00
CPC分类号： C07D249/08 , C07D231/12 , C07D231/16 , C07D231/56 , C07D233/56
摘要： N-hydroxypyrazoles of the general formula I ##STR1## where R.sup.1, R.sup.2 and R.sup.3 may be identical or different and are each hydrogen, alkyl, halogen or aryl, or R.sup.1 and R.sup.2 or R.sup.2 and R.sup.3 together with the carbon atoms carrying these radicals form an aromatic or nonaromatic ring of 5 or 6 carbon atoms are prepared by a process in which(A) a pyrazole of the general formula II ##STR2## is converted in a conventional manner with an alkali metal hydroxide, alkali metal hydride or alkali metal carbonate into one of its metal salts of the general formula III ##STR3## where ME.sym. is a cation of an alkali metal, and (B) the resulting metal salt of the general formula III is reacted with dibenzoyl peroxide in an inert organic solvent or in a 2-phase system, in the presence or absence of a phase transfer catalyst.
摘要翻译：通式I的N-羟基吡唑（I）其中R 1，R 2和R 3可以相同或不同，各自为氢，烷基，卤素或芳基，或R 1和R 2或R 2和R 3与携带的碳原子一起这些基团形成5或6个碳原子的芳族或非芳族环是通过以下方法制备的：其中（A）通式II的吡唑（II）以常规方式用碱金属氢氧化物，碱金属氢化物或碱金属碳酸盐转化成其通式III（III）的金属盐之一，其中ME（+）是碱金属的阳离子，和（B）所得到的通式III的金属盐是在相转移催化剂存在或不存在下，在惰性有机溶剂或2-相体系中与二苯甲酰基过氧化物反应。

52. 发明授权

US4827014A 2-Hydroxy-3-aminopropionic-n,n-diacetic acid and derivatives thereof, preparation thereof, and detergents containing same 失效
标题翻译： 2-羟基-3-氨基丙酸，正二乙酸及其衍生物，其制备物和含有它们的洗涤剂
公开(公告)号：US4827014A
公开(公告)日：1989-05-02
申请号：US177084
申请日：1988-04-04
申请人： Richard Baur , Felix Richter , Stefan Birnbach , Rolf Fikentscher , Alfred Oftring , Ekhard Winkler , Werner Bochnitschek
发明人： Richard Baur , Felix Richter , Stefan Birnbach , Rolf Fikentscher , Alfred Oftring , Ekhard Winkler , Werner Bochnitschek
IPC分类号： G01N31/00 , C07C67/00 , C07C227/16 , C07C227/18 , C07C229/22 , C07C229/24 , C07C229/76 , C07C231/00 , C07C231/12 , C07C237/06 , C07C253/00 , C07C253/30 , C07C255/24 , C07C255/26 , C09K3/00 , C11D3/33 , C11D3/39 , C07C101/20 , C07C101/30
CPC分类号： C07C255/00 , C11D3/33 , C11D3/394
摘要： 2-Hydroxy-3-aminopropionic-N,N-diacetic acid and derivatives thereof are used in particular as complexing agents, bleaching agent stabilizers and builders in detergents.
摘要翻译： 2-羟基-3-氨基丙酸-N，N-二乙酸及其衍生物特别用作洗涤剂中的络合剂，漂白剂稳定剂和助洗剂。

53. 发明授权

US4705649A Preparation of acyloxybenzenesulfonic acids and their alkali metal and alkaline earth metal salts 失效
标题翻译：酰氧基苯磺酸及其碱金属和碱土金属盐的制备
公开(公告)号：US4705649A
公开(公告)日：1987-11-10
申请号：US928696
申请日：1986-11-07
申请人： Wolf-Dieter Balzer , Hans-Heinrich Bechtolsheimer , Karl-Heinz Beyer , Rolf Fikentscher , Johannes Perner , Rudi Widder , Helmut Wolf
发明人： Wolf-Dieter Balzer , Hans-Heinrich Bechtolsheimer , Karl-Heinz Beyer , Rolf Fikentscher , Johannes Perner , Rudi Widder , Helmut Wolf
IPC分类号： C07C309/42 , C07C67/00 , C07C69/00 , C07C69/76 , C07C301/00 , C07C303/04 , C07C303/06 , C07C303/08 , C07C303/22 , C07C303/32 , C07C309/41
CPC分类号： C07C303/42 , C07C309/00
摘要： Acyloxybenzenesulfonic acids and their alkali metal and alkaline earth metal salts are prepared by sulfonation of phenol in the presence of a small amount of a complexing agent for the sulfonating agent SO.sub.3 or chlorosulfonic acid, followed by esterification and, if required, neutralization to give the alkali metal or alkaline earth metal salt.
摘要翻译：芳氧基苯磺酸及其碱金属和碱土金属盐通过在少量磺化剂SO 3或氯磺酸络合剂存在下磺化苯酚，然后进行酯化反应制备，如果需要，中和得到碱金属或碱土金属盐。

54. 发明授权

US4695412A Preparation of acyloxybenzenesulfonic acids and their alkali metal and alkaline earth metal salts 失效
标题翻译：酰氧基苯磺酸及其碱金属和碱土金属盐的制备
公开(公告)号：US4695412A
公开(公告)日：1987-09-22
申请号：US933354
申请日：1986-11-19
申请人： Wolf-Dieter Balzer , Hans-Heinrich Bechtolsheimer , Karl-Heinz Beyer , Rolf Fikentscher , Johannes Perner , Rudi Widder , Helmut Wolf
发明人： Wolf-Dieter Balzer , Hans-Heinrich Bechtolsheimer , Karl-Heinz Beyer , Rolf Fikentscher , Johannes Perner , Rudi Widder , Helmut Wolf
IPC分类号： C07C309/42 , C07C67/00 , C07C301/00 , C07C303/06 , C07C303/08 , C07C303/22 , C07C303/32 , C07C143/52
CPC分类号： C07C309/00
摘要： Acyloxybenzenesulfonic acids and their alkali metal and alkaline earth metal salts are prepared by a process comprising sulfonation of a phenyl ester in the presence or absence of a small amount of a complexing agent for the sulfonating agent SO.sub.3 or chlorosulfonic acid, subsequent acylation and, if desired, neutralization to give the alkali metal or alkaline earth metal salt, and, if required, subjecting the latter to oxidative bleaching before drying.
摘要翻译：芳氧基苯磺酸及其碱金属和碱土金属盐通过包括在存在或不存在少量用于磺化剂SO 3或氯磺酸的络合剂的情况下苯基酯磺化的方法制备，随后进行酰化，如果需要中和，得到碱金属或碱土金属盐，如果需要，在干燥前对其进行氧化漂白。

55. 发明授权

US4670591A Preparation of N-.alpha.-alkoxyethylformamides 失效
标题翻译：制备N-烷氧基乙酰甲酰胺
公开(公告)号：US4670591A
公开(公告)日：1987-06-02
申请号：US863167
申请日：1986-05-14
申请人： Alfred Oftring , Erwin Hahn , Rolf Fikentscher
发明人： Alfred Oftring , Erwin Hahn , Rolf Fikentscher
IPC分类号： C07C231/00 , C07C233/00 , C07C233/16 , C07C233/18 , C07C103/44 , C07C103/38
CPC分类号： C07C233/00 , C07C233/16
摘要： N-.alpha.-alkoxyethylformamides of the formula ##STR1## where R is C.sub.1 -C.sub.18 -alkyl, are prepared by reacting a vinyl ether of the formulaCH.sub.2 .dbd.CH--OR (II),where R has the meaning stated in the formula I, with formamide in the presence of an acidic or basic catalyst at from -10.degree. to 150.degree. C.
摘要翻译：通过使式CH 2 = CH-OR（II）的乙烯基醚反应制备其中R为C 1 -C 18 - 烷基的通式为其中R为具有如下定义的含义的式（I）的N- 式I化合物与甲酰胺在-10至150℃的酸性或碱性催化剂存在下反应。

56. 发明授权

US4652669A 2-(1-hydroxycarbalkoxymethyl)-acrylonitriles and 2-(1-hydroxycarbalkoxymethyl)-acrylates and their preparation 失效
标题翻译： 2-（1-羟基烷氧基甲基） - 丙烯腈和2-（1-羟基烷氧基甲基） - 丙烯酸酯及其制备方法
公开(公告)号：US4652669A
公开(公告)日：1987-03-24
申请号：US804121
申请日：1985-12-03
申请人： Rolf Fikentscher , Erwin Hahn , Alexander Kud , Alfred Oftring
发明人： Rolf Fikentscher , Erwin Hahn , Alexander Kud , Alfred Oftring
IPC分类号： C08F20/00 , C07C67/00 , C07C67/343 , C07C69/732 , C07C253/00 , C07C255/23 , C08F20/10 , C08F20/42 , C08F20/52 , C08F220/00 , C07C121/30
CPC分类号： C07C255/00
摘要： 2-(1-Hydroxycarbalkoxymethyl)-acrylonitriles and 2-(1-hydroxycarbalkoxymethyl)-acrylates are prepared by a process in which an acrylonitrile or an acrylate is reacted with a glyoxylate in an aqueous medium at a pH greater than or equal to 6, in the presence of a tertiary amine as a catalyst.
摘要翻译： 2-（1-羟基烷氧基甲基） - 丙烯腈和2-（1-羟基烷氧基甲基） - 丙烯酸酯是通过丙烯腈或丙烯酸酯在水性介质中以大于或等于6的pH与乙醛酸反应的方法制备的，在叔胺作为催化剂存在下进行。

57. 发明授权

US4614613A Preparation of .beta.-N-aziridinopropionates 失效
标题翻译：制备β-N-氮丙啶丙酸酯
公开(公告)号：US4614613A
公开(公告)日：1986-09-30
申请号：US628773
申请日：1984-07-09
申请人： Rolf Fikentscher , Siegfried Schneider , Erhard Klahr , Friedrich Reinert , Gunter Eckert , Adolf Stuebinger
发明人： Rolf Fikentscher , Siegfried Schneider , Erhard Klahr , Friedrich Reinert , Gunter Eckert , Adolf Stuebinger
IPC分类号： B01J31/12 , C07B61/00 , C07D203/08
CPC分类号： C07D203/08
摘要： .beta.-N-aziridinopropionates of relatively high boiling alcohols or polyalcohols are prepared by transesterifying a .beta.-N-aziridinopropionate of a lower alcohol of 1 to 4 carbon atoms with a relatively high boiling alcohol or polyalcohol by a process in which the transesterification is carried out in the presence of, as a transesterification catalyst, a titanium(IV) or tin(IV) compound which is soluble in an organic medium.
摘要翻译：相对高沸点的醇或多元醇的β-N-吖丙啶丙酸酯通过一种具有1-4个碳原子的低级醇的β-N-氮丙啶基丙酸酯与相对高沸点醇或多元醇的酯交换反应来制备在作为酯交换催化剂存在下，可溶于有机介质的钛（IV）或锡（IV）化合物。

58. 发明授权

US4592757A Production of dyed or undyed wool with an antifelting finish: quaternized piperazine condensate 失效
标题翻译：生产染色或未染色的羊毛，具有抗结垢作用：季铵化的哌嗪缩合物
公开(公告)号：US4592757A
公开(公告)日：1986-06-03
申请号：US729221
申请日：1985-05-01
申请人： Rolf Fikentscher , Heinrich Mertens , Klaus Reincke
发明人： Rolf Fikentscher , Heinrich Mertens , Klaus Reincke
IPC分类号： D06M13/46 , D06M11/30 , D06M13/02 , D06M13/322 , D06M13/355 , D06M13/385 , D06M13/47 , D06M13/477 , D06M101/00 , D06M101/02 , D06M101/10 , D06M101/12 , D06P5/06 , C09B67/00
CPC分类号： D06M13/385 , D06M11/30 , D06M13/355 , Y10S8/917
摘要： Undyed or dyed wool with an antifelting finish is produced by a method in which the wool is chlorinated at a pH of less than 4 and then an aqueous solution of a quaternary product is applied onto the wool, this product being obtained by condensation of(a) piperazine and piperazine derivatives with(b) crosslinking agents, such as epichlorohydrin and ethylene chloride, in a molar ratio of from 1:0.9 to 1:1, and quaternization of the condensate with benzyl chloride, for 0.15 to 1.0 mole of benzyl chloride being employed per equivalent of nitrogen in component (a) in the quaternization.To produce dyed wool with an antifelting finish, dyeing is carried out after the wool has been chlorinated.
摘要翻译：通过以下方法制造具有抗熔涂层的未染色或染色的羊毛，其中羊毛在pH小于4的条件下氯化，然后将季铵产物的水溶液施加到羊毛上，该产品通过（a ）哌嗪和哌嗪衍生物与（b）交联剂，如表氯醇和氯化乙烯，摩尔比为1:0.9至1:1，以及缩合物与苄基氯的季铵化，得到0.15-1.0摩尔苄基氯在季铵化中每组分（a）中每当量的氮被使用。为了生产具有抗熔层的染色羊毛，羊毛被氯化后进行染色。

59. 发明授权

US4425238A Removal of anionic compounds from water 失效
标题翻译：从水中去除阴离子化合物
公开(公告)号：US4425238A
公开(公告)日：1984-01-10
申请号：US350142
申请日：1982-02-19
申请人： Hans-Juergen Degen , Wolf Guender , Friedrich Linhart , Werner Auhorn , Guenter Frey , Werner Streit , Rolf Fikentscher
发明人： Hans-Juergen Degen , Wolf Guender , Friedrich Linhart , Werner Auhorn , Guenter Frey , Werner Streit , Rolf Fikentscher
IPC分类号： C02F1/58 , C02F1/28 , C02F1/52 , C02F1/54 , C02F1/56
CPC分类号： C02F1/54 , C02F1/281 , C02F1/52 , C02F1/5236 , Y10S210/917
摘要： A process for removing anionic compounds from water which is recycled in manufacturing processes, and from waste water, by adding (1) water-soluble products obtained by reacting an alkylating agent, having an aromatic substituent, with a cationic polyelectrolyte and (2) mineral adsorbents and/or a magnesium salt, aluminum salt or iron salt, with formation and flocculation of water-insoluble reaction products.
摘要翻译：通过添加（1）通过使具有芳族取代基的烷基化剂与阳离子聚电解质反应获得的水溶性产物和（2）矿物质，从制造工艺和废水中再循环的水中除去阴离子化合物的方法吸附剂和/或镁盐，铝盐或铁盐，形成和絮凝的水不溶性反应产物。

60. 发明授权

US4383834A Coloring of paper 失效
标题翻译：着色纸
公开(公告)号：US4383834A
公开(公告)日：1983-05-17
申请号：US350143
申请日：1982-02-19
申请人： Hans-Juergen Degen , Wolf Guender , Guenter Frey , Werner Streit , Rolf Fikentscher , Klaus Wulz
发明人： Hans-Juergen Degen , Wolf Guender , Guenter Frey , Werner Streit , Rolf Fikentscher , Klaus Wulz
IPC分类号： D21H19/10 , D21H17/07 , D21H17/55 , D21H21/28 , D21D3/00 , D06P1/46 , D21H3/80 , D21H3/82
CPC分类号： D21H21/28 , D21H17/55 , Y10S8/919
摘要： A process for coloring paper with an acid dye and/or direct dye in an aqueous medium in the presence of a water-soluble reaction product of an alkylating agent, possessing an aromatic substituent, with a cationic polyelectrolyte.The process gives papers with high color strength and substantially avoids cylinder twosidedness of the coloration.
摘要翻译：在具有芳族取代基的烷基化剂与阳离子聚电解质的水溶性反应产物的存在下，在含水介质中用酸性染料和/或直接染料着色纸的方法。该方法提供了具有高色强度的纸张，并且基本上避免了着色的圆筒形二次。

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