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41. 发明授权

US3862209A Process of making nitro phenoxybenzoic acid esters 失效
标题翻译：制备硝基苯甲酸酯的方法
公开(公告)号：US3862209A
公开(公告)日：1975-01-21
申请号：US25278072
申请日：1972-05-12
申请人： MOBIL OIL CORP
发明人： THEISSEN ROBERT JAMES
IPC分类号： C07C205/59 , C07C101/54
CPC分类号： C07C201/08 , C07C201/12 , C07C205/58 , C07C205/59
摘要： Improved process for the synthesis of certain nitro phenoxybenzoic acid esters in which high yield, high purity, herbicidally effective compounds are obtained. In general the improvement comprises: 1. ESTERIFICATION OF A HALOBENZOYL HALIDE WITH ISOPROPANOL THEREBY FACILITATING SEPARATION OF ISOMERIC IMPURITIES FROM THE DESIRED ISOPROPYL-NITROBENZOATE ESTER INTERMEDIATE. 2. TRANSESTERIFICATION OF A PHENOXY DERIVATIVE OF SAID ESTER TO THE DESIRED PHENOXYBENZOIC ACID ESTER.
摘要翻译：用于合成某些硝基苯氧基苯甲酸酯的改进方法，其中获得高产率，高纯度，除草有效的化合物。一般来说，改进包括：

42. 发明授权

US3847974A Continuous production of anthranilic acid 失效
标题翻译：连续生产硫酸
公开(公告)号：US3847974A
公开(公告)日：1974-11-12
申请号：US7862270
申请日：1970-10-06
申请人： BASF AG
发明人： ARMBRUST H , STURM H , KEMPTER F
IPC分类号： C07C67/00 , C07C227/00 , C07C227/04 , C07C227/22 , C07C229/56 , C07D265/26 , C07C101/54
CPC分类号： C07D265/26
摘要： 1. A PROCESS FOR THE CONTINUOUS PRODUCTION OF ANTHRANILIC ACID WHICH COMPRISES REACTING A STRATING COMPOUND SELECTED FROM THE GROUP CONSISTING OF THE ALKALI METAL SALTS OF PHTHALAMIC OF STAGES, THE FRIST REACTION AQUEOUS MEDIUM IN A PLURALITY OF STAGES, THE REACTION STAGES FOR CONVERTING THE STARTING COMPOUND INTO THE ALKALI METAL SALT OF PHENYL ISOCYANATE-2-CARBOXYLIC ACID BEING CARRIED OUT UNDER SUBSTANTIALLY ADIABATIC CONDITIONS WHILE SUBSTANTIALLY AVOIDING ANY BACKMIXING, THE RESULTING REACTION MIXTURE BEING IMMEDIATELY WITHDRAWN FROM THE REACTION ZONE OF SAID FIRST STAGES AND THEN SUPPLIED SUBSTNATIALLY WITHOUT BACKMIXING TO THE REACTION ZONE OF AT LEAST ONE SUBSEQUENT STAGE FOR HYDROLYSIS AND DECARBOXYLATION OF SAID PHENYL ISOCYANATE-2-CARBOXYLIC ACID INTO ANTHRANILLIC ACID, A REDUCING AGENT SELECTED FROM THE GROUP CONSISTING OF SODIUM BOROHYDRIDE, LITHIUM TRIETHOXY ALUMINUM HYDRIDE, SODIUM SULFIDE, SODIUM HYDROGEN SULFIDE, AMMONIUM SULFIDE, SULFUROUS ACID, SULFUR DIOXIDE, SODIUM DITHIONITE, SODIUM, THIOSULFATE, SODIUM FORMALDEHYDE SULFOXYLATE, THIOUREA DIOXIDE, HYDRAZINE AND ITS SALTS, GLUCOSE SODIUM SULFITE AND SODIUM BISULFATE BEING ADDED TO THE REACTION MIXTURE WITHDRAWN FROM THE REACTION ZONE OF SAID FIRST STAGES AND BEFORE THE REACTION HAS BEEN COMPLETED.

43. 发明授权

US3703546A Preparation of 3-amino-2,5-dichlorobenzoic acid 失效
标题翻译： 3-氨基-2,5-二氯苯甲酸的制备
公开(公告)号：US3703546A
公开(公告)日：1972-11-21
申请号：US3703546D
申请日：1968-10-24
申请人： AMCHEM PROD
发明人： LEAPER JOSEPH MICHAEL FARADAY , RAMAN HARVEY PETER JOHN
IPC分类号： C07C63/70 , C07C205/58 , C07C101/54
CPC分类号： C07C67/14 , C07C201/08 , C07C201/16 , C07C205/58 , C07C69/76
摘要： 3-AMINO-2,5-DICHLOROBENZOIC ACID IS PREPARED IN HIGH YIELD BY CHLORINATING BENZOYLCHLORIDE AND ESTERIFYING THE RESULTING MIXTURE, SEPARATING THE DESIRED 2,5-DICHLORO ISOMER FROM THE MIXTURE BY FREEZE CRYSTALLIZATION, NITRATING AND ISOLATING 3-NITRO-2,5-DICHLOROBENZOIC ACID FROM THE MIXTURE OF NITRO ISOMERS BY ACID HYDROLYSIS AND TREATING WITH A REDUCING AGENT.

44. 发明授权

US3678094A Substituted anilino carboxylic acids 失效
标题翻译：取代的苯胺羧酸
公开(公告)号：US3678094A
公开(公告)日：1972-07-18
申请号：US3678094D
申请日：1970-04-20
申请人： MERCK & CO INC
发明人： SHEN TSUNG-YING , WITZEL BRUCE E , WALFORD GORDON L
IPC分类号： A61K31/60 , C07C101/54
CPC分类号： A61K31/60 , Y10S514/866 , Y10S514/869 , Y10S514/87 , Y10S514/916
摘要： New substituted anilino carboxylic acids and non-toxic pharmaceutically acceptable salts, esters, amides, and various derivatives thereof are claimed. The substituted anilinocarboxylic acids described herein have anti-inflammatory, antipyretic, and analgesic activity. Also included is a method of preparing said anilino carboxylic acids and method of treatment using certain of these substituted anilino carboxylic acids.
摘要翻译：要求保护新的取代的苯胺基羧酸和无毒的药学上可接受的盐，酯，酰胺及其各种衍生物。本文所述的取代的苯胺基羧酸具有抗炎，抗热解和止痛活性。还包括制备所述苯胺基羧酸的方法和使用某些这些取代的苯胺基羧酸进行处理的方法。

45. 发明授权

US3641133A Intermediates in the preparation of 4-aminodibenzo(a d)-cycloalken-5-ones 失效
标题翻译： 4-氨基苯并（A） - 环烯-5-酮的制备中的中间体
公开(公告)号：US3641133A
公开(公告)日：1972-02-08
申请号：US3641133D
申请日：1968-09-30
申请人： SANDOZ AG
发明人： GALANTAY EUGENE E , OTT HANS
IPC分类号： C07C101/54
CPC分类号： C07D213/68 , Y10S514/96
摘要： A 4-CHLORO-7-AMINO-3-SUBSTITUTED PHTALIDE, E.G., 3-BPHENETHYL-4-CHLORO-7-METHYLAMINOPHTHALIDE, IS SAPONIFIED AND THE SAPONIFICATION PRODUCT REDUCED TO OBTAIN THE CORRESPONDING 6-PHEN(ALKYL)-ANTHRANILIC ACID, E.G., 6-B-PHENETHYL-N-METHYL-ANTHRANILIC ACID, WHICH IS THEN CYCLIZED TO THE CORRESPONDING PHARMACEUTICALLY USEFUL 4-AMINO-10,11DIHYDRO-5H-DIBENZO(A,D)CYCLOHEPTEN-5-ONE OR 4-AMINO-5, 10,11,12-TETRAHYDRODIBENZO(A,D)CYCLOOCTEN-5-ONE.

46. 发明授权

US3574722A Carboxylation of aromatic compounds 失效
标题翻译：芳香化合物的羧基化
公开(公告)号：US3574722A
公开(公告)日：1971-04-13
申请号：US3574722D
申请日：1968-03-20
申请人： UNIVERSAL OIL PROD CO
发明人： LOUVAR JAMES J
IPC分类号： C07C51/00 , C07C205/57 , C07C63/04 , C07C101/54
CPC分类号： C07C201/12 , C07C51/00 , C07C201/16 , Y02P20/582 , C07C63/04 , C07C63/36 , C07C205/57
摘要： AROMATIC COMPOUNDS MAY BE CARBOXYLATED BY TREATING THE COMPOUND WITH A SOLUTION OF BORON TRIFLUORIDE IN A CARBOXYLIC ACID TO FORM CARBOXYLATED AROMATIC COMPOUNDS.

47. 发明授权

US4658054A Process for the preparation of 5,6-dialkoxyanthranilic acids 失效
标题翻译： 5,6-二烷氧基邻氨基苯甲酸的制备方法
公开(公告)号：US4658054A
公开(公告)日：1987-04-14
申请号：US759974
申请日：1985-07-29
申请人： Richard A. Conley
发明人： Richard A. Conley
IPC分类号： C07C229/64 , C07C67/00 , C07C229/52 , C07C229/58 , C07C231/00 , C07C231/02 , C07C231/08 , C07C231/12 , C07C233/16 , C07C233/54 , C07C233/91 , C07C101/54
CPC分类号： C07C233/16
摘要： A process for the preparation of 5,6-dialkoxyanthranilic acids is described. The 5,6-dialkoxyanthranilic acids are useful in the preparation of substituted quinazolinediones which are active cardiotonic agents.
摘要翻译：描述了制备5,6-二烷氧基邻氨基苯甲酸的方法。 5,6-二烷氧基邻氨基酸可用于制备作为活性强心剂的取代喹唑啉二酮。

48. 发明授权

US4633009A Synthesis of methyl N-methylanthranilate 失效
标题翻译： N-甲基邻氨基苯甲酸甲酯的合成
公开(公告)号：US4633009A
公开(公告)日：1986-12-30
申请号：US745894
申请日：1985-06-18
申请人： David I. Lerner
发明人： David I. Lerner
IPC分类号： C07C101/54
CPC分类号： C07C227/18
摘要： Methyl N-methylanthranilate is prepared by reductive alkylation of methylanthranilate with formaldehyde and hydrogen in the presence of a hydrogenation catalyst and an acid catalyst.
摘要翻译：在氢化催化剂和酸催化剂存在下，通过用甲醛和氢还原烷基化甲基邻氨基苯甲酸甲酯来制备N-甲基异戊酸甲酯。

49. 发明授权

US4306074A Preparation of a mixture of an alkyl 3-chloroanthranilate and an alkyl 6-chloroanthranilate 失效
标题翻译：制备3-氯邻氨基苯甲酸烷基酯和6-氯邻氨基苯甲酸烷基酯的混合物
公开(公告)号：US4306074A
公开(公告)日：1981-12-15
申请号：US153576
申请日：1980-05-27
申请人： Peter Tonne , Heinz-Guenter Oeser , Dietrich Mangold
发明人： Peter Tonne , Heinz-Guenter Oeser , Dietrich Mangold
IPC分类号： C07C67/00 , C07C227/00 , C07C227/12 , C07C227/22 , C07C229/56 , C07D209/48 , C07D265/26 , C07C101/54
CPC分类号： C07D209/48 , C07D265/26
摘要： A mixture of an alkyl 3-chloroanthranilate and an alkyl 6-chloroanthranilate, with a particular molar ratio of the components, is prepared by (a) reacting 3-chlorophthalic anhydride with ammonia, an alkali metal hydroxide and an alkali metal hypochlorite or (b) converting 3-chlorophthalic anhydride to 3-chlorophthalimide followed by reaction of the latter with an alkali metal hydroxide and an alkali metal hypochlorite, and, finally, esterifying the mixture of 5-chloroisatoic anhydride and 8-chloroisatoic anhydride, obtained by method (a) or method (b), with an alkanol.The compounds obtainable by the process of the invention are valuable starting materials for the preparation of dyes, crop protection agents and scents.
摘要翻译：通过（a）使3-氯邻苯二甲酸酐与氨，碱金属氢氧化物和碱金属次氯酸盐或（b）反应，制备具有特定摩尔比的组分的3-氯邻氨基苯甲酸烷基酯和6-氯氨基甲酸烷基酯的混合物）将3-氯邻苯二甲酸酐转化为3-氯邻苯二甲酰亚胺，随后将其与碱金属氢氧化物和碱金属次氯酸盐反应，最后酯化通过方法（a）得到的5-氯代酸酐和8-氯代酸酐的混合物）或方法（b）与链烷醇反应。通过本发明的方法可获得的化合物是用于制备染料，作物保护剂和香料的有价值的起始材料。

50. 发明授权

US4260557A Polymer containing amino groups and hydroxyl and/or mercapto groups and the use thereof for the production of polyurethane resins 失效
标题翻译：含有氨基和羟基和/或巯基的聚合物及其用于生产聚氨酯树脂的用途
公开(公告)号：US4260557A
公开(公告)日：1981-04-07
申请号：US33343
申请日：1979-04-26
申请人： Jan Mazanek , Johannes Blahak
发明人： Jan Mazanek , Johannes Blahak
IPC分类号： C08G2/00 , C08G2/18 , C08G18/00 , C08G18/50 , C08G18/52 , C08G65/00 , C08G65/32 , C08G65/332 , C08G65/333 , C08G65/338 , C08G75/02 , C07C153/023 , C07C101/54
CPC分类号： C08G75/02 , C08G18/5027 , C08G18/5072 , C08G18/52 , C08G65/332 , C08G65/33306 , C08G65/33324 , C08G65/338
摘要： The invention relates to compositions containing both amino groups and hydroxyl and/or mercapto groups. The products are obtained by reacting relatively high molecular weight polyols and/or polythiols with less than equivalent quantities of isatoic acid anhydride.
摘要翻译：本发明涉及含有氨基和羟基和/或巯基的组合物。该产物通过使相对较高分子量的多元醇和/或多硫醇与少于等当量的丙酮酸酐反应而获得。

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