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41. 发明申请

US20090087698A1 MEMBRANE ELECTRODE ASSEMBLY WITH HYDROGENATABLE MATERIAL FOR A FUEL CELL 有权
标题翻译：用于燃料电池的可加氢材料的膜电极组件
公开(公告)号：US20090087698A1
公开(公告)日：2009-04-02
申请号：US12208411
申请日：2008-09-11
申请人： ANDREAS HUTH , CHRISTIANE JACKSCH , MARTIN THOMAS
发明人： ANDREAS HUTH , CHRISTIANE JACKSCH , MARTIN THOMAS
IPC分类号： H01M8/04 , H01M8/02 , H01M8/10
CPC分类号： H01M8/04067 , C01B6/02 , C01B6/04 , C01B6/24 , H01M4/8605 , H01M4/8642 , H01M8/04216 , H01M8/04268 , H01M2008/1095
摘要： The invention relates to a membrane-electrode assembly (14) for a fuel cell (10) with (a) a proton-conducting membrane (16), (b) two catalyst layers (20a, 20b) adjoining both sides of the membrane (16), wherein the catalyst layers have an electrically conductive base material and at least one catalytic material deposited on the base material, and (c) two gas diffusion layers (22a, 22b) adjoining the catalyst layers. The membrane (16) and/or at least one of the catalyst layers (20a, 20b) and/or at least one of the gas diffusion layers (22a, 22b) includes at least one hydrogenatable material capable of binding hydrogen in a reversible exothermic hydrogenation operation by forming a hydride, depending on the temperature and/or pressure. The hydrogenatable material can be distributed in the gas diffusion layer (22a, 22b) and/or in the catalyst layer (20a, 20b) or can be present as a separate layer (32, 34) on at least one side of the gas diffusion electrode (18a, 18b) or the membrane (16).
摘要翻译：本发明涉及一种用于燃料电池（10）的膜 - 电极组件（14），其具有（a）质子传导膜（16），（b）两个邻接膜两侧的催化剂层（20a，20b） 16），其中所述催化剂层具有导电基材和沉积在所述基材上的至少一种催化材料，和（c）与所述催化剂层相邻的两个气体扩散层（22a，22b）。所述膜（16）和/或所述催化剂层（20a，20b）中的至少一个和/或所述气体扩散层（22a，22b）中的至少一个包括至少一种能够在可逆放热中结合氢的可氢化材料根据温度和/或压力，通过形成氢化物进行氢化操作。可氢化材料可以分布在气体扩散层（22a，22b）和/或催化剂层（20a，20b）中，或者可以作为分离层（32,34）存在于气体扩散层的至少一侧电极（18a，18b）或膜（16）。

42. 发明申请

US20070042223A1 Light element complex hydride film and method for synthesis thereof 审中-公开
标题翻译：轻元素复合氢化物膜及其合成方法
公开(公告)号：US20070042223A1
公开(公告)日：2007-02-22
申请号：US10575076
申请日：2004-10-08
申请人： Shin-ichi Orimo , Yuko Nakamori , Masaki Yokoyama , Tetsuto Yamagishi
发明人： Shin-ichi Orimo , Yuko Nakamori , Masaki Yokoyama , Tetsuto Yamagishi
IPC分类号： C23C16/00 , B32B9/00
CPC分类号： C01B6/04 , C01B3/001 , C01B3/0084 , C01B6/003 , C01B6/21 , Y02E60/327
摘要： The present invention provides a complex hydride (such as LiBH4 or LiNH2) of a lightweight metal thin film having a low melting point, and to a method for manufacturing the same, and the present invention relates to a method for manufacturing a thin film of a complex hydride having a nano structure, by vapor deposition, using as raw materials one or more metals selected from among lightweight metals having a low melting point (such as Li, Na, Mg, K, and Ca) and one or more elements selected from among nitrogen, carbon, boron, and aluminum, and to a light element complex hydride thin film, and with the method of the present invention, it is possible conveniently to form a thin film of a complex hydride of a lightweight metal having a low melting point, and a complex hydride thin film thus formed is useful, for example, as a multi-functional material having superconductivity, optical characteristics, hydrogen storage characteristics, and the like.
摘要翻译：本发明提供具有低熔点的轻质金属薄膜的复合氢化物（例如LiBH 4或LiNH 2/2）及其制造方法本发明涉及一种具有纳米结构的复合氢化物的薄膜的制造方法，通过气相沉积法，使用一种或多种选自低熔点的轻金属（例如Li， Na，Mg，K和Ca）和一种或多种选自氮，碳，硼和铝的元素，以及轻质复合氢化物薄膜，并且利用本发明的方法，形成具有低熔点的轻质金属的复合氢化物的薄膜，并且由此形成的复合氢化物薄膜可用作例如具有超导性，光学特性，储氢特性的多功能材料喜欢。

43. 发明授权

US06680042B1 Method of rapidly carrying out a hydrogenation of a hydrogen storage material 失效
标题翻译：快速进行储氢材料氢化的方法
公开(公告)号：US06680042B1
公开(公告)日：2004-01-20
申请号：US09706809
申请日：2000-11-07
申请人： Robert Schulz , Salim Bouaricha , Jacques Huot , Daniel Guay
发明人： Robert Schulz , Salim Bouaricha , Jacques Huot , Daniel Guay
IPC分类号： C01B600
CPC分类号： C01B6/04 , C01B3/0005 , Y02E60/325 , Y02E60/327
摘要： Disclosed is a method for rapidly carrying out a hydrogenation of a material capable of absorbing hydrogen. It was discovered that when a powder of a material capable of absorbing hydrogen is ground under a hydrogen pressure, not at room temperature but at a higher temperature (about 300° C. in the case of magnesium) and in the presence of a hydrogenation activator such as graphite and optionally a catalyst, it is possible to transform completely the powder of this material into a hydride. Such a transformation is achieved in a period of time less than 1 hour whereas the known methods call for periods of time as much as 10 times longer. This is an unexpected result which gives rise to a considerable reduction in the cost of manufacture of an hydride, particularly MgH2.
摘要翻译：公开了一种快速进行能够吸收氢的材料的氢化的方法。已经发现，当在氢气压力下，不是在室温下而是在较高的温度（在镁的情况下约为300℃）和在氢化活化剂的存在下研磨能够吸收氢的材料的粉末例如石墨和任选的催化剂，可以将该材料的粉末完全转变为氢化物。这种转变是在不到1小时的时间内实现的，而已知的方法需要多达10倍的时间。这是意想不到的结果，其导致氢化物，特别是MgH 2的制造成本的显着降低。

44. 发明授权

US06593017B1 High capacity calcium lithium based hydrogen storage material and method of making the same 失效
标题翻译：高容量钙锂储氢材料及其制备方法
公开(公告)号：US06593017B1
公开(公告)日：2003-07-15
申请号：US10059778
申请日：2002-01-30
申请人： Zhaosheng Tan , Krishna Sapru
发明人： Zhaosheng Tan , Krishna Sapru
IPC分类号： H01M818
CPC分类号： C01B3/065 , C01B6/04 , C01B6/24 , H01M8/065 , Y02E60/321 , Y02E60/327 , Y02E60/362 , Y02P70/56
摘要： A nonreversible metal hydride for use as a hydrogen fuel. The nonreversible metal hydride is formed from an intermetallic compound having the formula Ca1+aLi2+b. The Ca1+aLi2+b is formed by melting amounts of elemental lithium and calcium together by induction heating in an argon atmosphere. The Ca1+aLi2+b is cooled and crushed into a powder. The alloy powder is subsequently hydrogenated at ambient temperatures or lower. Resulting is a metal hydride having exceptional reactivity to water during hydrolysis due to its nano-crystalline structure. Dehydrogenation of the metal hydride does not regularly occur due to the absorbed hydrogen being chemically bonded to the lithium and calcium. The Ca1+aLi2+b hydride may be used in a variety of applications as a hydrogen fuel and the Ca1+aLi2+b alloy may be used as a desiccant for removing moisture from hydrogen or hydrogen containing streams.
摘要翻译：用作氢燃料的不可逆金属氢化物。不可逆金属氢化物由具有式Ca1 + aLi2 + b的金属间化合物形成。 Ca1 + aLi2 + b通过在氩气气氛中的感应加热一起熔化元素锂和钙而形成。将Ca1 + aLi2 + b冷却并粉碎成粉末。随后在环境温度或更低温度下将合金粉末氢化。导致金属氢化物由于其纳米晶体结构而在水解过程中对水具有特殊的反应性。由于吸收的氢化学键合到锂和钙上，金属氢化物的脱氢并不经常发生。 Ca1 + aLi2 + b氢化物可用作各种应用中的氢燃料，Ca1 + aLi2 + b合金可用作干燥剂，用于从含氢或含氢气流中除去水分。

45. 发明授权

US5141676A Soluble magnesium hydrides, method of preparing them, and use thereof 失效
标题翻译：可溶性氢氧化镁，其制备方法及其用途
公开(公告)号：US5141676A
公开(公告)日：1992-08-25
申请号：US686727
申请日：1991-04-17
申请人： Borislav Bogdanovic , Manfred Schwickardi
发明人： Borislav Bogdanovic , Manfred Schwickardi
IPC分类号： C01B6/04 , C07D453/02 , C07F3/00 , C07F3/02 , C07F5/02 , C07F5/06
CPC分类号： C07D453/02 , C01B6/04 , C07F3/003 , C07F3/02 , C07F5/027 , C07F5/062
摘要： Organic-solvent soluble magnesium hydrides of the formulas(MgH.sub.2).sub.n. MgQ.sub.2 (II)(MgH.sub.2).sub.n. RMgX (III) ##STR1## are prepared by catalytically hydrogenating finely powdered magnesium, optionally in the presence of a magnesium halide, in an organic solvent in the presence of their MgH.sub.2 -free counterparts in whichQ is an alkyl, alkenyl, alkoxy, dialkylamino, aralkyl, aryl or diarylamino group, each with up to 18 carbon atoms,R is an alkenyl, aralkyl or aryl group, each with up to 18 carbon atoms,X is chlorine, bromine, or iodine,--E D.fwdarw. is a chelating ligand,E is --CH.sub.2, --N(R)-- or --O--, is an alkylene radical of the formula --(CH.sub.2).sub.p,D is a dialkylamino, diarylamino or alkoxy group, each with up to 19 carbon atoms,M is aluminum or boron,m is 1, 2, or 3, and1
摘要翻译：式（MgH 2）n的有机溶剂可溶性氢氧化镁。 MgQ2（II）（MgH2）n。（VI）（VI）（VI）（MgH 2）n.MQmX 3-m（VII）和（VIII）通过催化氢化细粉末镁，任选地在卤化镁的存在下，在有机溶剂中，在其不含MgH 2的对应物存在下，其中Q为烷基，链烯基，烷氧基，二烷基氨基，芳烷基，芳基或二芳基氨基，每个具有多至18个碳原子，R 是具有至多18个碳原子的烯基，芳烷基或芳基，X是氯，溴或碘，-E D->是螯合配体，E是-CH 2，-N（R） - 或-O - 是式 - （CH 2）p的亚烷基，D是二烷基氨基，二芳基氨基或烷氧基，各自具有至多19个碳原子，M是铝或硼，m是1,2或3，和1

46. 发明授权

US4605547A Continuous hydrogenation of lithium into lithium hydride 失效
标题翻译：将锂连续氢化成氢化锂
公开(公告)号：US4605547A
公开(公告)日：1986-08-12
申请号：US707153
申请日：1985-03-01
申请人： Jean-Yves Dumousseau , Jean Grosbois , Serge Jacubert
发明人： Jean-Yves Dumousseau , Jean Grosbois , Serge Jacubert
IPC分类号： C01B6/04 , C01F15/00
CPC分类号： C01B6/04
摘要： Lithium is continuously converted into lithium hydride, is suitable phase contactor/decanter apparatus, by continuously hydrogenating in a first reaction zone, at elevated temperatures, an agitated intimate admixture of metallic lithium in a mixture of molten salts, continuously discharging the effluent of said hydrogenation reaction to a second zone of decantation, whereby said effluent is separated into a floating light phase essentially consisting of unreacted lithium metal and a heavy phase which comprises product lithium hydride dissolved in said mixture of molten salts, continuously recycling floating light phase back to the hydrogenation reaction zone, continuously withdrawing heavy phase from said zone of decantation, and recovering product lithium hydride from said withdrawn heavy phase.
摘要翻译：锂是连续转化为氢化锂，是适合的相接触器/滗析器装置，通过在高温下连续氢化第一反应区，在熔融盐混合物中搅拌均匀的金属锂混合物，连续排出所述氢化物的流出物反应到第二倾析区域，由此所述流出物被分离成基本上由未反应的锂金属和重相组成的漂浮光相，所述重相包含溶解在所述熔融盐混合物中的产物氢化锂，将浮质轻相连续回流回氢化反应区，从所述倾析区连续取出重相，并从所述抽出的重相中回收产物氢化锂。

47. 发明授权

US4396589A Alkali metal complex compounds, and their use in the hydrogenation and nitridation of alkali metals 失效
标题翻译：碱金属络合物，以及它们在碱金属氢化和氮化中的应用
公开(公告)号：US4396589A
公开(公告)日：1983-08-02
申请号：US426495
申请日：1982-09-29
申请人： Borislav Bogdanovic
发明人： Borislav Bogdanovic
IPC分类号： C07C49/92 , B01J31/00 , B01J31/16 , B01J31/22 , C01B6/04 , C01B21/06 , C07C45/00 , C07C67/00 , C07C325/00 , C07C325/02 , C07C327/10 , C07C327/18 , C07D307/06 , C07D339/04 , C07D495/04 , C07F1/00 , C07F1/02 , C07F1/04 , C07F1/06
CPC分类号： B01J31/2204 , B01J31/1805 , B01J31/2291 , B01J31/2295 , C01B21/0607 , C01B21/061 , C01B6/04 , C07D339/04 , C07D495/04 , C07F1/005 , B01J2231/62 , B01J2531/10 , B01J2531/11 , B01J2531/12
摘要： The invention includes novel alkali metal complex compounds which are useful, inter alia for the hydrogenation of alkali metals at room temperature or below room temperature to form hydrides or nitrides.
摘要翻译：本发明包括新的碱金属络合物，其特别用于在室温或室温以下氢化碱金属以形成氢化物或氮化物。

48. 发明授权

US4041136A Process for the production of silane 失效
标题翻译：硅烷生产工艺
公开(公告)号：US4041136A
公开(公告)日：1977-08-09
申请号：US726115
申请日：1976-09-24
申请人： Robert E. Franklin , Arthur W. Francis , Gregorio Tarancon
发明人： Robert E. Franklin , Arthur W. Francis , Gregorio Tarancon
IPC分类号： C01B6/04 , C01B33/04 , C01B33/107
CPC分类号： C01B33/043 , C01B6/04 , Y10S423/12
摘要： A process for the production of silane in a reaction vessel comprising (i) a single closed chamber, (ii) a hollow tube open at both ends, said tube being disposed in the lower portion of the chamber; and (iii) means for circulating liquid in the lower portion of the chamber in such a manner that the liquid flows in a downward direction through the tube and in an upward direction outside of the tubeComprising the following steps:A. maintaining a melt of lithium chloride in the lower portion of the chamber, the level of the melt being above the tube;B. activating the circulating means;C. introducing liquid lithium into the melt in such a manner that at least a part thereof is brought to the surface of the melt;D. introducing hydrogen gas above the surface of the melt in such a manner that hydrogen gas reacts with lithium at the surface of the melt to form lithium hydride,The lithium, lithium hydride, and melt being admixed by the circulating means to provide a homogeneous mixture thereof;E. introducing, as a gas, a compound or a mixture of compounds having the formulaSiH.sub.x Cl.sub.4.sub.-x whereinx is 0 or an integer from 1 to 3 in such a manner that the gas is dispersed by the circulating means into the mixture whereby the gas contacts the lithium hydride to form silane gas; andF. removing the silane gas from the chamber.
摘要翻译：一种在反应容器中生产硅烷的方法，包括（i）单个封闭室，（ii）在两端开口的中空管，所述管设置在所述室的下部; 和（iii）使液体在室的下部循环的装置，使得液体沿着向下的方向通过管并且沿着包括以下步骤的管的向上方向流动：

49. 发明授权

US4007257A Alkali metal hydride formation 失效
标题翻译：碱金属氢化物形成
公开(公告)号：US4007257A
公开(公告)日：1977-02-08
申请号：US562807
申请日：1975-03-27
申请人： Raymond Urgel Lemieux , Emerson Cecil Sanford , John Fraser Prescott
发明人： Raymond Urgel Lemieux , Emerson Cecil Sanford , John Fraser Prescott
IPC分类号： C01B3/00 , C01B4/00 , C01B6/04 , C01B1/02
CPC分类号： C01B4/00 , C01B3/0015 , C01B3/0026 , C01B6/04 , Y02E60/327 , Y02E60/328
摘要： The present invention relates to a method of producing alkali metal hydrides by absorbing hydrogen gas under pressure into a mixture of lower alkyl mono amines and alkali metal alkyl amides selected from sodium and potassium amides formed from said amines. The present invention also includes purification of a mixture of the amines and amides which contain impurities, such as is used as a catalytic exchange liquid in the enrichment of deuterium, involving the formation of the alkali metal hydride.
摘要翻译：本发明涉及通过在压力下将氢气吸收到低级烷基一胺和选自所述胺形成的酰胺钠和碱金属烷基酰胺的混合物中来制备碱金属氢化物的方法。本发明还包括纯化含有杂质的胺和酰胺的混合物，例如用作富含氘的催化交换液体，涉及形成碱金属氢化物。

50. 发明授权

US3864464A Preparation of beryllium hydride 失效
标题翻译：氢化铍的制备
公开(公告)号：US3864464A
公开(公告)日：1975-02-04
申请号：US43023765
申请日：1965-01-27
申请人： ETHYL CORP
发明人： SHEPHARD JR LAWRENCE H , KOBETZ PAUL , LARAN ROY J , JOHNSON JR ROBERT W
IPC分类号： C01B6/04 , C07F3/00 , C07F5/02 , C01B6/00
CPC分类号： C07F5/027 , C01B6/04 , C07F3/00
摘要： 1. Process for the preparation of beryllium hydride which comprises reacting, at a temperature of from 75* to about 200*C, an organodiborane of the general formula R4B2H2 with a dihydrocarbyl beryllium compound of the general formula R2''Be wherein R and R'' represent radicals selected from the group consisting of alkyl, monocyclic cycloalkyl and monocyclic aryl radicals containing from 1 to about 10, 5 to about 10 and 6 to about 10 carbon atoms, respectively, and recovering beryllium hydride from the reaction product.
摘要翻译： 1.制备氢化铍的方法，其包括在75℃至约200℃的温度下将通式为R 4 B 2 H 2的有机基二硼烷与通式为R 2'B e的二烃基铍化合物反应，其中R和R' 分别表示选自含有1至约10至5至约10至6至约10个碳原子的烷基，单环环烷基和单环芳基的基团，并从反应产物中回收氢化铍。

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