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41. 发明授权

US06951966B1 Orthoalkylation catalyst for phenol and process for producing orthoalkylated phenol with use thereof 失效
标题翻译：苯酚正烷基化催化剂及其制备原烷基化苯酚的方法
公开(公告)号：US06951966B1
公开(公告)日：2005-10-04
申请号：US09555255
申请日：1999-09-28
申请人： Mitsuhiro Higashi , Masamitsu Tanaka , Kenji Ekawa
发明人： Mitsuhiro Higashi , Masamitsu Tanaka , Kenji Ekawa
IPC分类号： B01J21/10 , B01J23/34 , C07C37/00 , C07C37/16
CPC分类号： C07C37/16 , B01J21/10 , B01J23/34 , Y02P20/52 , Y02P20/584 , C07C39/07
摘要： The orthoalkylation catalyst for phenols of the invention is one produced by calcining a catalyst precursor comprising basic magnesium carbonate (a) and magnesium oxide (b) optionally together with manganese oxalate (c), the basic magnesium carbonate (a) and magnesium oxide (b) being mixed together at a weight ratio ((a)/(b)) of 20/80 to 80/20. The process for producing an orthoalkylated phenol according to the invention comprises performing a vapor phase reaction of a phenol with an alkyl alcohol in the presence of the above orthoalkylation catalyst so that an orthoalkylated phenol is obtained.The invention enables obtaining an orthoalkylation catalyst for phenols which has high activity and high selectivity, has long catalytic life and exhibits more stable catalytic life than those of conventional orthoalkylation catalysts for phenols. Moreover, by virtue of the use of the catalyst capable of exerting these effects, there can be obtained a process for producing an orthoalkylated phenol which ensures prolonged and constant catalyst regeneration cycle.
摘要翻译：本发明酚类的正烷基化催化剂是通过将含有碱式碳酸镁（a）和氧化镁（b）的催化剂前体任选与草酸锰（c），碱式碳酸镁（a）和氧化镁（b））以20/80至80/20的重量比（（a）/（b））混合在一起。根据本发明的用于生产原烷基化苯酚的方法包括在上述正烷基化催化剂的存在下进行酚与烷基醇的气相反应，从而得到原烷基化苯酚。本发明能够获得具有高活性和高选择性的酚的正烷基化催化剂，具有长的催化寿命并且比常规的酚类正烷基化催化剂的催化寿命更加稳定。此外，通过使用能够发挥这些效果的催化剂，可以获得一种生产原烷基化苯酚的方法，其确保延长和恒定的催化剂再生循环。

42. 发明授权

US06872858B2 Diphenol and process for producing the same 有权
标题翻译：二苯酚及其制备方法
公开(公告)号：US06872858B2
公开(公告)日：2005-03-29
申请号：US10467187
申请日：2002-02-07
申请人： Kouji Muragaki , Tadashi Hiramine , Hiroyasu Ohno
发明人： Kouji Muragaki , Tadashi Hiramine , Hiroyasu Ohno
IPC分类号： C07C37/06 , C07C37/52 , C07C39/15 , C07C39/17 , C07C39/23 , C07L39/12
CPC分类号： C07C39/23 , C07C37/003 , C07C37/06 , C07C37/20 , C07C37/52 , C07C39/15 , C07C39/17 , C07C2601/14 , C07C2601/16
摘要： The invention provides a diphenol represented by the general formula (I) wherein X is a divalent cyclic hydrocarbon group selected from 1-cyclohexene-1,4-ylene group, 1,4-cyclohexylene group and p-phenylene group, R is an alkyl group of 1-4 carbon atoms, n is 0 or an integer of 1-3 when X is 1-cyclohexene-1,4-ylene group and an integer of 1-3 when X is 1,4-cyclohexylene group or p-phenylene group. The invention further provides a process for the production of the same.
摘要翻译：本发明提供由通式（I）表示的二酚，其中X为选自1-环己烯-1,4-亚基，1,4-亚环己基和对亚苯基的二价环状烃基，R为烷基 1-4个碳原子的基团，当X是1-环己烯-1,4-亚基时，n是0或1-3的整数，当X是1,4-亚环己基或对 - 亚苯基。本发明还提供了一种制备该方法的方法。

43. 发明授权

US5847237A Catalyst for ortho-alkylation of phenols, a precursor thereof, and production of ortho-alkylated phenols by use of said catalyst 失效
标题翻译：用于酚的邻烷基化的催化剂，其前体，以及通过使用所述催化剂生产邻烷基化酚
公开(公告)号：US5847237A
公开(公告)日：1998-12-08
申请号：US675497
申请日：1996-07-03
申请人： Shunji Yago , Takashi Kakiuchi , Keiji Arimatsu , Fujihisa Matsunaga
发明人： Shunji Yago , Takashi Kakiuchi , Keiji Arimatsu , Fujihisa Matsunaga
IPC分类号： B01J23/34 , B01J31/26 , B01J37/08 , C07B61/00 , C07C37/16 , C07C39/06 , C07C37/00 , B01J23/32
CPC分类号： B01J37/082 , B01J23/34 , B01J37/086 , C07C37/16
摘要： There is disclosed a catalyst for ortho-alkylation of phenols obtained by calcination of a catalyst precursor comprising a dry mixture of: (a) manganese oxalate; (b) phenolic resin fine particles; and (c) at least one magnesium compound selected from the group consisting of basic magnesium carbonate and magnesium hydroxide. There is further disclosed a process for producing ortho-alkylated phenols by the gas phase reaction between an alkyl alcohol and a phenol in the presence of the ortho-alkylation catalyst defined above.
摘要翻译：公开了一种通过煅烧催化剂前体而获得的酚的正烷基化催化剂，该催化剂前体包含以下干燥混合物：（a）草酸锰; （b）酚醛树脂微粒; 和（c）至少一种选自碱式碳酸镁和氢氧化镁的镁化合物。还公开了在上述定义的烷基化催化剂存在下，通过烷基醇和苯酚之间的气相反应生产邻烷基化酚的方法。

44. 发明申请

US20220380286A1 METHOD FOR PRODUCING 2,2'-BIS(CARBOXYMETHOXY)-1,1'-BINAPHTHYL 有权
公开(公告)号：US20220380286A1
公开(公告)日：2022-12-01
申请号：US17771427
申请日：2020-11-26
申请人： HONSHU CHEMICAL INDUSTRY CO., LTD.
发明人： Daichi SAKUMA , Takeru SUTO
IPC分类号： C07C51/02 , C07C51/47
摘要： A method for producing 2,2′-bis(carboxymethoxy)-1,1′-binaphthyl includes a separation step of separating a metal salt of 2,2′-bis(carboxymethoxy)-1,1′-binaphthyl from a reaction mixture by solid-liquid separation. In the method, a 2,2′-bis(alkoxycarbonylmethoxy)-1,1′-binaphthyl is used as a starting material.

45. 发明申请

US20220127216A1 PRODUCTION METHOD FOR 4-HYDROXY-2-METHYLBENZOIC ACID 有权
公开(公告)号：US20220127216A1
公开(公告)日：2022-04-28
申请号：US17433192
申请日：2020-03-03
申请人： HONSHU CHEMICAL INDUSTRY CO., LTD.
发明人： Ryota IMAI , Kazuhito ASHIDA
IPC分类号： C07C51/15 , C07C51/377
摘要： An object is to provide a novel production method for 4-hydroxy-2-methylbenzoic acid that is suitable for industrial use. As a solution, a production method for 4-hydroxy-2-methylbenzoic acid that includes performing a step (I) of reacting a compound represented by general formula (1) with carbon dioxide to obtain a compound represented by general formula (2), and then a step (II) of dealkylating the compound represented by general formula (2), is provided.

46. 发明申请

US20210054142A1 AROMATIC POLYCARBONATE OLIGOMER SOLID 有权
公开(公告)号：US20210054142A1
公开(公告)日：2021-02-25
申请号：US16608138
申请日：2018-05-17
申请人： HONSHU CHEMICAL INDUSTRY CO., LTD.
发明人： Mitsutaka OZAKI , Miwa HASHIMOTO , Takeru SUTO , Ryoto KANO
IPC分类号： C08G64/06 , C08G63/64
摘要： The purpose of the present invention is to provide an aromatic polycarbonate oligomer solid with substantially reduced low-molecular-weight components, no or a substantially reduced amount of chlorine-containing compounds, high loose bulk density, and ease of handling. The aromatic polycarbonate oligomer solid contains a repeating unit represented by general formula (1), has a weight average molecular weight of 500 to 10000, low-molecular-weight components less than or equal to 5.0 area % measured with high-speed liquid chromatography, and a loose bulk density of greater than or equal to 0.30 g/cm3.

47. 发明申请

US20210053916A1 NOVEL ALKOXYMETHYL-SUBSTITUTED BISPHENOL COMPOUND 有权
公开(公告)号：US20210053916A1
公开(公告)日：2021-02-25
申请号：US16475637
申请日：2018-01-11
申请人： HONSHU CHEMICAL INDUSTRY CO., LTD.
发明人： Akihito NASU
IPC分类号： C07C317/22
摘要： The present invention addresses the problem of providing a novel alkoxymethyl-substituted bisphenol compound having exceptional storage stability and exceptional solvent solubility, heat resistance, and optical properties when used as a resin raw material. This problem can be solved by using an alkoxymethyl-substituted bisphenol compound represented by General Formula (1): (wherein each R independently represents an alkyl group having 1 to 4 carbon atoms).

48. 发明授权

US09522868B2 Tetrakis(ether-substituted formylphenyl) 有权
标题翻译：四（乙醚取代甲酰基苯基）
公开(公告)号：US09522868B2
公开(公告)日：2016-12-20
申请号：US14868233
申请日：2015-09-28
申请人： HONSHU CHEMICAL INDUSTRY CO., LTD.
发明人： Akira Yoshitomo , Tatsuya Iwai
IPC分类号： C07C69/76 , C07C69/738 , C07C39/17 , C07C47/57 , C07C59/70 , C07C69/712
CPC分类号： C07C69/738 , C07C39/17 , C07C47/57 , C07C59/70 , C07C69/712 , C07C2601/14 , C07C2603/74
摘要： A tetrakis(ether-substituted formylphenyl) expressed by General Formula (1): wherein R1 represents an alkyl group with 1 to 8 carbon atoms or alkoxyl group with 1 to 8 carbon atoms, or aromatic hydrocarbon group or saturated hydrocarbon group with 1 to 8 carbon atoms having an aromatic hydrocarbon group, n represents 0 or an integer of 1 to 3, R2 represents a divalent monocyclic or fused-ring aromatic hydrocarbon group with 6 to 15 carbon atoms or divalent aliphatic hydrocarbon group with 1 to 8 carbon atoms that may have a monocyclic or fused-ring aromatic hydrocarbon group with 6 to 15 carbon atoms, R3 represents a hydrogen atom or alkyl group with 1 to 6 carbon atoms, A represents a tetravalent carbon atom group or tetravalent saturated hydrocarbon group with 2 or more carbon atoms, where, if A is a tetravalent saturated hydrocarbon group with 2 or more carbon atoms, the two carbon atoms in the A group are bonded with two phenyl groups, respectively.

49. 发明授权

US09090547B2 Method for producing trisphenols and monoester-substituted products thereof, and 4-acylaralkylphenol derivatives 有权
标题翻译：三酚类及其单酯取代物的制造方法以及4-酰基烷基苯酚衍生物
公开(公告)号：US09090547B2
公开(公告)日：2015-07-28
申请号：US13321535
申请日：2010-05-19
申请人： Akihiko Ojiri , Takafumi Tsujigami , Kouichi Tanba
发明人： Akihiko Ojiri , Takafumi Tsujigami , Kouichi Tanba
IPC分类号： C07C39/04 , C07C49/82 , C07C37/055 , C07C37/20 , C07C45/45 , C07C45/67 , C07C49/83 , C07C67/08 , C07C67/14 , C07C67/29 , C07C69/017 , C07C69/157
CPC分类号： C07C49/82 , C07C37/0555 , C07C37/20 , C07C45/455 , C07C45/673 , C07C49/83 , C07C67/08 , C07C67/14 , C07C67/29 , C07C69/017 , C07C69/157 , C07C39/16
摘要： Trisphenols of general formula (1), which are useful as starting materials for polymer, are industrially easily produced by a method using as a starting material 4-aralkylphenol derivatives expressed by general formula (2): wherein X represents a hydrogen atom or leaving group that can be substituted with a hydrogen atom.
摘要翻译：可用作聚合物原料的通式（1）的三酚在工业上容易地通过使用由通式（2）表示的原料4-芳烷基酚衍生物的方法制备：其中X表示氢原子或离去基团其可以被氢原子取代。

50. 发明授权

US08816135B2 Trisphenol compound 有权
标题翻译：三酚化合物
公开(公告)号：US08816135B2
公开(公告)日：2014-08-26
申请号：US13395062
申请日：2010-09-09
申请人： Akira Yoshitomo , Shihoko Nakano
发明人： Akira Yoshitomo , Shihoko Nakano
IPC分类号： C07C39/14 , C07C39/15 , C07C37/20
CPC分类号： C07C39/15 , C07C37/20
摘要： A trisphenol compound is expressed by formula (1), wherein R represents an alkyl group or alkoxyl group with 1 to 8 carbon atoms, phenyl group or hydroxyl group; R1 represents an alkyl group or alkoxyl group with 1 to 8 carbon atoms, or phenyl group; R2 represents an alkyl group or alkoxyl group with 1 to 8 carbon atoms; R3 represents a hydrogen atom or alkyl group with 1 to 8 carbon atoms; a represents 0, 1, 2, or 3; b represents 1 or 2; and c and d represent 0, 1, 2, 3, or 4; where the sum of b and c is 5 or less; R's may be either the same or different when a is 2 or more; R1's may be either the same or different when c is 2 or more; and R2's may be either the same or different when d is 2 or more.
摘要翻译：三酚化合物由式（1）表示，其中R表示烷基或具有1至8个碳原子的烷氧基，苯基或羟基; R1表示碳原子数为1〜8的烷基或烷氧基，或苯基。 R2表示碳原子数为1〜8的烷基或烷氧基， R3表示氢原子或碳原子数为1〜8的烷基; a表示0,1,2或3; b表示1或2; 和c和d代表0，1，2，3或4; 其中b和c之和为5或更小; 当a为2以上时，R可以相同或不同; 当c为2以上时，R1可以相同或不同; 当d为2或更多时，R2的可能相同或不同。

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