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41. 发明授权

US06750278B2 Polyvinyl chloride resins 失效
标题翻译：聚氯乙烯树脂
公开(公告)号：US06750278B2
公开(公告)日：2004-06-15
申请号：US10238172
申请日：2002-09-10
申请人： Abhimanyu O. Patil , Donald N. Schulz , Manika Varma-Nair , David J. Lohse , Christine A. Costello , Richard H. Schlosberg , Michael G. Matturro
发明人： Abhimanyu O. Patil , Donald N. Schulz , Manika Varma-Nair , David J. Lohse , Christine A. Costello , Richard H. Schlosberg , Michael G. Matturro
IPC分类号： C08L2706
CPC分类号： C08L27/06 , C08G67/02 , C08L73/00 , C08L2666/14 , C08L2666/04
摘要： The invention is directed towards a PVC resin composition comprising polyvinyl chloride and a plasticizer selected from the group consisting of: i) a non-linear, paraffin-soluble olefin-CO copolymer; ii) an olefin-CO-X terpolymer derived from non-pure feeds; iii) a non-linear olefin-CO copolymer derived from non-pure feeds; and iv) a non-linear CO-X copolymer; wherein X is selected from the group consisting of alpha-olefin, vinyl acetate, neo vinyl ester and mixtures thereof. The invention also provides a method for a preparing the PVC resin composition as well as a product formed using the PVC resin.
摘要翻译：本发明涉及包含聚氯乙烯和选自以下的增塑剂的PVC树脂组合物：i）非线性，石蜡溶解的烯烃-CO共聚物; ii）衍生自非纯饲料的烯烃-CO-X三元共聚物; iii）衍生自非纯饲料的非线性烯烃-CO共聚物; 和iv）非线性CO-X共聚物; 其中X选自α-烯烃，乙酸乙烯酯，新乙烯基酯及其混合物。本发明还提供了制备PVC树脂组合物的方法以及使用PVC树脂形成的产品。

42. 发明授权

US06627723B2 Adhesive alpha-olefin inter-polymers 有权
标题翻译：粘合剂α-烯烃聚合物
公开(公告)号：US06627723B2
公开(公告)日：2003-09-30
申请号：US09746332
申请日：2000-12-21
申请人： Anthony G. Karandinos , David J. Lohse , Keith A. Nelson , Jean M. Tancrede , Bruce Allan Harrington , Olivier J. F. Georjon , Kenneth Lewtas
发明人： Anthony G. Karandinos , David J. Lohse , Keith A. Nelson , Jean M. Tancrede , Bruce Allan Harrington , Olivier J. F. Georjon , Kenneth Lewtas
IPC分类号： C08F21016
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/14 , C08F2500/17 , C08F210/16 , C08F2500/12 , C08F2500/03
摘要： The invention relates to novel adhesive alpha-olefin inter-polymers which are largely amorphous and have a rheological behavior that makes them suitable for adhesive use, both without and with minimized amounts of tackifying resins. Specifically, the invention poly-alpha olefin inter-polymer may be composed of A) from 60 to 94 mol % of units derived from one alpha mono-olefin having from 3 to 6 carbon atoms and B) from 6 to 40 mol % of units derived from one or more other mono-olefins having from 4 to 10 carbon atoms and at least one carbon atom more than A); and C) optionally from 0 to 10 mol % of units derived from another copolymerizable unsaturated hydrocarbon, different from A) and B); the diad distribution of component A in the polymer as determined by 13C NMR as described herein showing a ratio of experimentally determined diad distribution over the calculated Bernoullian diad distribution of less than 1.07; and the storage modulus G′ of said polymer, determined upon cooling as described herein, intersecting a value of 3.105 Pa at a temperature of less than 85° C. The invention also describes polymerization processes suitable for the manufacture of these adhesive alpha-olefin inter-polymers.
摘要翻译：本发明涉及新型粘合剂α-烯烃聚合物，它们大部分是无定形的并且具有使其适合于粘合剂使用的流变行为，两者都没有和最少量的增粘树脂。具体而言，本发明的聚α烯烃聚合物可以由A）60〜94摩尔％的来自1个具有3〜6个碳原子的α-单烯烃的单元组成，B）6〜40摩尔％的单元衍生自一种或多种其它具有4至10个碳原子和至少一个碳原子的单烯烃，比A）多; 和C）任选地0至10mol％衍生自不同于A）和B）的另一种可共聚不饱和烃的单元; 如本文所述，通过13 C NMR确定的聚合物中组分A的二元分布显示出计算的伯努利二元分布的实验测定的二单元分布的比例小于1.07; 并且在本文所述的冷却下测定的所述聚合物的储能模量G'在小于85℃的温度下与3.10 5 Pa的值相交。本发明还描述了适用于制造这些粘合剂α 烯烃聚合物。

43. 发明授权

US06391998B1 Processing olefin copolymers 有权
标题翻译：加工烯烃共聚物
公开(公告)号：US06391998B1
公开(公告)日：2002-05-21
申请号：US09943540
申请日：2001-08-30
申请人： Cesar A. Garcia-Franco , David J. Lohse , Robert A. Mendelson , Lewis J. Fetters , Scott T. Milner , Nikos Hadjichristidis , David W. Mead
发明人： Cesar A. Garcia-Franco , David J. Lohse , Robert A. Mendelson , Lewis J. Fetters , Scott T. Milner , Nikos Hadjichristidis , David W. Mead
IPC分类号： C08F29900
CPC分类号： C08L23/0815 , C08F110/02 , C08F255/00 , C08F255/02 , C08F257/02 , C08F279/02 , C08F290/042 , C08F290/044 , C08F290/06 , C08F297/08 , C08L23/02 , C08L51/06 , C08L55/00 , C08L55/005 , C08L2666/02 , C08L2666/24 , C08L2666/04 , C08F2500/03 , C08F2500/09 , C08F2500/12
摘要： The invention is directed to essentially saturated hydrocarbon polymer composition comprising essentially saturated hydrocarbon polymers having A) a backbone chain, B) a plurality of essentially hydrocarbyl sidechains connected to A), said sidechains each having a number-average molecular weight of from 2500 Daltons to 125,000 Daltons and a MWD by SEC of 1.0-3.5; and having A) a Newtonian limiting viscosity (&eegr;0) at 190° C. at least 50% greater than that of a linear olefinic polymer of the same chemical composition and weight average molecular weight, preferably at least twice as great as that of said linear polymer, B) a ratio of the rubbery plateau modulus at 190° C. to that of a linear polymer of the same chemical composition less than 0.5, preferably
摘要翻译：本发明涉及基本上饱和的烃聚合物组合物，其包含基本上饱和的烃聚合物，其具有A）主链，B）与A）连接的多个基本上烃基的侧链，所述侧链的数均分子量为2500道尔顿至 125,000道尔顿和SEC的MWD为1.0-3.5; 并且具有A）在190℃下的牛顿极限粘度（eta0）比具有相同化学组成和重均分子量的线性烯烃聚合物的牛顿极限粘度（eta0）至少大50％，优选至少是所述线性聚合物，B）190℃下的橡胶平稳度模量与相同化学组成小于0.5，优选<0.3的线性聚合物的比率，C）牛顿极限粘度（η）与绝对值的比率振荡剪切下的复数粘度值（eta *）在190℃下在100rad / sec下的值至少为5，D）在应变速率1秒-1，190℃下测量的拉伸粘度比，时间= 3秒（即3的应变）与在相同温度和时间为2或更大的线性粘弹性预测的时间。通过阴离子聚合和氢化制备的乙烯 - 丁烯和通过配位聚合制备的乙烯 - 己烯共聚说明了本发明。本发明聚合物表现出改进的加工特性，因为剪切稀化行为与理想聚合物的剪切变稀行为密切相关，并表现出改进的应变增厚。

44. 发明授权

US5578237A Gel-free .alpha.-olefin dispersant additives useful in oleaginous compositions 失效
标题翻译：无油α-烯烃分散剂，适用于含油组合物
公开(公告)号：US5578237A
公开(公告)日：1996-11-26
申请号：US338287
申请日：1994-11-10
申请人： Jacob Emert , Robert D. Lundberg , David J. Lohse
发明人： Jacob Emert , Robert D. Lundberg , David J. Lohse
IPC分类号： C10L1/192 , C08F8/00 , C08F8/32 , C08F290/00 , C08F290/06 , C10L1/14 , C10L1/16 , C10L1/18 , C10L1/195 , C10L1/196 , C10L1/198 , C10L1/20 , C10L1/22 , C10L1/234 , C10L1/236 , C10L1/238 , C10L1/2383 , C10L1/2387 , C10L1/24 , C10L1/26 , C10L1/30 , C10L10/18 , C10M129/95 , C10M133/52 , C10M143/02 , C10M143/06 , C10M145/10 , C10M149/02 , C10M149/06 , C10N20/04 , C10N30/04 , C10N40/25 , C10N70/00 , C10M145/22 , C10M145/20
CPC分类号： C10M149/02 , C08F255/023 , C08F255/04 , C08F8/14 , C08F8/32 , C10L1/143 , C10L1/196 , C10L1/198 , C10L1/236 , C10L1/238 , C10L1/2383 , C10L1/2387 , C10L1/2475 , C10M129/95 , C10M133/52 , C10M143/02 , C10M145/10 , C08F2810/20 , C10L1/1616 , C10L1/1832 , C10L1/1963 , C10L1/1966 , C10L1/1985 , C10L1/201 , C10L1/2364 , C10L1/2366 , C10L1/2368 , C10L1/2468 , C10L1/2641 , C10L1/306 , C10M2207/282 , C10M2207/287 , C10M2207/288 , C10M2207/289 , C10M2207/34 , C10M2215/04 , C10M2215/042 , C10M2215/086 , C10M2215/22 , C10M2215/221 , C10M2215/225 , C10M2215/226 , C10M2215/26 , C10M2215/28 , C10M2215/30 , C10M2217/022 , C10M2217/023 , C10M2217/024 , C10M2217/028 , C10M2217/046 , C10M2217/06 , C10N2240/00 , C10N2240/02 , C10N2240/08 , C10N2240/10 , C10N2240/101 , C10N2240/102 , C10N2240/103 , C10N2240/104 , C10N2240/106 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66 , C10N2270/02
摘要： Gel-free dispersant additives for lubricating and fuel oil compositions comprise at least one adduct of (A) .alpha.-olefin homopolymer or interpolymer of 700 to 10,000 number average molecular weight, free radically grafted with an average of from about 0.5 to about 5 carboxylic acid producing moieties per polymer chain, and (B) at least one non-aromatic nucleophilic post-treating reactant selected from (i) amine compounds containing only a single reactive amino group per molecule, (ii) alcohol compounds containing only a single hydroxy group per molecule, (iii) polyamine compounds containing at least two reactive amino groups per molecule, (iv) polyol compounds containing at least two reactive hydroxy groups per molecule, (v) aminoalcohol compounds containing at least one reactive amino group and at least one reactive hydroxy group per molecule, and (vi) mixtures of (i) to (v); provided that when said post-treating reactant includes one or more of (iii), (iv) or (v), the reaction between (A) and (B) is conducted in the presence of sufficient chain-stopping or end-capping co-reactant (C) to ensure that the grafted and post-reacted product mixture is gel-free.
摘要翻译：用于润滑和燃料油组合物的无凝胶分散剂添加剂包含至少一种（A）α-烯烃均聚物或数均分子量为700至10,000的互聚物的至少一种加合物，其平均具有约0.5至约5个羧酸自由基接枝每个聚合物链产生部分，和（B）至少一种非芳族亲核后处理反应物，其选自（i）每分子仅含有单个反应性氨基的胺化合物，（ii）仅含有单个羟基的醇化合物分子，（iii）每分子含有至少两个反应性氨基的多胺化合物，（iv）每分子含有至少两个反应性羟基的多元醇化合物，（v）含有至少一个反应性氨基的氨基醇化合物和至少一种反应性羟基（vi）（i）至（v）的混合物; 条件是当所述后处理反应物包含（iii），（iv）或（v）中的一种或多种时，（A）和（B）之间的反应在足够的链终止或封端共聚物存在下进行 - 反应物（C），以确保接枝和后反应的产物混合物不凝胶。

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