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41. 发明申请

US20070260082A1 Silicone Composition and Cured Silicone Resin 失效
标题翻译：硅酮组合物和固化硅树脂
公开(公告)号：US20070260082A1
公开(公告)日：2007-11-08
申请号：US11662857
申请日：2005-11-01
申请人： Michael Smith , Bizhong Zhu
发明人： Michael Smith , Bizhong Zhu
IPC分类号： C08K5/54 , C08L83/04
CPC分类号： C08K5/5403 , C08G77/12 , C08G77/20 , C08K5/5425 , C08L83/04 , C08L2205/02 , C08L83/00
摘要： A silicone composition according to the present invention comprises (A) an organopolysiloxane resin having an average of at least two silicon-bonded alkenyl groups per molecule, (B) an organohydrogensilane in an amount sufficient to cure the composition, (C) an effective amount of a reactive diluent comprising (i) an organosiloxane having an average of at least two alkenyl groups per molecule and a viscosity of from 0.001 to 2 Pa·s at 25° C., wherein the viscosity of (C)(i) is not greater than 20% of the viscosity of component (A), and (ii) an organohydrogensiloxane having an average of at least two silicon-bonded hydrogen atoms per molecule and a viscosity of from 0.001 to 2 Pa·s at 25° C., in an amount sufficient to provide from 0.5 to 3 moles of silicon-bonded hydrogen atoms in (C)(ii) to moles of alkenyl groups in (C)(i), and (D) a catalytic amount of a hydrosilylation catalyst; and a cured silicone resin prepared by curing the silicone composition.
摘要翻译：根据本发明的硅氧烷组合物包含（A）每分子平均具有至少两个硅键合的烯基的有机聚硅氧烷树脂，（B）足以固化组合物的量的有机氢硅烷，（C）有效量的反应性稀释剂，其包含（i）每分子平均具有至少两个烯基的有机硅氧烷，并且在25℃下的粘度为0.001至2Pa.s，其中（C）（i）的粘度不是组分（A）的粘度大于20％，和（ii）每分子平均具有至少两个硅键合的氢原子的有机氢硅氧烷，在25℃下的粘度为0.001至2Pa.s，（C）（ⅱ）中足以提供0.5至3摩尔硅键合的氢原子与（C）（ⅰ）中烯基摩尔数的量，和（D）催化量的氢化硅烷化催化剂; 和通过固化硅氧烷组合物制备的固化的硅氧烷树脂。

42. 发明授权

US06596821B1 Hydrosilyation cured silicone resins obtained by fractionation 失效
$Hydrosilyation cured silicone resins obtained by fractionation$
标题翻译：通过分级得到的水解固化的硅氧烷树脂
公开(公告)号：US06596821B1
公开(公告)日：2003-07-22
申请号：US10091678
申请日：2002-03-05
申请人： Dimitris E. Katsoulis , Bizhong Zhu , John R. Keryk , Frederick J. McGarry , Zhongtao Li
发明人： Dimitris E. Katsoulis , Bizhong Zhu , John R. Keryk , Frederick J. McGarry , Zhongtao Li
IPC分类号： C08G7704
CPC分类号： C08G77/04 , C08G77/36 , C08K5/0025
摘要： A process for producing a cured silsesquioxane resin. The process includes fractionating the silsesquioxane resin a plurality of times utilizing an organic solvent in combination with an organic non-solvent. The fractionated resin is then stripped of excess solvent. The stripped resin is then mixed with a cross-linking compound to form a curable composition. The curable composition is cured to form a cured resin having high fracture toughness and strength without the loss of elastic modulus.
摘要翻译：固化倍半硅氧烷树脂的制造方法。该方法包括使用有机溶剂与有机非溶剂组合多次分级倍半硅氧烷树脂。然后将分馏的树脂汽提出过量的溶剂。然后将剥离的树脂与交联化合物混合以形成可固化组合物。可固化组合物固化以形成具有高断裂韧性和强度的固化树脂，而不损失弹性模量。

43. 发明授权

US06310146B1 Silsesquioxane resin with high strength and fracture toughness and method for the preparation thereof 有权
$Silsesquioxane resin with high strength and fracture toughness and method for the preparation thereof$
标题翻译：具有高强度和断裂韧性的倍半硅氧烷树脂及其制备方法
公开(公告)号：US06310146B1
公开(公告)日：2001-10-30
申请号：US09345638
申请日：1999-07-01
申请人： Dimitris Elias Katsoulis , Zhongtao Li , Frederick Jerome McGarry , Bihn Thanh Nguyen , Bizhong Zhu
发明人： Dimitris Elias Katsoulis , Zhongtao Li , Frederick Jerome McGarry , Bihn Thanh Nguyen , Bizhong Zhu
IPC分类号： C08L8305
CPC分类号： C08L83/14 , C08G77/12 , C08G77/20 , C08L83/04 , C09D183/14 , C08L2666/44
摘要： A cured silsesquioxane resin and method for its preparation are disclosed. By using a silyl-terminated hydrocarbon in the hydrosilylation reaction curable composition used to prepare the cured silsesquioxane resin, the cured silsesquioxane resin has improved strength and toughness without significant loss of modulus. A typical silyl-terminated hydrocarbon useful in this invention is silphenylene.
摘要翻译：公开了一种固化的倍半硅氧烷树脂及其制备方法。通过在用于制备固化倍半硅氧烷树脂的氢化硅烷化反应固化性组合物中使用甲硅烷基封端的烃，固化的倍半硅氧烷树脂具有改善的强度和韧性，而没有显着的模量损失。用于本发明的典型甲硅烷基封端的烃是硅亚苯基。

44. 发明授权

US08795560B2 Low thermal distortion silicone composite molds 有权
标题翻译：低热变形硅胶复合模具
公开(公告)号：US08795560B2
公开(公告)日：2014-08-05
申请号：US12294767
申请日：2007-03-09
申请人： Bizhong Zhu , Wei Chen
发明人： Bizhong Zhu , Wei Chen
IPC分类号： B29C47/76 , B29C37/00
CPC分类号： H01L31/0481 , B29C37/0064 , B82Y10/00 , B82Y40/00 , C08G77/12 , C08G77/20 , C08K5/5425 , C08L83/04 , G03F7/0002 , H01L31/022441 , H01L31/048 , Y02E10/50 , C08L83/00
摘要： The present invention provides compositions and methods that may be used to form low thermal distortion molds. The composition may include a curable elastomeric silicone composition formed using a de-volatilized polymer and at least one de-volatilized cross-linker. One embodiment of the method may include forming a pattern on a first side of an elastomer that is impregnated with a fibrous material proximate a second side of the elastomer.
摘要翻译：本发明提供可用于形成低热变形模具的组合物和方法。组合物可以包括使用去挥发的聚合物和至少一种去挥发的交联剂形成的可固化的弹性体硅氧烷组合物。该方法的一个实施方案可以包括在弹性体的第一侧上形成图案，所述弹性体的第一侧被浸渍在靠近弹性体的第二侧的纤维材料。

45. 发明授权

US08092910B2 Reinforced silicone resin film and method of preparing same 失效
标题翻译：增强硅树脂薄膜及其制备方法
公开(公告)号：US08092910B2
公开(公告)日：2012-01-10
申请号：US11794924
申请日：2006-02-01
申请人： Debbie Bailey , Dimitris Elias Katsoulis , Michitaka Suto , Bizhong Zhu
发明人： Debbie Bailey , Dimitris Elias Katsoulis , Michitaka Suto , Bizhong Zhu
IPC分类号： B32B27/28
CPC分类号： C08J5/04 , C08J5/24 , C08J2383/04 , C08J2383/14 , C09D183/04 , C09D183/14 , Y10T428/31598 , C08L83/00
摘要： A method of preparing a reinforced silicone resin film, the method comprising the steps of impregnating a fiber reinforcement in a hydrosilylation-curable silicone composition comprising a silicone resin, and heating the impregnated fiber reinforcement at a temperature sufficient to cure the silicone resin, wherein the reinforced silicone resin film comprises from 10 to 99% (w/w) of the cured silicone resin and the film has a thickness of from 15 to 500 μm; and a reinforced silicone resin film prepared according to the method.
摘要翻译：一种制备增强硅树脂薄膜的方法，该方法包括以下步骤：将纤维增强物浸渍在包含硅树脂的氢化硅烷化可固化的硅氧烷组合物中，并在足以固化硅树脂的温度下加热浸渍的纤维增强体，其中增强的有机硅树脂膜包含10至99％（w / w）的固化的有机硅树脂，并且该膜具有15至500μm的厚度; 和根据该方法制备的增强硅树脂膜。

46. 发明授权

US08084097B2 Silicone resin film, method of preparing same, and nanomaterial-filled silicone composition 失效
标题翻译：硅树脂膜，其制备方法和纳米材料填充的有机硅组合物
公开(公告)号：US08084097B2
公开(公告)日：2011-12-27
申请号：US12223225
申请日：2007-01-11
申请人： Mark Fisher , Bizhong Zhu
发明人： Mark Fisher , Bizhong Zhu
IPC分类号： B05D3/02 , C08L83/04
CPC分类号： C09D183/04 , Y10S977/753 , C08L83/00
摘要： A method of preparing a silicone resin film comprising coating a release liner with a nanomaterial-filled silicone composition comprising (i) a free radical-curable silicone composition comprising a silicone resin and (ii) a carbon nanomaterial, and curing the silicone resin of the coated release liner; a silicone resin film prepared according to the preceding method; and a nanomaterial-filled silicone composition.
摘要翻译：一种制备有机硅树脂膜的方法，包括用纳米材料填充的硅氧烷组合物涂覆剥离衬垫，所述硅氧烷组合物包含（i）包含硅树脂的自由基可固化有机硅组合物和（ii）碳纳米材料，并固化所述硅树脂涂层剥离衬垫; 根据前述方法制备的有机硅树脂膜; 和纳米材料填充的硅氧烷组合物。

47. 发明申请

US20110223421A1 Silicone Composition And A Method For Preparing The Same 有权
标题翻译：硅胶组合物及其制备方法
公开(公告)号：US20110223421A1
公开(公告)日：2011-09-15
申请号：US13129926
申请日：2009-11-18
申请人： Yukinari Harimoto , Bizhong Zhu
发明人： Yukinari Harimoto , Bizhong Zhu
IPC分类号： B32B7/12 , C08L83/04 , C08K3/22 , B32B17/06 , C08K9/06 , B82Y30/00
CPC分类号： C09C1/00 , C01P2006/22 , C01P2006/60 , C08G77/12 , C08G77/20 , C08G77/70 , C08K9/08 , C08L83/04 , C09C1/3081 , C09C1/3684 , C09C1/407 , C09C3/12 , Y10T428/2852 , Y10T428/31612 , C08L2666/54
摘要： A silicone composition comprises (a) a curable silicone resin, (b) an inorganic particle having a polymeric surface coating formed thereon, and (c) a cross-linking compound. The (a) curable silicone resin comprises units having a functional group R1 selected from an aryl group, an alkyl group, an alkenyl group, and hydrogen. The polymeric surface coating comprises an organopolysiloxane. The organopolysiloxane comprises units selected from R23SiO1/2, R22SiO2/2, R2SiO3/2, and combinations thereof. R2 is selected from an aryl group, an alkyl group, an alkenyl group, hydrogen, and combinations thereof, and R1 equals R2. The (c) cross-linking compound is reactive with at least one of (a) and the polymeric surface coating.
摘要翻译：有机硅组合物包含（a）可固化有机硅树脂，（b）其上形成有聚合物表面涂层的无机颗粒，和（c）交联化合物。（a）可固化有机硅树脂包括具有选自芳基，烷基，烯基和氢的官能团R1的单元。聚合物表面涂层包含有机聚硅氧烷。有机聚硅氧烷包括选自R 23 SiO 1/2，R 22 SiO 2/2，R 2 SiO 3/2的单元及其组合。 R2选自芳基，烷基，烯基，氢及其组合，并且R 1等于R 2。（c）交联化合物与（a）和聚合物表面涂层中的至少一种具有反应性。

48. 发明申请

US20110021736A1 Polyborosiloxane and Method of Preparing Same 审中-公开
标题翻译：聚硼硅氧烷及其制备方法
公开(公告)号：US20110021736A1
公开(公告)日：2011-01-27
申请号：US12867896
申请日：2008-03-04
申请人： Bizhong Zhu
发明人： Bizhong Zhu
IPC分类号： C08G79/08
CPC分类号： C08G77/56 , C08G77/20 , C09J183/14 , C08K5/5403 , C08K5/5419 , C08K5/56
摘要： A polyborosiloxane having a low content of boron-bonded hydroxy groups; and a method of preparing the polyborosiloxane.
摘要翻译：具有低硼键羟基含量的聚硼硅氧烷; 和聚硼硅氧烷的制备方法。

49. 发明申请

US20100280172A1 Reinforced Silicone Resin Film and Method of Preparing Same 审中-公开
标题翻译：增强硅树脂薄膜及其制备方法
公开(公告)号：US20100280172A1
公开(公告)日：2010-11-04
申请号：US12301049
申请日：2007-06-13
申请人： Bizhong Zhu
发明人： Bizhong Zhu
IPC分类号： C08L83/00 , B05D3/02
CPC分类号： C09D183/14 , B29B15/10 , B29C70/44 , B29K2083/00 , B29K2083/005 , B29K2105/0845 , B29K2105/128 , B29K2105/24
摘要： A method of preparing a reinforced silicone resin film, the method comprising impregnating a fiber reinforcement in a silicone composition comprising (A) a silicone resin having disilyloxane units and (B) an organic solvent, and curing the silicone resin of the impregnated fiber reinforcement; and a reinforced silicone resin film prepared according to the method.
摘要翻译：一种制备增强有机硅树脂薄膜的方法，该方法包括在硅氧烷组合物中浸渍纤维增强物，所述硅酮组合物包含（A）具有二硅氧烷单元的有机硅树脂和（B）有机溶剂，并固化浸渍纤维增强体的硅树脂; 和根据该方法制备的增强硅树脂膜。

50. 发明申请

US20100273972A1 Method of Preparing a Silicone Resin 有权
标题翻译：硅树脂的制备方法
公开(公告)号：US20100273972A1
公开(公告)日：2010-10-28
申请号：US12374378
申请日：2007-06-13
申请人： Bizhong Zhu
发明人： Bizhong Zhu
IPC分类号： C08G77/14
CPC分类号： C08G77/48 , C08G77/06
摘要： A method of preparing a silicone resin, the method comprising reacting at least one halodisilane and, optionally, at least one halosilane with at least one alcohol in the presence of an organic solvent to produce an alcoholysis product; reacting the alcoholysis product with water to produce a hydrolyzate; and heating the hydrolyzate to produce the resin.
摘要翻译：一种制备有机硅树脂的方法，所述方法包括在有机溶剂存在下使至少一种卤代硅烷和任选的至少一种卤代硅烷与至少一种醇反应以产生醇解产物; 使醇解产物与水反应产生水解产物; 并加热水解产物以制备树脂。

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