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41. 发明授权

US4552563A Composition for the alkaline bleaching of textiles containing peroxyamine 失效
标题翻译：用于含有过氧胺的纺织品的碱性漂白的组合物
公开(公告)号：US4552563A
公开(公告)日：1985-11-12
申请号：US650778
申请日：1984-09-13
申请人： Bernard Dubreux , Jackie Emeraud , Gerard Tatin , Jean-Pierre Schirmann
发明人： Bernard Dubreux , Jackie Emeraud , Gerard Tatin , Jean-Pierre Schirmann
IPC分类号： C11D3/395 , C07C67/00 , C07C407/00 , C07C409/40 , C11D3/39 , D06L3/02 , D06L3/00
CPC分类号： C11D3/3945 , D06L3/025
摘要： A composition for the alkaline bleaching of textiles during washing comprising a washing product and at least one peroxide derivative of the general formula: ##STR1## where R.sub.1, R.sub.2, R.sub.3, and R.sub.4 are hydrogen, a linear alkyl radical containing from 1 to 12 carbon atoms, a cycloalkyl or branched alkyl radical containing from 3 to 12 carbon atoms, or an aromatic hydrocarbon radical having from 6 to 12 carbon atoms; said radicals being unsubstituted or substituted by chlorine, bromine, fluorine, a nitro group, hydroxy group, alkoxy group, ethylenic derivatives, or carboxylic ester and R.sub.1 and R.sub.2 and/or R.sub.3 and R.sub.4, respectively, capable of forming only a single linear or branched radical having from 3 to 12 carbon atoms and the process of alkaline bleaching using the same.
摘要翻译：用于洗涤期间纺织品的碱性漂白的组合物包含洗涤产物和至少一种通式如下的过氧化物衍生物：其中R 1，R 2，R 3和R 4是氢，含有1个至12个碳原子，含有3至12个碳原子的环烷基或支链烷基或具有6至12个碳原子的芳族烃基; 所述自由基是未取代的或被氯，溴，氟，硝基，羟基，烷氧基，烯属衍生物或羧酸酯取代，R 1和R 2和/或R 3和R 4分别仅能形成单个直链或具有3至12个碳原子的支链基和使用其的碱性漂白过程。

42. 发明授权

US4303587A Catalytic epoxidation of olefins 失效
标题翻译：烯烃的催化环氧化
公开(公告)号：US4303587A
公开(公告)日：1981-12-01
申请号：US73440
申请日：1979-09-07
申请人： Jean-Pierre Schirmann , Serge Y. Delavarenne
发明人： Jean-Pierre Schirmann , Serge Y. Delavarenne
IPC分类号： B01J21/00 , B01J31/00 , C07B61/00 , C07D301/12 , C07D303/04
CPC分类号： C07D301/12 , C07D303/04
摘要： The invention disclosed provides a method for the direct epoxidation of olefins in the liquid phase by reacting the olefin with hydrogen peroxide in the presence of a boron containing catalyst while continuously removing water from the reaction mixture.
摘要翻译：所公开的本发明提供了一种通过在含硼催化剂存在下使烯烃与过氧化氢反应而在液相中直接环氧化的方法，同时从反应混合物中连续除去水。

43. 发明授权

US4303586A Catalytic epoxidation of olefins 失效
标题翻译：烯烃的催化环氧化
公开(公告)号：US4303586A
公开(公告)日：1981-12-01
申请号：US38182
申请日：1979-05-11
申请人： Jean-Pierre Schirmann , Serge Y. Delavarenne
发明人： Jean-Pierre Schirmann , Serge Y. Delavarenne
IPC分类号： B01J21/00 , B01J31/00 , C07B61/00 , C07D301/12 , C07D303/04
CPC分类号： C07D301/12 , C07D303/04
摘要： The invention disclosed provides a method for the direct expoxidation of olefins in the liquid phase by reacting the olefin with hydrogen peroxide in the presence of a boron containing catalyst while continuously removing water from the reaction mixture.
摘要翻译：所公开的本发明提供了一种通过在含硼催化剂存在下使烯烃与过氧化氢反应，同时从反应混合物中连续除去水来直接对液相烯烃进行过氧化的方法。

44. 发明授权

US4049712A Method for manufacturing hydrazodicarbonamide 失效
标题翻译：制备肼基二酰胺的方法
公开(公告)号：US4049712A
公开(公告)日：1977-09-20
申请号：US265749
申请日：1972-06-23
申请人： Jean-Pierre Schirmann , Francis Weiss
发明人： Jean-Pierre Schirmann , Francis Weiss
IPC分类号： C07C67/00 , C07C239/00 , C07C281/02 , C07C281/06 , C07C133/02 , C01B21/16
CPC分类号： C07C281/06
摘要： This invention relates to a method for preparing hydrazodicarbonamide ##STR1## which comprises reacting urea, sulfuric acid, water and an azine or a solution containing an azine of the formula ##STR2## wherein R.sub.1 is hydrogen and R.sub.2 or R.sub.1 and R.sub.2 each is a straight or branched alkyl radical or cycloalkyl radical of up to 6 carbon atoms or R.sub.1 and R.sub.2 of both the >C=N-- moieties together form a straight or branched chain alkylene radical of from 3 to 5 carbon atoms and recovering the hydrazodicarbonamide from the reaction medium.
摘要翻译：本发明涉及一种制备肼基二羰酰胺（I）的方法，其包括使尿素，硫酸，水和吖嗪或含有式（Ⅺ）的吖嗪的溶液，其中R 1为氢，R 2或R 1 并且R 2各自是具有至多6个碳原子的直链或支链烷基或环烷基，或者两个> C = N-部分的R 1和R 2一起形成3至5个碳原子的直链或支链亚烷基，并回收来自反应介质的肼基二酰胺。

45. 发明授权

US3978049A Process for the preparation of hydrazine compounds 失效
公开(公告)号：US3978049A
公开(公告)日：1976-08-31
申请号：US433710
申请日：1974-01-16
申请人： Jean-Pierre Schirmann , Pierre Tellier , Henri Mathais , Francis Weiss
发明人： Jean-Pierre Schirmann , Pierre Tellier , Henri Mathais , Francis Weiss
IPC分类号： C07D213/42 , B01J21/00 , B01J23/00 , C07B43/00 , C07B61/00 , C07C20060101 , C07C67/00 , C07C241/00 , C07C251/76 , C07C251/82 , C07C251/84 , C07C251/86 , C07C251/88 , C07D213/53 , C07C109/00
CPC分类号： C07C251/88 , C07C249/16
摘要： This invention relates to a method for preparing an azine of the formula ##EQU1## wherein R.sub.1 and R.sub.2, which may be the same or different, represent a hydrogen atom or a straight alkyl radical of from 1 to 12 carbon atoms, a branched alkyl or cycloalkyl radical of 3 to 12 carbon atoms, or a hydrocarbon radical of from 6 to 12 carbon atoms containing a benzene, naphthalene, or pyridine aromatic ring or R.sub.1 and R.sub.2 together form a straight or branched alkylene radical of 3 to 11 carbon atoms, one of which may be replaced by an oxygen atom, all of the above being unsubstituted or substituted with chlorine, bromine, or fluorine atoms, or ethylene, nitro, hydroxy, alkoxy, carboxylic or percarboxylic acid, amide, nitrile, or carboxylic ester groups, or a mixture of an azine of formula (I) and a hydrazone of the formula ##EQU2## wherein R.sub.1 and R.sub.2 are as defined above and R.sub.3 and R.sub.4, which may be the same or different, represent a straight alkyl radical of from 1 to 12 carbon atoms, a branched alkyl or cycloalkyl radical of 3 to 12 carbon atoms, or a hydrocarbon radical of from 6 to 12 carbon atoms containing a benzene, naphthalene, or pyridine aromatic ring or R.sub.1 and R.sub.2 together form a straight or branched alkylene radical of 3 to 11 carbon atoms, one of which may be replaced by an oxygen atom, all of the above being unsubstituted or substituted by chlorine, bromine, fluorine, or iodine atoms, or hydroxy, ether oxide, carboxylic acid, carboxylic ester, nitrile, nitro, or sulphonic acid or amide groups or one of the two radicals R.sub.3 and R.sub.4 can represent a hydrogen atom, which comprises reacting hydrogen peroxide with ammonia or with a mixture of ammonia and primary or secondary amine of the formula ##EQU3## wherein R.sub.3 and R.sub.4 are as defined above, in the presence of a carbonyl compound of the formula ##EQU4## wherein R.sub.1 and R.sub.2 are as defined above, and a catalyst containing selenium.

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