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41. 发明授权

US5763133A Toner compositions and processes 失效
标题翻译：调色剂组成和工艺
公开(公告)号：US5763133A
公开(公告)日：1998-06-09
申请号：US825451
申请日：1997-03-28
申请人： Beng S. Ong , Walter Mychajlowskij , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
发明人： Beng S. Ong , Walter Mychajlowskij , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
IPC分类号： G03G9/08 , G03G9/087 , G03G9/09 , G03G9/097
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08733
摘要： A process for the preparation of toner comprising (i) blending (a) an aqueous pigment dispersion containing a first ionic surfactant and an optional charge control agent with (b) a latex blend comprised of linear polymer and crosslinked polymer particles, optional nonionic surfactant and a second ionic surfactant with a charge polarity opposite to that of said first ionic surfactant in said pigment dispersion; (ii) heating the resulting mixture at about below the glass transition temperature (Tg) of the linear latex polymer to form toner sized aggregates; and (iii) subsequently heating said aggregate suspension about above the Tg of the linear latex polymer to effect fusion or coalescence of said aggregates.
摘要翻译：一种制备调色剂的方法，包括（i）将（a）含有第一离子型表面活性剂和任选的电荷控制剂的水性颜料分散体与（b）由线性聚合物和交联聚合物颗粒组成的胶乳共混物，任选的非离子表面活性剂和在所述颜料分散体中具有与所述第一离子型表面活性剂相反的电荷极性的第二离子表面活性剂; （ii）将所得混合物加热至低于线性胶乳聚合物的玻璃化转变温度（Tg），以形成调色剂尺寸的聚集体; 和（iii）随后将所述聚集体悬浮液加热至高于线性胶乳聚合物的Tg，以实现所述聚集体的熔融或聚结。

42. 发明授权

US5747215A Toner compositions and processes 失效
标题翻译：调色剂组成和工艺
公开(公告)号：US5747215A
公开(公告)日：1998-05-05
申请号：US841300
申请日：1997-04-29
申请人： Beng S. Ong , Walter Mychajlowskijj , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
发明人： Beng S. Ong , Walter Mychajlowskijj , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
IPC分类号： G03G9/08 , G03G9/087 , G03G9/09 , G03G9/097
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08733
摘要： A process for the preparation of toner comprising (i) blending (a) a colorant dispersion containing a first ionic surfactant and an optional charge control agent with (b) a latex blend comprised of linear polymer and crosslinked polymer particles, optional nonionic surfactant and a second ionic surfactant with a charge polarity opposite to that of said first ionic surfactant in said colorant dispersion; (ii) heating the resulting mixture at about below the glass transition temperature (Tg) of the linear latex polymer to form toner sized aggregates; and (iii) subsequently heating said aggregate suspension about above the Tg of the linear latex polymer to effect fusion or coalescence of said aggregates, and wherein said linear polymer is of an M.sub.w of from about 20,000 to about 40,000.
摘要翻译：一种制备调色剂的方法，包括（i）将（a）含有第一离子型表面活性剂和任选的电荷控制剂的着色剂分散体与（b）由直链聚合物和交联聚合物颗粒组成的胶乳共混物，任选的非离子表面活性剂和第二离子表面活性剂，其电荷极性与所述着色剂分散体中所述第一离子表面活性剂的极性相反; （ii）将所得混合物加热至低于线性胶乳聚合物的玻璃化转变温度（Tg），以形成调色剂尺寸的聚集体; 和（iii）随后将所述聚集体悬浮液加热至高于线性胶乳聚合物的Tg以实现所述聚集体的熔融或聚结，并且其中所述线性聚合物的Mw为约20,000至约40,000。

43. 发明授权

US5698223A Toner process 失效
标题翻译：调色剂过程
公开(公告)号：US5698223A
公开(公告)日：1997-12-16
申请号：US829551
申请日：1997-03-28
申请人： Walter Mychajlowskij , Guerino G. Sacripante , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz
发明人： Walter Mychajlowskij , Guerino G. Sacripante , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/0804 , G03G9/08768
摘要： A process for the preparation of toner comprising (i) solubilizing an imide based resin in water at pH of from about 10 to about 13 and which solubilizing is accomplished in the presence of nonionic surfactants and anionic surfactants; followed by precipitating the resulting dissolved imide resin into colloidal particles with a size diameter of from about 20 nanometers to about 500 nanometers, and which precipitating is accomplished with a high shearing device operating at a speed of from about 500 to about 2,000 revolutions per minute; acidifying the resulting mixture to a pH of from about 2 to about 4; (ii) preparing a pigment dispersion in water, which dispersion is comprised of a pigment, an oppositely charged ionic surfactant and optionally charge control agent; (iii) shearing (i) and (ii), thereby causing a flocculation of the resin, pigment, surfactants, and optional charge control agent; (iv) heating the resulting flocculent mixture of (iii) with stirring at a temperature of from about 25.degree. C. to about 1.degree. C. below the glass transition temperature (Tg) of the imide resin to effect formation of electrostatically bounded toner sized aggregates, and wherein the imide resin has a Tg of from about 45.degree. C. to about 65.degree. C.; (v) heating the resulting aggregate suspension of (iv) in the presence of additional anionic surfactant selected in an amount of from about 0.01 to about 5 weight percent based on the weight percent of the total reaction mixture solids, and which heating is at a temperature of from about 10.degree. C. to about 55.degree. C. above the Tg of the imide resin; and optionally cooling, and optionally (vi) separating said toner by washing, and thereafter drying said toner.
摘要翻译：一种制备调色剂的方法，包括（i）将酰亚胺基树脂溶解在约10至约13的pH下，并且在非离子表面活性剂和阴离子表面活性剂存在下进行增溶; 然后将所得溶解的酰亚胺树脂沉淀成尺寸直径为约20纳米至约500纳米的胶体颗粒，并且以约500至约2000转/分钟的速度运行的高剪切装置完成沉淀; 将所得混合物酸化至约2至约4的pH; （ii）在水中制备颜料分散体，该分散体由颜料，相反电荷的离子表面活性剂和任选的电荷控制剂组成; （iii）剪切（i）和（ii），从而引起树脂，颜料，表面活性剂和任选的电荷控制剂的絮凝; （iv）在低于酰亚胺树脂的玻璃化转变温度（Tg）的约25℃至约1℃的温度下搅拌加热得到的（ⅲ）絮状混合物，以形成静电有界调色剂尺寸聚集体，并且其中所述酰亚胺树脂的Tg为约45℃至约65℃。（v）在所选择的另外的阴离子表面活性剂存在下加热得到的（iv）聚集体悬浮液，其量为总反应混合物固体的重量百分比为约0.01至约5重量％，加热为温度高于酰亚胺树脂的Tg约10℃至约55℃; 并任选地冷却，并且任选地（vi）通过洗涤分离所述调色剂，然后干燥所述调色剂。

44. 发明授权

US5683848A Acrylonitrile-modified toner composition and processes 失效
标题翻译：丙烯腈改性调色剂组合物和方法
公开(公告)号：US5683848A
公开(公告)日：1997-11-04
申请号：US720736
申请日：1996-10-02
申请人： Beng S. Ong , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , Walter Mychajlowskij , David J. Sanders , T. Hwee Ng
发明人： Beng S. Ong , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , Walter Mychajlowskij , David J. Sanders , T. Hwee Ng
IPC分类号： G03G9/08 , G03G9/087 , G03G9/097
CPC分类号： G03G9/08795 , G03G9/0806 , G03G9/08711 , G03G9/08731 , G03G9/09725
摘要： A toner comprised of pigment, and an addition polymer resin generated from about 55 to about 80 weight percent of styrene, from about 1 to about 25 weight percent of acrylate, from about 1 to about 20 weight percent of acrylonitrile, and from about 0.5 to about 5 weight percent of acrylic acid.
摘要翻译：由颜料组成的调色剂和由约55至约80重量％的苯乙烯，约1至约25重量％的丙烯酸酯，约1至约20重量％的丙烯腈和约0.5至约20重量％的丙烯腈产生的加成聚合物树脂约5重量％的丙烯酸。

45. 发明授权

US06673500B1 Document security processes 失效
标题翻译：文档安全流程
公开(公告)号：US06673500B1
公开(公告)日：2004-01-06
申请号：US10225214
申请日：2002-08-20
申请人： Raj D. Patel , Fatima M. Mayer , Michael A. Hopper , Kurt I. Halfyard
发明人： Raj D. Patel , Fatima M. Mayer , Michael A. Hopper , Kurt I. Halfyard
IPC分类号： G03G908
CPC分类号： G03G9/0926 , B41M3/14 , B41M3/144 , G03G9/0821 , G03G9/08795 , G03G9/08797 , G03G9/0902 , G03G9/0908 , G03G9/0916 , G03G9/0924 , G03G9/09708
摘要： A process comprising applying a toner security mark on a document generated by xerographic means, and which mark possesses white glossy characteristics, and wherein said toner is comprised of a waterborne polymer resin and a colorant, and optionally a second security mark generated by a toner comprised of a waterborne polymer resin and a UV fluorescent component.
摘要翻译：一种方法，包括在由静电印刷装置产生的文件上施加调色剂安全标记，以及哪个标记具有白色光泽特性，并且其中所述调色剂由水性聚合物树脂和着色剂组成，并且可选地由包含的调色剂产生的第二安全标记的水性聚合物树脂和UV荧光成分。

46. 发明授权

US06627373B1 Toner processes 失效
标题翻译：墨粉处理
公开(公告)号：US06627373B1
公开(公告)日：2003-09-30
申请号：US10106514
申请日：2002-03-25
申请人： Raj D. Patel , Michael A. Hopper
发明人： Raj D. Patel , Michael A. Hopper
IPC分类号： G03G9083
CPC分类号： G03G9/0804 , G03G9/0821 , G03G9/0833 , G03G9/08782 , G03G9/0904
摘要： An emulsion aggregation process for the preparation of a magnetite toner, and where the magnetite can function as a negatively charged coagulant to facilitate aggregation of a basic cationic latex, a cationic carbon black dispersion and a cationic wax dispersion.
摘要翻译：用于制备磁铁矿调色剂的乳液聚集方法，其中磁铁矿可以充当带负电荷的凝结剂以促进碱性阳离子胶乳，阳离子炭黑分散体和阳离子蜡分散体的聚集。

47. 发明授权

US06617092B1 Toner processes 失效
标题翻译：墨粉处理
公开(公告)号：US06617092B1
公开(公告)日：2003-09-09
申请号：US10106519
申请日：2002-03-25
申请人： Raj D. Patel , Michael A. Hopper
发明人： Raj D. Patel , Michael A. Hopper
IPC分类号： G03G9083
CPC分类号： G03G9/08795 , G03G9/0804 , G03G9/0833 , G03G9/08782 , G03G9/08797 , G03G9/0904
摘要： An emulsion aggregation process for the preparation of a magnetite toner, and where the magnetite can function as a coagulant.
摘要翻译：用于制备磁铁矿调色剂的乳液聚集方法，其中磁铁矿可用作凝结剂。

48. 发明授权

US06268102B1 Toner coagulant processes 有权
标题翻译：调色剂凝结剂工艺
公开(公告)号：US06268102B1
公开(公告)日：2001-07-31
申请号：US09551465
申请日：2000-04-17
申请人： Michael A. Hopper , Raj D. Patel , Tanya J. Martin
发明人： Michael A. Hopper , Raj D. Patel , Tanya J. Martin
IPC分类号： G03G908
CPC分类号： G03G9/0804 , G03G9/09708 , G03G9/09775
摘要： A process for the preparation of toner comprising mixing a colorant, a latex, optionally a wax and a polyaluminum sulfosilicate.
摘要翻译：一种制备调色剂的方法，包括将着色剂，胶乳，任选的蜡和聚硅磺酸硅铝混合。

49. 发明授权

US06984480B2 Toner processes 失效
标题翻译：墨粉处理
公开(公告)号：US06984480B2
公开(公告)日：2006-01-10
申请号：US10603449
申请日：2003-06-25
申请人： Daryl Vanbesien , Michael A. Hopper , Raj D. Patel
发明人： Daryl Vanbesien , Michael A. Hopper , Raj D. Patel
IPC分类号： G03G9/08
CPC分类号： G03G9/0804 , G03G9/09725
摘要： A process comprising heating a mixture of colorant and latex in the presence of a coagulant and a silicate salt, and wherein said heating comprises a first heating equal to or below about the glass transition temperature of a polymer contained in said latex, and a second heating equal to or about the glass transition temperature of a polymer contained in said latex; wherein said first heating enables the formation of aggregates and said second heating enables the fusion of said colorant and said polymer; and optionally wherein said silicate is contained in an alkali metal hydroxide.
摘要翻译：一种方法，包括在凝结剂和硅酸盐存在下加热着色剂和胶乳的混合物，并且其中所述加热包括等于或低于所述胶乳中包含的聚合物的玻璃化转变温度的第一加热，和第二加热等于或约为所述胶乳中包含的聚合物的玻璃化转变温度; 其中所述第一加热使得能够形成聚集体，并且所述第二加热使得所述着色剂和所述聚合物融合; 并且任选地，其中所述硅酸盐包含在碱金属氢氧化物中。

50. 发明授权

US06210853B1 Toner aggregation processes 有权
标题翻译：调色剂聚合过程
公开(公告)号：US06210853B1
公开(公告)日：2001-04-03
申请号：US09657340
申请日：2000-09-07
申请人： Raj D. Patel , Michael A. Hopper , Emily L. Moore , Guerino G. Sacripante
发明人： Raj D. Patel , Michael A. Hopper , Emily L. Moore , Guerino G. Sacripante
IPC分类号： G03G9087
CPC分类号： G03G9/08708 , G03G9/0806 , G03G9/0819 , G03G9/08711 , G03G9/08755
摘要： A process for the preparation of toner including (i) gerating by emulsion polymerization in the presence of an initiator a first resin latex emulsion; (ii) generating by polycondensation a second resin latex optionally in the presence of a catalyst; (iib) dispersing the resin of (ii) in water; (iii) mixing (iib) with a colorant thereby providing a colorant dispersion; (iiib) mixing the resin latex emulsion of (i) with the resin/colorant mixture of (iii) to provide a blend of a resin and colorant; (iv) adding an aqueous inorganic cationic coagulant solution of a polymeric metal salt and optionally an organic cationic coagulant to the resin/colorant blend of (iiib); (v) heating at a temperature of from about 5 to about 10 degrees Centigrade below the resin Tg of (i), to thereby form aggregate particles and which particles are optionally at a pH of from about 2 to about 3.5; (vi) adjusting the pH of (v) to about 6.5 to about 9 by the addition of a base; (vii) heating the aggregate particles of (v) at a temperature of from about 5 to about 50 degrees Centigrade above the Tg of the resin of (i), followed by a reduction of the pH to from about 2.5 to about 5 by the addition of an acid resulting in coalesced toner; (viii) optionally isolating the toner.
摘要翻译：一种制备调色剂的方法，包括（i）在引发剂存在下通过乳液聚合第一树脂胶乳乳液; （ii）任选地在催化剂存在下通过缩聚产生第二树脂胶乳; （iib）将（ii）的树脂分散在水中; （iii）将混合（iib）与着色剂混合，从而提供着色剂分散体; （iiib）将（i）的树脂胶乳乳液与（iii）的树脂/着色剂混合物混合以提供树脂和着色剂的共混物; （iv）将聚合金属盐和任选的有机阳离子凝结剂的无机阳离子凝结剂水溶液加入到（iiib）的树脂/着色剂混合物中; （v）在（i）的树脂Tg以下约5至约10摄氏度的温度下加热，从而形成聚集体颗粒，并且哪些颗粒任选处于约2至约3.5的pH值; （vi）通过添加碱将（v）的pH调节至约6.5至约9; （vii）在（i）的树脂的Tg以上约5至约50摄氏度的温度下加热（ⅴ）的聚集体颗粒，随后将pH降低至约2.5至约5 加入导致聚结的调色剂的酸; （viii）任选地分离调色剂。

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