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41. 发明授权

US06210606B1 Polycrystalline conducting polymers and precursors thereof having adjustable morphology and properties 有权
标题翻译：具有可调节形态和性质的多晶导电聚合物及其前体
公开(公告)号：US06210606B1
公开(公告)日：2001-04-03
申请号：US09268527
申请日：1999-03-12
申请人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
发明人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
IPC分类号： H01B112
CPC分类号： C08G61/12 , H01B1/128 , Y10T428/249958
摘要： Polycrystalline materials containing crystallites of precursors to electrically conductive polymers and electrically conductive polymers are described which have an adjustable high degree of crystallinity. The intersticial regions between the crystallites contains amorphous material containing precursors to electrically conductive polymers and/or electrically conductive polymers. The degree of crystallinity is achieved by preparing the materials under conditions which provide a high degree of mobility to the polymer molecules permitting them to associate with one another to form a crystalline state. This is preferable achieved by including additives, such as plasticizers and diluents, to the solution from which the polycrystalline material is formed. The morphology of the polycrystalline material is adjustable to modify the properties of the material such as the degree of crystallinity, crystal grain size, glass transition temperature, thermal coefficient of expansion and degree of electrical conductivity. High levels of electrical conductivity are achieved in the electrically conductive polycrystalline materials without stretch orienting the material. The enhanced electrical conductivity is isotropic as compared to a stretch oriented film which has isotropic electrical conductivity.
摘要翻译：描述了具有可调高结晶度的导电聚合物和导电聚合物的前体微晶的多晶材料。微晶之间的区域包含含有导电聚合物和/或导电聚合物的前体的无定形材料。通过在允许它们彼此结合以形成结晶状态的聚合物分子提供高度迁移率的条件下制备材料来实现结晶度。优选通过将诸如增塑剂和稀释剂的添加剂添加到形成多晶材料的溶液中来实现。可以调节多晶材料的形态，以改变材料的性质，例如结晶度，晶粒尺寸，玻璃化转变温度，热膨胀系数和电导率。在导电多晶材料中实现高水平的导电性而不使材料拉伸取向。与具有各向同性电导率的拉伸取向膜相比，增强的导电性是各向同性的。

42. 发明授权

US06193909B1 Cross-linked electrically conductive polymers, precursors thereof 失效
标题翻译：交联导电聚合物及其前体
公开(公告)号：US06193909B1
公开(公告)日：2001-02-27
申请号：US08595853
申请日：1996-02-02
申请人： Marie Angelopoulos , Jeffrey D. Gelorme , Yun Hsin Liao , Jane M. Shaw
发明人： Marie Angelopoulos , Jeffrey D. Gelorme , Yun Hsin Liao , Jane M. Shaw
IPC分类号： H01B112
CPC分类号： C08G73/1071 , H01B1/128
摘要： Cross-linked electrically conductive polymers, in particular electrically conductive, polyaniline are described. Dopants and substituents having pendant cross-linkable functionality are used which form a cross-linked conducting polymer network. The cross-linking functionality can be hydrogen-bonding as well as chemically polymerizable or cross-linkable. A conjugated path between chains can also be incorporated. The resulting cross-linked conducting polymers have enhanced thermal and environmental stability. The dopant cannot readily be washed out with solvents or diffuse out upon exposure to heat. In addition, the cross-linked polymers have enhanced electrical conductivity.
摘要翻译：描述了交联的导电聚合物，特别是导电的聚苯胺。使用具有侧链可交联官能团的掺杂剂和取代基，其形成交联的导电聚合物网络。交联官能团可以是氢键合以及化学上可聚合的或可交联的。还可以并入链之间的共轭路径。所得的交联导电聚合物具有增强的热和环境稳定性。掺杂剂不容易用溶剂洗涤或在暴露于热量时扩散出来。此外，交联聚合物具有增强的导电性。

43. 发明授权

US06180292B2 Structure and manufacture of X-ray mask pellicle with washer-shaped member 失效
标题翻译：具有垫圈构件的X射线掩模防护薄膜的结构和制造
公开(公告)号：US06180292B2
公开(公告)日：2001-01-30
申请号：US09335536
申请日：1999-06-18
申请人： Raul Edmundo Acosta , Marie Angelopoulos , Steven Allen Cordes
发明人： Raul Edmundo Acosta , Marie Angelopoulos , Steven Allen Cordes
IPC分类号： G03F900
CPC分类号： G03F1/22 , G03F1/62 , G03F1/64 , Y10S430/167
摘要： A precise thickness bulk etchable wafer material, that is responsive to protection with an oxide that inhibits insertion of an etch responsiveness altering material, is assembled with a membrane material that is susceptible to deposition processes. A bulk etch then removes most of the wafer. The arrangement permits the strength and rigidity of the bulk spacer to serve to permit the finely controllable deposition processes for ultra thin and wider ranges of membrane materials, the selective protection for spacer shaping and finally, the removal by the low stress process of etching, of the unused bulk spacer material. An oxide layer is patterned on a bulk spacer material wafer that has a thickness of the gap between an X-ray mask and the to be patterned oxide. The oxide on the bulk spacer material prevents conversion, through the exposed surface of the bulk spacer material wafer, of a portion of the wafer that is to serve as the spacer to a different etch responsiveness from that of the bulk spacer material. The exposed bulk spacer material wafer is converted to a depth that will serve as the spacer and to protect the edges. The oxide is then removed. The membrane is deposited over the full surface of the bulk spacer material. The bulk wafer is removed down to the converted portion using the imparted different etch responsivness.
摘要翻译：使用易于沉积工艺的膜材料组装精确厚度的可块状可蚀刻晶片材料，该晶片材料响应于防止蚀刻反应性改变材料插入的氧化物的保护。体蚀刻然后去除大部分晶片。该布置允许散装隔板的强度和刚度用于允许对薄膜材料的超薄和更宽范围的精细可控的沉积工艺，用于间隔件成形的选择性保护以及最终通过蚀刻的低应力过程的去除未使用的散装隔板材料。将氧化物层图案化在具有X射线掩模和待图案化氧化物之间的间隙厚度的块状间隔物材料晶片上。块状隔离物材料上的氧化物防止了通过体隔片材料晶片的暴露表面将用作间隔物的晶片的一部分与块状间隔物材料的不同的蚀刻响应性的转换。将暴露的块状间隔材料晶片转换成将用作间隔物并保护边缘的深度。然后除去氧化物。膜沉积在整块隔板材料的整个表面上。使用赋予的不同蚀刻响应将体晶片除去到转化部分。

44. 发明授权

US6132644A Energy sensitive electrically conductive admixtures 失效
标题翻译：能量敏感的导电外加剂
公开(公告)号：US6132644A
公开(公告)日：2000-10-17
申请号：US086238
申请日：1998-05-28
申请人： Marie Angelopoulos , Edward D. Babich , Inna V. Babich , Kuang-Jung Chen , Wayne Martin Moreau , David E. Seeger
发明人： Marie Angelopoulos , Edward D. Babich , Inna V. Babich , Kuang-Jung Chen , Wayne Martin Moreau , David E. Seeger
IPC分类号： H01B1/12 , H01L23/532 , H01B1/20
CPC分类号： H01B1/12 , H01L23/5328 , H01L2924/0002
摘要： The present invention is an admixture of an electrically conductive material and an energy sensitive material resulting in a conductive energy sensitive composition. The structures are useful for lithography in microelectronic fabrication to avoid the effects of charging on resists from electron beams. The compositions are also useful in applications of scanning electron metrology and static dissipation.
摘要翻译：本发明是导电材料和能量敏感材料的混合物，导致导电能量敏感组合物。该结构可用于微电子制造中的光刻，以避免对来自电子束的抗蚀剂充电的影响。该组合物也可用于扫描电子测量和静电消散的应用中。

45. 发明授权

US6087472A Methods of fabrication of deaggregated electrically conductive polymers and precursors thereof 失效
标题翻译：解聚集的导电聚合物及其前体的制备方法
公开(公告)号：US6087472A
公开(公告)日：2000-07-11
申请号：US370128
申请日：1995-01-09
申请人： Marie Angelopoulos , Bruce K. Furman
发明人： Marie Angelopoulos , Bruce K. Furman
IPC分类号： C08K5/00 , C08J3/20 , C08K5/09 , C08L49/00 , C08L65/00 , C08L65/02 , C08L79/00 , C08L81/02 , C08L101/12 , H01B1/12 , C08J3/00 , C08G73/00 , H01B1/06
CPC分类号： H01B1/128 , C08G2261/312
摘要： Deaggregated substituted and unsubstitued polyparaphenylenes, polyparaphenylevevinyles, polyanilines, polyazines, polythiophenes, poly-p-phenylene sulfides, polyfuranes, polypyrroles, polysclenophene, polyacetylenes formed from soluble precursors and combinations thereof and copolymers thereof and methods of fabrication are described. The deaggregated polymer molecules when subsequently doped show higher electrical conductivity. Agents such as lithium chloride, m-cresol and nonylphenol are used to deaggregate the polymer molecules. The deaggregating agents can be added prior to or during doping the molecules.
摘要翻译：描述了聚集的取代和未取代的聚对苯二酚，聚对苯乙烯基乙烯基，聚苯胺，聚嗪，聚噻吩，聚对苯硫醚，聚呋喃，聚吡咯，聚烯烃，由可溶性前体及其组合形成的聚乙炔及其共聚物及其制备方法。随后掺杂时的解聚聚合物分子显示更高的导电性。诸如氯化锂，间甲酚和壬基苯酚的试剂用于解聚聚合物分子。解聚剂可以在掺杂分子之前或期间加入。

46. 发明授权

US6057902A Pixels for wide viewing angle liquid crystal display 有权
标题翻译：广视角液晶显示器的像素
公开(公告)号：US6057902A
公开(公告)日：2000-05-02
申请号：US129736
申请日：1998-08-05
申请人： Marie Angelopoulos , David Andrew Lewis , Shui-Chih Alan Lien
发明人： Marie Angelopoulos , David Andrew Lewis , Shui-Chih Alan Lien
IPC分类号： G02F1/1337
CPC分类号： G02F1/133753 , G02F1/133788 , G02F2001/133761
摘要： A structure for providing a wide viewing angle for a liquid crystal display or similar comprising the formation of more than one region within a pixel (for each color) which provides more than one pretilt angle is provided by controlling chemistry of a second layer placed in predetermined locations within a single pixel.
摘要翻译：提供用于液晶显示器或类似物的宽视角的结构，其通过控制设置在预定角度的第二层的化学性质来提供，所述结构包括在提供多于一个预倾角的像素内（用于每种颜色）形成多于一个区域单个像素内的位置。

47. 发明授权

US5990249A Methods of fabrication of deaggregated electrically conductive polymers and precursors thereof 失效
标题翻译：解聚集的导电聚合物及其前体的制备方法
公开(公告)号：US5990249A
公开(公告)日：1999-11-23
申请号：US919740
申请日：1997-08-28
申请人： Marie Angelopoulos , Bruce K. Furman
发明人： Marie Angelopoulos , Bruce K. Furman
IPC分类号： C08F283/00 , C08G61/12
CPC分类号： C08F283/00 , C08G61/12
摘要： Deaggregated substituted and unsubstituted polyparaphenylenes, polyparaphenylevevinyles, polyanilines, polyazines, polythiophenes, poly-p-phenylene sulfides, polyfuranes, polypyrroles, polyselenophene, polyacetylenes formed from soluble precursors and combinations thereof and copolymers thereof and methods of fabrication are described. The deaggregated polymer molecules when subsequently doped show higher electrical conductivity. Agents such as lithium chloride, m-cresol and nonylphenol are used to deaggregate the polymer molecules. The deaggregating agents can be added prior to or during doping the molecules.
摘要翻译：描述了聚集的取代和未取代的聚对苯二酚，聚对苯乙烯基乙烯基，聚苯胺，聚嗪，聚噻吩，聚对苯硫醚，聚呋喃，聚吡咯，聚硒酚，由可溶性前体及其组合形成的聚乙炔及其共聚物及其制备方法。随后掺杂时的解聚聚合物分子显示更高的导电性。诸如氯化锂，间甲酚和壬基苯酚的试剂用于解聚聚合物分子。解聚剂可以在掺杂分子之前或期间加入。

48. 发明授权

US5922466A Composite comprising a metal substrate and a corrosion protecting layer 失效
标题翻译：复合材料包括金属基底和腐蚀保护层
公开(公告)号：US5922466A
公开(公告)日：1999-07-13
申请号：US928468
申请日：1997-09-12
申请人： Marie Angelopoulos , Vlasta A. Brusic , Teresita Ordonez Graham , Sampath Purushothaman , Ravi F. Saraf , Jane Margaret Shaw , Judith Marie Roldan , Alfred Viehbeck
发明人： Marie Angelopoulos , Vlasta A. Brusic , Teresita Ordonez Graham , Sampath Purushothaman , Ravi F. Saraf , Jane Margaret Shaw , Judith Marie Roldan , Alfred Viehbeck
IPC分类号： C08G61/12 , C08L33/00 , C08L65/00 , C09D5/08 , C09D5/24 , C09J9/02 , H01B1/12 , H01B1/22 , H01B1/24 , H05K3/32 , H05K9/00 , B32B15/08
CPC分类号： H05K9/0083 , C08G61/12 , C08L65/00 , C09D5/08 , C09D5/24 , C09J9/02 , H01B1/125 , H01B1/127 , H01B1/128 , H01B1/22 , H01B1/24 , H05K3/321 , H05K9/0079 , H05K9/0088 , C08L33/00 , H05K2201/0329 , Y10S428/901 , Y10T428/24917 , Y10T428/25 , Y10T428/31529 , Y10T428/31533 , Y10T428/31605 , Y10T428/31663 , Y10T428/31678 , Y10T428/31681 , Y10T428/31692 , Y10T428/31721 , Y10T428/31725 , Y10T428/31855
摘要： A composite comprising a metal substrate and as a corrosion protecting layer on at least one major surface of said substrate, a composition comprising a thermoset or thermoplastic polymeric matrix, and a conductive filler component, where said filler component comprises electrically conductive particles.
摘要翻译：一种复合材料，其包含金属基材和作为所述基材的至少一个主表面上的腐蚀保护层，包含热固性或热塑性聚合物基质的组合物和导电填料组分，其中所述填料组分包含导电颗粒。

49. 发明授权

US5916486A Method for providing discharge protection or shielding 失效
标题翻译：提供放电保护或屏蔽的方法
公开(公告)号：US5916486A
公开(公告)日：1999-06-29
申请号：US928496
申请日：1997-09-12
申请人： Marie Angelopoulos , Vlasta A. Brusic , Teresita Ordonez Graham , Sampath Purushothaman , Ravi F. Saraf , Jane Margaret Shaw , Judith Marie Roldan , Alfred Viehbeck
发明人： Marie Angelopoulos , Vlasta A. Brusic , Teresita Ordonez Graham , Sampath Purushothaman , Ravi F. Saraf , Jane Margaret Shaw , Judith Marie Roldan , Alfred Viehbeck
IPC分类号： C08G61/12 , C08L33/00 , C08L65/00 , C09D5/08 , C09D5/24 , C09J9/02 , H01B1/12 , H01B1/22 , H01B1/24 , H05K3/32 , H05K9/00 , B05D5/12 , B29D9/00
CPC分类号： H05K9/0083 , C08G61/12 , C08L65/00 , C09D5/08 , C09D5/24 , C09J9/02 , H01B1/125 , H01B1/127 , H01B1/128 , H01B1/22 , H01B1/24 , H05K3/321 , H05K9/0079 , H05K9/0088 , C08L33/00 , H05K2201/0329 , Y10S428/901 , Y10T428/24917 , Y10T428/25 , Y10T428/31529 , Y10T428/31533 , Y10T428/31605 , Y10T428/31663 , Y10T428/31678 , Y10T428/31681 , Y10T428/31692 , Y10T428/31721 , Y10T428/31725 , Y10T428/31855
摘要： Electrostatic discharge protection and electromagnetic interference shielding is provided by applying to a dielectric substrate a composition comprising a polymeric matrix and a conductive filler component. The conductive filler component comprises electrically conductive metal particles and at least one electrically conducting polymer.
摘要翻译：通过向电介质基片施加包含聚合物基质和导电填料组分的组合物来提供静电放电保护和电磁干扰屏蔽。导电填料组分包括导电金属颗粒和至少一种导电聚合物。

50. 发明授权

US5700398A Composition containing a polymer and conductive filler and use thereof 失效
标题翻译：含有聚合物和导电填料的组合物及其用途
公开(公告)号：US5700398A
公开(公告)日：1997-12-23
申请号：US356026
申请日：1994-12-14
申请人： Marie Angelopoulos , Vlasta A. Brusic , Teresita Ordonez Graham , Sampath Purushothaman , Ravi F. Saraf , Jane Margaret Shaw , Judith Marie Roldan , Alfred Viehbeck
发明人： Marie Angelopoulos , Vlasta A. Brusic , Teresita Ordonez Graham , Sampath Purushothaman , Ravi F. Saraf , Jane Margaret Shaw , Judith Marie Roldan , Alfred Viehbeck
IPC分类号： C08G61/12 , C08L33/00 , C08L65/00 , C09D5/08 , C09D5/24 , C09J9/02 , H01B1/12 , H01B1/22 , H01B1/24 , H05K3/32 , H05K9/00 , H01B1/06
CPC分类号： H05K9/0083 , C08G61/12 , C08L65/00 , C09D5/08 , C09D5/24 , C09J9/02 , H01B1/125 , H01B1/127 , H01B1/128 , H01B1/22 , H01B1/24 , H05K3/321 , H05K9/0079 , H05K9/0088 , C08L33/00 , H05K2201/0329 , Y10S428/901 , Y10T428/24917 , Y10T428/25 , Y10T428/31529 , Y10T428/31533 , Y10T428/31605 , Y10T428/31663 , Y10T428/31678 , Y10T428/31681 , Y10T428/31692 , Y10T428/31721 , Y10T428/31725 , Y10T428/31855
摘要： A composition containing a polymeric matrix and a conductive filler component is provided. The conductive filler component comprises conductive particles and a polymer selected from the group consisting of substituted and unsubstituted polyanilines, substituted and unsubstituted polyparaphenylenevinylenes, substituted and unsubstituted polythiophenes, substituted and unsubstituted polyazines, substituted and unsubstituted polyparaphenylenes, substituted and unsubstituted polyfuranes, substituted and unsubstituted polypyrroles, substituted and unsubstituted polyselenophene, substituted and unsubstituted poly-p-phenylene sulfides and substiututed and unsubstituted polyacetylenes, and mixtures thereof, and copolymers thereof. Compositions of the present invention are useful as corrosion protecting layers for metal substrates, for electrostatic discharge protection, electromagnetic interference shielding, and as adhesives for interconnect technology as alternatives to solder interconnections. In addition, films of polyanilines are useful as corrosion protecting layers with or without the conductive metal particles.
摘要翻译：提供含有聚合物基质和导电填料组分的组合物。导电填料组分包括导电颗粒和选自取代和未取代的聚苯胺，取代和未取代的聚对亚苯基亚乙烯基，取代和未取代的聚噻吩，取代和未取代的聚吡嗪，取代和未取代的聚对苯二甲酸，取代和未取代的聚呋喃，取代和未取代的聚吡咯取代和未取代的聚硒吩，取代和未取代的聚对苯硫醚和取代和未取代的聚乙炔，及其混合物，及其共聚物。本发明的组合物可用作金属基材的防腐层，用于静电放电保护，电磁干扰屏蔽，以及作为焊接互连替代物的互连技术的粘合剂。此外，聚苯胺的膜可用作具有或不具有导电金属颗粒的防腐蚀层。

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