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    • 50. 发明授权
    • Method for forming metal nitride film
    • 形成金属氮化物膜的方法
    • US06335277B2
    • 2002-01-01
    • US09318807
    • 1999-05-26
    • Koichi Ohto
    • Koichi Ohto
    • H01L2144
    • H01L21/76864H01L21/28556H01L21/76843H01L21/76856
    • A method for forming a titanium nitride film of an excellent quality on a semiconductor substrate at a low temperature is achieved. With a heated semiconductor substrate on a susceptor held at a temperature of about 500° C., titanium tetrachloride and ammonia are introduced into a reactor to carry out the deposition of the titanium nitride film. After the deposition is completed, the semiconductor substrate within the reactor is continuously held at a temperature of 500° C. After a low pressure mercury lamp is turned on, while the inner part of the reactor is irradiated with ultraviolet rays with a wavelength of 170-280 nm emitted from the lamp, an ammonia gas is introduced, with the flow rate adjusted to about 1000 sccm, into the reactor held at a pressure of about 10 Torr to carry out annealing in an ammonia atmosphere for about 60 seconds.
    • 实现了在低温下在半导体基板上形成质量优异的氮化钛膜的方法。 在保持在约500℃的温度下的基座上加热半导体衬底,将四氯化钛和氨引入反应器中以进行氮化钛膜的沉积。 沉积完成后,反应器内的半导体衬底被连续地保持在500℃的温度。在低压汞灯开启之后,反应器的内部用紫外线照射波长为170 -280nm,将流量调节至约1000sccm的氨气引入保持在约10托的压力下的反应器中,以在氨气氛中进行退火约60秒。