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41. 发明授权

US5342961A Process for the production of low-viscosity imidazolinium surfactants by quaternization of 1-hydroxyethyl-2-alkyl imidazolines 失效
标题翻译：通过1-羟乙基-2-烷基咪唑的季铵化生产低粘度咪唑啉表面活性剂的方法
公开(公告)号：US5342961A
公开(公告)日：1994-08-30
申请号：US70411
申请日：1993-08-06
申请人： Guenter Uphues , Sven Jaensch , Uwe Ploog , Udo Steinberner
发明人： Guenter Uphues , Sven Jaensch , Uwe Ploog , Udo Steinberner
IPC分类号： C07D233/14 , C07D233/60 , C07D233/04
CPC分类号： C07D233/14
摘要： A process is disclosed for producing fluid imidazolinium tensides by reaction of 1-hydroxyethyl-2-alkylimidazolines with neutralized quaternary agents and hydrolysis of the quaternary products thus obtained with aqueous bases. The 1-hydroxyethyl -2-alkylimidazolines are added at a high temperature to an aqueous solution of the neutralized quaternary agents at a molar proportion between imidazoline derivates and the quaternary agents from 1:1.5 to 1:3. The reaction mixture thus obtained is maintained at a temperature in a range of 70.degree. to 85.degree. C. for 30 to 120 minutes, 0.85 to 1.0 mol alkali metal hydroxides, referred to the amount of quaternary agents added during step (a), are added thereto within the 30 to 120 minutes at a temperature in the range of 75.degree. to 85.degree. C., and the reaction mixture thus obtained is maintained at a temperature in the range of 75.degree. to 90.degree. C. for 140 to 220 minutes. The end products are obtained by a process that is easy to carry out if during step (a) a solution of neutralized quaternary agents is used that contains 0.025 to 0.5 mol of carboxylic acids, referred to the amount to be added of 1-hydroxyethyl-2-alkylimidazolines, and if acids are added to the reaction mixture obtained during step (d), so that when the reaction mixture is diluted with water up to a 10 wt % concentration of the product, a pH value in the range of 7 to 10 is set.
摘要翻译： PCT No.PCT / EP91 / 02254 Sec。 371日期：1993年8月6日 102（e）日期1993年8月6日PCT 1991年11月28日PCT PCT。公开号WO92 / 10481 日期：1992年6月25日。公开了通过1-羟乙基-2-烷基咪唑与中和的季铵化合物反应制备流体咪唑啉表面活性剂的方法，并用水性碱水解所得的季产物。 1-羟乙基-2-烷基咪唑啉在高温下加入到中和的季铵盐的水溶液中，咪唑啉衍生物与季胺之间的摩尔比例为1:1.5至1:3。将如此得到的反应混合物保持在70〜85℃的温度下30〜120分钟，在工序（a）中添加的季铵化合物的量为0.85〜1.0摩尔碱金属氢氧化物为在75〜85℃的温度下在30〜120分钟内加入，将得到的反应混合物在75〜90℃的温度下保持140〜220分钟。如果在步骤（a）中使用含有0.025至0.5mol羧酸的中和季铵盐溶液，则称为最终产物，其中加入的1-羟乙基 - 2-烷基咪唑啉，并且如果将酸加入到步骤（d）中获得的反应混合物中，使得当反应混合物用水稀释至10重量％浓度的产物时，pH值在7至 10设置。

42. 发明授权

US4983778A Alkoxylation process using a catalyst composition containing esters of titanic acid and zirconic acid 失效
标题翻译：使用含有钛酸和锆酸的酯的催化剂组合物的烷氧基化方法
公开(公告)号：US4983778A
公开(公告)日：1991-01-08
申请号：US346037
申请日：1989-05-02
申请人： Uwe Ploog
发明人： Uwe Ploog
IPC分类号： B01J31/02 , C07B61/00 , C07C41/00 , C07C41/03 , C07C43/11 , C07C67/00
CPC分类号： C07C41/03
摘要： Alkoxylation products of organic compounds containing active H atoms with a narrow homolog distribution range is produced by using as a catalyst in the alkoxylation process a catalyst composition comprising:a. Esters of titanic and/or zirconic acid with monoalkanols containing 1 to 4 carbon atoms in combination with,b. sulfuric acid and/or alkanesulfonic acid containing 1 to 6 carbon atoms and/or hydroxyarylsulfonic acids as catalysts for the ethoxylation or propoxylation of compounds containing active H atoms provide the alkoxylation products with a narrow homolog distribution range.
摘要翻译：通过在烷氧基化方法中使用催化剂组合物作为催化剂，通过使用包含以下物质的催化剂组合物来制备含有具有窄同系物分布范围的活性H原子的有机化合物的烷氧基化产物：a。含有1至4个碳原子的单链烷醇的钛酸和/或锆酸的酯与b组合。含有1至6个碳原子的硫酸和/或链烷磺酸和/或羟基芳基磺酸作为用于含有活性H原子的化合物的乙氧基化或丙氧基化的催化剂提供了具有窄的同系物分布范围的烷氧基化产物。

43. 发明授权

US4865614A Quaternary 2-alkylimidazolinium salts as fabric softeners 失效
标题翻译：第四纪2-烷基咪唑啉鎓盐作为织物柔软剂
公开(公告)号：US4865614A
公开(公告)日：1989-09-12
申请号：US57555
申请日：1987-06-03
申请人： Uwe Ploog , Guenter Uphues
发明人： Uwe Ploog , Guenter Uphues
IPC分类号： C07D233/06 , C07D233/14 , C07D233/16 , D06M13/02 , D06M13/322 , D06M13/352 , D06M13/46 , D06M13/47 , D06M13/473
CPC分类号： C07D233/14 , C07D233/16 , D06M13/352
摘要： The reaction of 2-alkylimidazolines with ethylene oxide or propylene oxide gives quaternary 2-alkyl-2-imidazolinium salts corresponding to the following general formula ##STR1## wherein R.sup.1 represents a straight-chain or branched-chain substituted or unsubstituted alkyl or alkenyl radical containing from 7 to 21 carbon atoms,R.sup.2 represents one of the following radicals ##STR2## R.sup.3 represents hydrogen or methyl, R.sup.4 represents hydrogen or methyl,X.sup..crclbar. represents the anion of a non-oxidizing and non-corrosive inorganic acid or of an organic mono- or polycarboxylic acid,n statistically represents a whole or fraction number of from 1 to 20, andm represents an integer of from 1 to 3, which may be used for softening laundered fabrics.
摘要翻译： 2-烷基咪唑与环氧乙烷或环氧丙烷的反应产生对应于下列通式（I）的季铵-2-烷基-2-咪唑啉鎓盐，其中R 1表示直链或支链取代或未取代的烷基或含有7〜21个碳原子的链烯基，R2代表下列基团之一：R 3表示氢或甲基，R 4表示氢或甲基，X（ - ）表示非氧化性和非腐蚀性无机酸的阴离子或有机单羧酸或多元羧酸，n统计学上表示1至20的整数或级分数，m表示1至3的整数，其可用于软化洗涤织物。

44. 发明授权

US4820436A Detergents for low laundering temperatures 失效
标题翻译：洗涤剂的洗涤温度低
公开(公告)号：US4820436A
公开(公告)日：1989-04-11
申请号：US19278
申请日：1987-02-20
申请人： Hans Andree , Horst Baumann , Manfred Biermann , Frantisek Jost , Horst-Juergen Krause , Fritz Lange , Herbert Leiter , Alfred Meffert , Uwe Ploog , Harald Schnegelberger , Eduard Smulders , Eric Sung , Andreas Syldatk , Guenter Uphues , Guenther Vogt
发明人： Hans Andree , Horst Baumann , Manfred Biermann , Frantisek Jost , Horst-Juergen Krause , Fritz Lange , Herbert Leiter , Alfred Meffert , Uwe Ploog , Harald Schnegelberger , Eduard Smulders , Eric Sung , Andreas Syldatk , Guenter Uphues , Guenther Vogt
IPC分类号： C11D1/44 , C11D3/26 , C11D3/28 , C11D3/30 , C11D3/32 , C11D3/18
CPC分类号： C11D3/26 , C11D1/44 , C11D3/28 , C11D3/30 , C11D3/32
摘要： Detergents on the basis of anionic and nonionic surfactants contain as laundering power-enhancing additives an aliphatic amine compound which is selected such that its pK.sub.b value is at least equal to 14, minus the initial pH value of a 1% aqueous solution of the detergent containing the amine compound. Laundering power-enhancing amine compounds selected according to the rule mentioned are certain ether amines, amidoamines, glucamine derivatives or morpholine derivatives.
摘要翻译： PCT No.PCT / EP86 / 00356 Sec。 371日期1987年2月20日 102（e）1987年2月20日PCT PCT。1986年6月16日PCT公布。公开号WO86 / 07603 日期为1986年12月31日。基于阴离子和非离子表面活性剂的脱水剂含有作为洗涤力增强添加剂的脂族胺化合物，其选择为使得其pKb值至少等于14，减去初始pH值1 含有胺化合物的洗涤剂的％水溶液。根据上述规定选择的洗涤力增强胺化合物是某些醚胺，酰氨基胺，葡糖胺衍生物或吗啉衍生物。

45. 发明授权

US4814070A Alkyl sulfosuccinates based on alkoxylated fatty alcohols as collectors for non-sulfidic ores 失效
标题翻译：基于烷氧基化脂肪醇的烷基磺基琥珀酸盐作为非硫化矿石的收集剂
公开(公告)号：US4814070A
公开(公告)日：1989-03-21
申请号：US128135
申请日：1987-12-03
申请人： Rita Koester , Wolfgang von Rybinski , Uwe Ploog
发明人： Rita Koester , Wolfgang von Rybinski , Uwe Ploog
IPC分类号： B03D1/00 , B03D1/012 , B03D1/02
CPC分类号： B03D1/012 , B03D2201/02 , B03D2201/04 , B03D2203/04
摘要： Alkyl sulfosuccinates based on propoxylated and propoxylated and ethoxylated fatty alcohols as flotation collectors for non-sulfidic ores and to a process for the separation of non-sulfidic ores by flotation in which the alkyl sulfosuccinates used contain one or two identical or different, straight-chain and/or branched-chain, saturated or unsaturated alkyl radicals based on propoxylated or propoxylated and ethoxylated C.sub.8 -C.sub.22 fatty alcohols.
摘要翻译：基于丙氧基化和丙氧基化和乙氧基化脂肪醇的烷基磺基琥珀酸盐作为非硫化矿石的浮选捕收剂，以及通过浮选分离非硫化矿石的方法，其中使用的烷基磺基琥珀酸盐含有一个或两个相同或不同的直链和/或基于丙氧基化或丙氧基化和乙氧基化的C 8 -C 22脂肪醇的支链，饱和或不饱和的烷基。

46. 发明授权

US4803068A Hair-treatment preparation for improved wet combability 失效
标题翻译：用于改善湿梳理性能的头发处理剂
公开(公告)号：US4803068A
公开(公告)日：1989-02-07
申请号：US115553
申请日：1987-10-28
申请人： Uwe Ploog , Peter Busch , Klaus Thiele , Horst Hoffkes , Karl Giede
发明人： Uwe Ploog , Peter Busch , Klaus Thiele , Horst Hoffkes , Karl Giede
IPC分类号： A61K8/00 , A61K8/44 , A61K8/46 , A61K8/55 , A61Q5/00 , A61Q5/02 , A61Q5/12 , C11D3/36 , A61K7/075 , A61K7/08
CPC分类号： A61K8/55 , A61K8/442 , A61K8/463 , A61K8/466 , A61Q5/02 , A61Q5/12
摘要： Hair-treatment preparations containing as additive at least one surface-active phosphonic acid corresponding to general formula I, II or III below ##STR1## in which R.sup.1 represents a C.sub.5 -C.sub.21 alkyl, R.sup.2 represents hydrogen or --PO.sub.3 H.sub.2, and R.sup.3 represents hydrogen, hydroxyl, or, if R.sup.2 is --PO.sub.3 H.sub.2, --NH.sub.2, and R.sup.4 represents hydrogen or a lower alkyl group containing from 1 to 4 carbon atoms, or a water-soluble salt thereof, improved the wet combability of hair and reduce its tendency to develop static charges. Octane-1-phosphonic acid, decane-1-phosphonic acid and dodecane-1-phosphonic acid or their salts are particularly effective. The phophonic acids are used in quantities of from 0.05 to 10% by weight, and preferably in quantities of from 0.1 to 2.0% by weight together with anionic tensides.
摘要翻译：含有对应于下述通式I，II或III的至少一种表面活性膦酸作为添加剂的头发处理制剂，其中R1表示C5- C21烷基，R2表示氢或-PO3H2，R3表示氢，羟基，或者如果R2是-PO3H2，-NH2和R4表示氢或含有1至4个碳原子的低级烷基，或水溶性其改善了头发的湿梳理性，并降低了其产生静电荷的倾向。辛烷-1-膦酸，癸烷-1-膦酸和十二烷-1-膦酸或其盐是特别有效的。与阴离子表面活性剂一起使用的磷酸的量为0.05-10重量％，优选为0.1-2.0重量％。

47. 发明授权

US4309176A Process for the oiling and impregnation of leather and pelts 失效
标题翻译：皮革和毛皮的上油和浸渍工艺
公开(公告)号：US4309176A
公开(公告)日：1982-01-05
申请号：US185605
申请日：1980-09-10
申请人： Hans-Herbert Friese , Jurgen Plapper , Uwe Ploog , Emil Ruscheinsky
发明人： Hans-Herbert Friese , Jurgen Plapper , Uwe Ploog , Emil Ruscheinsky
IPC分类号： B01F17/00 , C14C9/02
CPC分类号： B01F17/0064 , B01F17/0057 , C14C9/02
摘要： This invention is directed to an improved process of oiling and impregnating leather or pelts in which the leather or pelts are contacted with one or more oiling substances in an aqueous liquor, wherein the improvement comprises using an alkylolamide ether sulfate or phosphate of fatty acids of the formulaR--CO--NH--(CH.sub.2).sub.n --O--(CH.sub.2 --CH.sub.2 --O).sub.m XwhereinR represents an aliphatic radical of from about 13 to 19 carbon atoms;n is a number of from 2 to 4;m is a number of from 1 to 4;X is --SO.sub.3 Y or --PO(OY).sub.2 ; andY is a sodium, potassium, or ammonium anionas an oiling substance in the liquor bath.
摘要翻译：本发明涉及一种改善的方法，其中提炼和浸渍皮革或毛皮，其中皮革或毛皮与水性液体中的一种或多种上油物质接触，其中改进包括使用烷基酰胺醚硫酸盐或磷酸脂肪酸式R-CO-NH-（CH2）nO-（CH2-CH2-O）mX其中R表示约13至19个碳原子的脂族基团; n是从2到4的数字; m是从1到4的数字; X是-SO 3 Y或-PO（OY）2; Y是在液浴中作为油性物质的钠，钾或铵阴离子。

48. 发明授权

US4292088A Beeswax substitute 失效
标题翻译：蜂蜡替代品
公开(公告)号：US4292088A
公开(公告)日：1981-09-29
申请号：US102266
申请日：1979-12-10
申请人： Ingeborg Scheuffgen , Uwe Ploog
发明人： Ingeborg Scheuffgen , Uwe Ploog
IPC分类号： A61K8/30 , A61K8/06 , A61K8/31 , A61K8/36 , A61K8/365 , A61K8/37 , A61K8/39 , A61Q1/00 , A61Q1/04 , A61Q1/06 , A61Q19/00 , C08L91/06 , C11B11/00 , A61K7/00 , A61K7/025 , C08L91/08
CPC分类号： A61K8/361 , A61K8/375 , A61K8/39 , A61Q1/06 , A61Q19/00 , C08L91/06
摘要： This invention is directed to a substitute beeswax composition comprised of:mono-, di-, and triglycerides of long-chain fatty acids;esters of long-chain fatty acids with higher-molecular fatty alcohols;higher fatty acids;optionally microcrystalline paraffins; andfrom about 3 to 15% by weight, based on the weight of the total composition, of .alpha.-branched, aliphatic monocarboxylic acids of the general formula ##STR1## in which R represents a linear alkyl radical with from about 12 to 20 carbon atoms. The substitute beeswax composition is useful in the preparation of cosmetic compositions.
摘要翻译：本发明涉及一种替代蜂蜡组合物，其包含：长链脂肪酸的一，二和甘油三酯; 长链脂肪酸与高分子脂肪醇的酯类; 高级脂肪酸; 任选的微晶石蜡; 和约3至15重量％，基于总组合物的重量，通式为“IMAGE”的α-支链脂肪族单羧酸，其中R表示具有约12至20个碳原子的直链烷基。替代蜂蜡组合物可用于制备化妆品组合物。

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