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41. 发明授权

US06444623B1 Methods for the production of sulfurized diphenyloxides and compositions made therefrom 失效
标题翻译：生产硫化二苯醚及其制备的组合物的方法
公开(公告)号：US06444623B1
公开(公告)日：2002-09-03
申请号：US09473556
申请日：1999-12-29
申请人： Margaret M. Wu , Philip Trotto , Rene B. LaPierre
发明人： Margaret M. Wu , Philip Trotto , Rene B. LaPierre
IPC分类号： C10M11102
CPC分类号： C07D327/08 , C07C319/14 , C07C323/20
摘要： The present invention relates to methods for production of sulfurized diphenyloxides wherein a diphenyloxide is reacted with elemental sulfur in the presence of solid acid catalyst. The solid acid catalyst can be a zeolite or a catalytic amount of a Friedel-Crafts compound. The present invention further relates to a composition containing between about 40 and about 80 weight percent diphenyloxide; no more than about 15 weight percent diphenyloxide thiol; between about 5 and about 45 weight percent phenoxathiin; and between about 3 and about 50 weight percent total of bis(diphenyloxide) sulfide, diphenyloxide phenoxathiin sulfide, and bis(phenoxathiin) sulfide.
摘要翻译：本发明涉及在固体酸催化剂存在下使二苯醚与元素硫反应生产硫化二苯醚的方法。固体酸催化剂可以是沸石或催化量的Friedel-Crafts化合物。本发明还涉及含有约40至约80重量％二苯醚的组合物; 不超过约15重量％的二苯醚硫醇; 约5至约45重量％的吩霉素; 和双（二苯醚）硫化物，二苯氧基苯硫硫脲硫化物和双（苯氧硫杂）硫化物的总计约3至约50重量％。

42. 发明授权

US5451704A Alpha-olefin oligomerization using supported metal halide catalysts 失效
标题翻译：使用负载金属卤化物催化剂的α-烯烃低聚
公开(公告)号：US5451704A
公开(公告)日：1995-09-19
申请号：US057029
申请日：1993-05-05
申请人： Suzzy C. Ho , Margaret M. Wu
发明人： Suzzy C. Ho , Margaret M. Wu
IPC分类号： B01J37/02 , B01J37/08 , C07C2/66 , C07C2/30
CPC分类号： B01J37/0215 , B01J37/086 , C07C2/66 , C07C2521/06 , C07C2521/08 , C07C2521/12 , C07C2523/10 , C07C2523/22 , C07C2527/167 , C07C2529/70
摘要： A process for the production of hydrocarbon lubricant basestock comprises contacting C.sub.2 to C.sub.20 alpha-olefin feedstock, or mixtures thereof, e.g., 1-decene, under heterogeneous oligomerization conditions with a catalyst comprising halides of a metal component anchored on an adsorbent inorganic oxide solid, e.g., silica, by an oxygen-metal bond to provide a reaction mixture containing said hydrocarbon lubricant basestock. The catalyst is prepared by contacting the inorganic oxide solid with organic metal halide of the formula RMXY wherein R is alkyl or aryl, M is aluminum, X is halogen and Y is selected from the group consisting of halogen, alkyl, alkenyl, aryl, alkoxy, and amido moieties.
摘要翻译：用于生产烃润滑剂基础油料的方法包括在非均相低聚条件下使C2-C20α-烯烃原料或其混合物例如1-癸烯与包含锚定在吸附剂无机氧化物固体上的金属组分的卤化物接触，例如二氧化硅，通过氧 - 金属键提供含有所述烃润滑剂基础油料的反应混合物。通过使无机氧化物固体与式RMXY的有机金属卤化物接触来制备催化剂，其中R是烷基或芳基，M是铝，X是卤素，Y选自卤素，烷基，烯基，芳基，烷氧基和酰氨基部分。

43. 发明授权

US5321190A Oligomerization of ethylene with a supported nickel catalyst 失效
标题翻译：乙烯与负载型镍催化剂的低聚
公开(公告)号：US5321190A
公开(公告)日：1994-06-14
申请号：US131360
申请日：1993-10-04
申请人： Brent A. Aufdembrink , Margaret M. Wu
发明人： Brent A. Aufdembrink , Margaret M. Wu
IPC分类号： B01J23/755 , B01J29/04 , C07C2/10 , C07C2/24 , C07C2/02
CPC分类号： B01J29/049 , B01J23/755 , C07C2/10 , C07C2521/06 , C07C2523/755 , Y02P20/52
摘要： There is provided a catalyst comprising nickel supported on a pillared (e.g., silica pillared) vacancy titanate material. There is also provided a method for preparing this catalyst. This method may involve impregnating a pillared vacancy titanate material with a nickel nitrate solution. There is further provided a process for oligomerizing ethylene using this catalyst.
摘要翻译：提供了包含负载在柱状（例如二氧化硅柱状）空位钛酸盐材料上的镍的催化剂。还提供了制备该催化剂的方法。该方法可以包括用硝酸镍溶液浸渍柱状空位钛酸盐材料。还提供了使用该催化剂使乙烯低聚的方法。

44. 发明授权

US5146022A High VI synthetic lubricants from cracked slack wax 失效
标题翻译：高VI合成润滑油从裂纹松散蜡
公开(公告)号：US5146022A
公开(公告)日：1992-09-08
申请号：US571345
申请日：1990-08-23
申请人： J. Scott Buchanan , Margaret M. Wu
发明人： J. Scott Buchanan , Margaret M. Wu
IPC分类号： C10M107/10
CPC分类号： C10M107/10 , C10M2205/028 , C10M2205/14 , C10M2205/16 , C10M2205/17 , C10M2205/18
摘要： A process is disclosed for the production of synthetic lubricants having high viscosity index and thermal stability by oligomerizing a mixture of C.sub.5 -C.sub.18 or C.sub.6 -C.sub.16 alpha-olefins produced from the thermal cracking of slack wax or recycled slack wax. The oligomerization is carried out with Lewis acid catalyst. Promoted aluminum chloride is a preferred catalyst.
摘要翻译：公开了通过使由松散蜡或回收的松散蜡的热裂解产生的C5-C18或C6-C16α-烯烃的混合物低聚而生产具有高粘度指数和热稳定性的合成润滑剂的方法。低聚反应用路易斯酸催化剂进行。促进的氯化铝是优选的催化剂。

45. 发明授权

US5113030A High viscosity index lubricant compositions 失效
标题翻译：高粘度指数润滑剂组合物
公开(公告)号：US5113030A
公开(公告)日：1992-05-12
申请号：US570745
申请日：1990-08-22
申请人： Catherine S. H. Chen , Margaret M. Wu
发明人： Catherine S. H. Chen , Margaret M. Wu
IPC分类号： C10G50/02 , C10M169/04
CPC分类号： C10G50/02 , C10M169/041 , C10M2203/0206 , C10M2205/024 , C10M2205/0245 , C10M2205/026 , C10M2205/0265 , C10M2205/028 , C10N2220/02
摘要： Novel synthetic lubricants having high viscosity index are made from lower olefins. These materials have a viscosity above about 2 cS at 100.degree. C. and viscosity index above about 130 and are characterized by internal methyl groups attached to side chain tertiary carbon atoms.Hydrocarbon lubricant can be based on propene feedstock with the resulting oligomer containing less than 2.5 methyl groups per 12 carbon atoms.
摘要翻译：具有高粘度指数的新型合成润滑剂由低级烯烃制成。这些材料在100℃下的粘度高于约2cS，粘度指数高于约130，其特征在于连接在侧链叔碳原子上的内部甲基。烃润滑剂可以基于丙烯原料，所得到的低聚物每12个碳原子含有少于2.5个甲基。

46. 发明授权

US5079385A Conversion of plastics 失效
标题翻译：塑料转换
公开(公告)号：US5079385A
公开(公告)日：1992-01-07
申请号：US394901
申请日：1989-08-17
申请人： Margaret M. Wu
发明人： Margaret M. Wu
IPC分类号： B09B3/00 , B29B17/00 , C07C4/00 , C10G1/08 , C10G1/10
CPC分类号： C07C4/00 , C10G1/08 , C07C2521/06 , C07C2521/10 , C07C2523/06 , C07C2523/08 , C07C2523/20 , C07C2523/26 , C07C2523/28 , C07C2523/30 , C07C2523/42 , C07C2523/44 , C07C2523/745 , C07C2523/75 , C07C2523/755 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/50 , C07C2529/60 , C07C2529/65 , C07C2529/70
摘要： A process for converting solid plastic materials, preferably waste materials, into usable lower molecular weight hydrocarbonaceous materials by reacting such plastic materials at elevated temperatures in effective contact with an acidic catalyst comprising at least one zeolite having acid activity.

47. 发明授权

US4668650A Catalyst composition for polymerizing alpha-olefin polymers of relatively narrow molecular weight distribution 失效
标题翻译：用于聚合具有相对较窄分子量分布的α-烯烃聚合物的催化剂组合物
公开(公告)号：US4668650A
公开(公告)日：1987-05-26
申请号：US815845
申请日：1986-01-03
申请人： Frederick Y. Lo , Thomas E. Nowlin , Margaret M. Wu
发明人： Frederick Y. Lo , Thomas E. Nowlin , Margaret M. Wu
IPC分类号： C08F4/60 , C08F4/62 , C08F4/64 , C08F10/00 , C08F4/68
CPC分类号： C08F10/00
摘要： A catalyst composition for polymerizing alpha-olefins is prepared by treating a carrier containing OH groups with a liquid solution containing an excess of an organomagnesium composition with respect to the OH groups and contacting the thus-formed magnesium-containing carrier with a hydrocarbyl alcohol and at least one transition metal compound. Prior to contacting the magnesium-containing carrier with the alcohol, most of the liquid must be removed therefrom, so that it comprises not more than about 6% of the liquid. The amount of the transition metal compound is such that the molar ratio thereof to magnesium in the reaction mixture is about 0.3 to about 0.9. Also disclosed is a process for polymerizing alpha-olefins in the presence of the catalyst of the invention.
摘要翻译：用于聚合α-烯烃的催化剂组合物通过用含有过量的有机镁组合物的液体溶液相对于OH基团处理含有OH基团的载体并将如此形成的含镁载体与烃基接触并在至少一种过渡金属化合物。在使含镁载体与醇接触之前，大部分液体必须从其中除去，使其不超过约6％的液体。过渡金属化合物的量使得其与反应混合物中的镁的摩尔比为约0.3至约0.9。还公开了在本发明催化剂存在下聚合α-烯烃的方法。

48. 发明授权

US4391998A Production of para-isopropylphenol 失效
标题翻译：对异丙基苯酚的生产
公开(公告)号：US4391998A
公开(公告)日：1983-07-05
申请号：US313425
申请日：1981-10-21
申请人： Margaret M. Wu
发明人： Margaret M. Wu
IPC分类号： C07C37/14 , C07C39/06
CPC分类号： C07C37/14 , C07C37/16
摘要： Phenol is catalytically alkylated with an isopropanol or propylene alkylating agent to form high yields of an isopropylphenol product enriched in the para-isomer of isopropylphenol. Such an alkylation process is carried out under catalytic alkylation conditions including a temperature of from about 200.degree. C. to 300.degree. C. and contact with a crystalline zeolite catalyst having a silica to alumina molar ratio of at least about 12 and a constraint index of about 1 to 12.
摘要翻译：苯酚用异丙醇或丙烯烷基化剂催化烷基化以形成富含异丙基苯酚对位异构体的异丙基苯酚产物的高收率。这样的烷基化方法在催化烷基化条件下进行，包括温度为约200℃至300℃，并与二氧化硅与氧化铝摩尔比至少约为12的结晶沸石催化剂接触，并且约束指数约1至12。

49. 发明授权

US4379027A Selective hydrogenation of vinyltoluene 失效
标题翻译：乙烯基甲苯的选择性氢化
公开(公告)号：US4379027A
公开(公告)日：1983-04-05
申请号：US334346
申请日：1981-12-24
申请人： John M. Klosek , Margaret M. Wu
发明人： John M. Klosek , Margaret M. Wu
IPC分类号： C07C7/163 , B01D3/14 , C07C5/10 , C07C7/04
CPC分类号： C07C7/163
摘要： This invention provides a process for obtaining m-methylstyrene from a mixture with p-methylstyrene that comprises hydrogenating a mixture of p-methylstyrene and m-methylstyrene in the presence of a zeolite having a Constraint Index of about 1 to about 12, a silica to alumina mole ratio of at least about 12, and a dried crystal density of not less than about 1.6 grams per cubic centimeter, modified with at least one element of Group IA, IIA, IVB, or VB of the Periodic Chart of the Elements and a metal of Group VIII of the Periodic Chart of the Elements; thereby obtaining a mixture of m-methylstyrene and p-ethyltoluene, and removing p-ethyltoluene by distillation.
摘要翻译：本发明提供从与对甲基苯乙烯的混合物中获得间甲基苯乙烯的方法，该方法包括在约1至约12的约束指数的沸石存在下氢化对甲基苯乙烯和间甲基苯乙烯的混合物，氧化铝摩尔比为至少约12，干燥晶体密度不小于约1.6克/立方厘米，用元素周期表的IA，IIA，IVB或VB族元素的至少一种元素修饰，元素周期表第八组金属; 从而获得间甲基苯乙烯和对乙基甲苯的混合物，并通过蒸馏除去对乙基甲苯。

50. 发明授权

US4197413A Production of 3-methylphenol 失效
标题翻译：生产3-甲基苯酚
公开(公告)号：US4197413A
公开(公告)日：1980-04-08
申请号：US969628
申请日：1978-12-14
申请人： Warren W. Kaeding , Margaret M. Wu , Lewis B. Young , George T. Burress
发明人： Warren W. Kaeding , Margaret M. Wu , Lewis B. Young , George T. Burress
IPC分类号： C07C2/66 , C07C4/18 , C07C7/148 , C07C37/08 , C07C39/07 , C07C409/08
CPC分类号： C07C409/08 , C07C2/66 , C07C37/08 , C07C4/18 , C07C407/00 , C07C7/148 , B01J2229/20 , C07C2529/40 , C07C2529/70 , Y02P20/582
摘要： A four-step method for the selective production of the 1,3-isomer of methylphenol comprising the alkylation of toluene with propylene in the presence of a specified type of zeolite alkylation catalyst followed by the selective reaction, via a specified type of shape selective zeolite, of the 1,4-isomer of the alkylation product to leave the 1,3-isomer thereof in excess of equilibrium. Subsequent oxidation and acid catalyzed rearrangement results in desirably high yield of 3-methylphenol.
摘要翻译：选择性生产甲基苯酚的1,3-异构体的四步法包括在特定类型的沸石烷基化催化剂的存在下，通过特定类型的形状选择性沸石，在特定类型的沸石烷基化催化剂存在下甲苯与甲苯进行烷基化反应的烷基化产物的1,4-异构体，以使其1,3-异构体超过平衡。随后的氧化和酸催化重排导致期望的高产率的3-甲基苯酚。

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