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41. 发明申请

US20120190895A1 PRODUCING ALPHA,BETA-UNSATURATED ALDEHYDES BY MEANS OF A REACTION MIXING PUMP 有权
标题翻译：通过反应混合泵生产ALPHA，BETA不饱和醛
公开(公告)号：US20120190895A1
公开(公告)日：2012-07-26
申请号：US13498690
申请日：2010-08-03
申请人： Alfred Kaizik , Hans-Gerd Lueken , Dirk Fridag , Wilfried Bueschken , Dirk Mackowiak , Frank Brocksien
发明人： Alfred Kaizik , Hans-Gerd Lueken , Dirk Fridag , Wilfried Bueschken , Dirk Mackowiak , Frank Brocksien
IPC分类号： C07C45/72
CPC分类号： C07C45/74 , Y02P20/582 , C07C47/21
摘要： The invention relates to a method for producing α,β-unsaturated aldehydes, wherein a catalytic aldol condensation of charged aldehydes is carried out in the presence of an aqueous base within a continuous-flow reactor. The aim of the invention is to provide a method for aldolizing aldehydes that can be carried out in a particularly economical manner. The aim is achieved by using a reaction mixing pump as the reactor.
摘要翻译：本发明涉及一种生产α，β-不饱和醛的方法，其中在连续流动反应器内的碱性水溶液存在下进行带电醛的催化醛醇缩合。本发明的目的是提供一种可以以特别经济的方式进行醛脱醛化的方法。目的是通过使用反应混合泵作为反应器来实现。

42. 发明授权

US08207375B2 Microporous catalyst and method for hydrogenating aromatic compounds 有权
标题翻译：微孔催化剂和芳烃化合物的加氢方法
公开(公告)号：US08207375B2
公开(公告)日：2012-06-26
申请号：US12025292
申请日：2008-02-04
申请人： Michael Grass , Alfred Kaizik , Wilfried Bueschken , Axel Tuchlenski , Dietrich Maschmeyer , Kurt-Alfred Gaudschun , Frank Brocksien
发明人： Michael Grass , Alfred Kaizik , Wilfried Bueschken , Axel Tuchlenski , Dietrich Maschmeyer , Kurt-Alfred Gaudschun , Frank Brocksien
IPC分类号： C08C19/02 , C07C51/36 , B01J35/10
CPC分类号： B01J21/063 , B01J23/40 , B01J23/462 , B01J35/10 , B01J35/1061 , B01J35/108 , B01J37/0018 , C07C51/36 , C07C67/303 , C07C2601/14 , Y02P20/582 , C07C61/135 , C07C69/75
摘要： The invention relates to the hydrogenation of aromatic compounds, in particular the preparation of alicyclic polycarboxylic acids or their esters by core hydrogenation of the corresponding aromatic polycarboxylic acids or their esters, and also to catalysts suitable therefore.
摘要翻译：本发明涉及芳族化合物的氢化，特别是通过相应的芳族多元羧酸或其酯的核心氢化制备脂环族多元羧酸或其酯，以及由此合适的催化剂。

43. 发明申请

US20110130595A1 PROCESS FOR PREPARING C5 ALDEHYDE MIXTURES WITH A HIGH N-PENTANAL CONTENT 有权
标题翻译：制备具有高N-PENTANAL CONTENT的C5醛类混合物的方法
公开(公告)号：US20110130595A1
公开(公告)日：2011-06-02
申请号：US12995800
申请日：2009-04-28
申请人： Hans-Gerd Lueken , Dirk Fridag , Udo Lenz , Hermann-Josef Schulte-Althoff , Klaus-Diether Wiese , Alfred Kaizik , Patrick Muhlack , Wilfried Bueschken , Frank Hoeper
发明人： Hans-Gerd Lueken , Dirk Fridag , Udo Lenz , Hermann-Josef Schulte-Althoff , Klaus-Diether Wiese , Alfred Kaizik , Patrick Muhlack , Wilfried Bueschken , Frank Hoeper
IPC分类号： C07C45/00
CPC分类号： B01J31/0237 , B01J31/185 , B01J2231/321 , B01J2531/822 , C07C45/50 , Y02P20/582 , C07C47/02
摘要： A process for preparing a C5 aldehyde mixture from a hydrocarbon mixture comprising at least one linear butene by terminal hydroformylation under isomerizing conditions, using a catalyst system comprising rhodium, a bisphosphite ligand, and an amine.
摘要翻译：一种通过使用包含铑，二亚磷酸酯配位体和胺的催化剂体系在异构化条件下通过末端加氢甲酰基化从包含至少一个直链丁烯的烃混合物制备C5醛混合物的方法。

44. 发明申请

US20090301348A1 MIXTURE OF DIESTERS OF DIANHYDROHEXITOL DERIVATIVES WITH CARBOXYLIC ACIDS OF THE EMPIRICAL FORMULA C8H17COOH, PROCESS FOR PREPARING THESE DIESTERS, AND USE OF THESE MIXTURES 有权
标题翻译：二恶烷衍生物与实施方案C8H17COOH的羧酸的混合物，制备这些柴油的方法和这些混合物的使用
公开(公告)号：US20090301348A1
公开(公告)日：2009-12-10
申请号：US12523906
申请日：2007-12-21
申请人： Michael Grass , Norbert Scholz , Alfred Kaizik , Wilfried Bueschken , Hans-Gerd Lueken
发明人： Michael Grass , Norbert Scholz , Alfred Kaizik , Wilfried Bueschken , Hans-Gerd Lueken
IPC分类号： C09D5/08 , C09K3/00 , C08L27/06
CPC分类号： C07D493/04 , C08K5/1535 , C08L27/06
摘要： The present invention relates to a mixture comprising diesters of the formula (I) where R1 to R8═H or alkyl group having from 1 to 6 carbon atoms, where the R1 to R8 radicals may be the same or different, which is characterized in that at least two different diesters I are present in the mixture, said diesters differing in the structure of at least one of the carboxylic acid radicals C8H17COO present, to a process for preparing diesters of an isosorbide derivative of the formula I, in which a hexahydric alcohol and/or a monoanhydro or dianhydro derivative of the alcohol is esterified with a mixture of at least two different carboxylic acids of the empirical formula C8H17COOH, and to the use of these mixtures in paints, inks or coatings, in plastisols, adhesives or adhesive components, in sealants, as plasticizers in polymers or polymer components, as solvents, as lubricant oil components and as assistants in metal processing, and also PVC compositions or plastisols comprising PVC and from 5 to 250 parts by mass of the mixture per 100 parts by mass of PVC.
摘要翻译：本发明涉及包含式（I）的二酯的混合物，其中R 1至R 8 -H或具有1至6个碳原子的烷基，其中R 1至R 8基团可以相同或不同，其特征在于混合物中存在至少两种不同的二酯I，所述二酯在存在的羧酸基团C 8 H 17 COO中的至少一种的结构上不同，制备式I的异山梨醇衍生物的二酯的制备方法，其中六元醇和/或醇的单酐或二氢衍生物与经验式C 8 H 17 COOH的至少两种不同羧酸的混合物酯化，并且在涂料，油墨或涂料中，在增塑溶胶，粘合剂或粘合剂组分中使用这些混合物，作为聚合物或聚合物组分中的增塑剂，作为溶剂，作为润滑油组分和金属加工助剂，以及包含PVC和f的PVC组合物或增塑溶胶相对于100质量份的PVC为5〜250质量份的混合物。

45. 发明授权

US07495134B2 Carbonylation method by adding secondary sterically hindered amines 有权
标题翻译：通过添加第二空间位阻胺的羰基化方法
公开(公告)号：US07495134B2
公开(公告)日：2009-02-24
申请号：US12065091
申请日：2006-06-02
申请人： Dieter Hess , Dagmara Ortmann , Oliver Moeller , Klaus-Diether Wiese , Dirk Fridag , Wilfried Bueschken
发明人： Dieter Hess , Dagmara Ortmann , Oliver Moeller , Klaus-Diether Wiese , Dirk Fridag , Wilfried Bueschken
IPC分类号： C07C45/50 , B01J31/00
CPC分类号： C07C45/50 , B01J31/0237 , B01J31/0247 , B01J31/24 , B01J2231/321 , C07F9/65744 , C07C47/02
摘要： The invention relates to a process for reaction of a carbonylatable compound using a metal complex catalyst comprising a metal of transition group VIII and an organophosphorus ligand and in the presence of a stabilizer based on a sterically hindered secondary amine.
摘要翻译：本发明涉及使用包含过渡族VIII金属和有机磷配体的金属络合物催化剂和基于空间位阻仲胺的稳定剂存在下使羰基化化合物反应的方法。

46. 发明授权

US07154012B2 Process for preparing alcohols from olefins by hydroformylation and hydrogenation 有权
公开(公告)号：US07154012B2
公开(公告)日：2006-12-26
申请号：US11296310
申请日：2005-12-08
申请人： Hans-Gerd Lueken , Alfred Kaizik , Wilfried Bueschken , Andreas Stenert
发明人： Hans-Gerd Lueken , Alfred Kaizik , Wilfried Bueschken , Andreas Stenert
IPC分类号： C07C29/14
CPC分类号： C07C45/50 , C07C29/141 , C07C31/125 , C07C47/02
摘要： A process for preparing aliphatic alcohols that includes cobalt-catalyzed hydroformylation of olefins, treatment of a hydroformylation mixture with oxygen-containing gases in the presence of acidic, aqueous cobalt(II) salt solutions, separation of a mixture into an aqueous phase comprising cobalt salts and an organic phase comprising the aliphatic aldehydes, and hydrogenation of an aldehyde-containing organic phase wherein the organic phase and treatment with an adsorbent to separate off cobalt compounds prior to hydrogenation.

47. 发明申请

US20060128998A1 Process for the hydroformylation of olefins 有权
标题翻译：烯烃加氢甲酰化方法
公开(公告)号：US20060128998A1
公开(公告)日：2006-06-15
申请号：US11291858
申请日：2005-12-02
申请人： Hans-Gerd Lueken , Alfred Kaizik , Stefan Drees , Wilfried Bueschken , Wilhelm Droste
发明人： Hans-Gerd Lueken , Alfred Kaizik , Stefan Drees , Wilfried Bueschken , Wilhelm Droste
IPC分类号： C07C45/50
CPC分类号： C07C45/50 , C07C47/02
摘要： A process for the catalytic hydroformylation of olefins having from 6 to 24 carbon atoms, in which the hydroformylation is carried out in one or more stage(s) and a mixture comprising at least one olefin and an aldehyde in a molar ratio of aldehyde to olefin of from 0.005:1 to 0.2:1 is used as feed in at least one of these stages which is carried out in the presence of an unmodified cobalt complex as catalyst.
摘要翻译：具有6至24个碳原子的烯烃的催化加氢甲酰化的方法，其中加氢甲酰化在一个或多个阶段中进行，并且包含至少一种烯烃和醛与醛与烯烃的摩尔比的混合物在作为催化剂的未改性钴络合物的存在下进行的这些阶段中的至少一个中使用0.005:1至0.2:1的进料。

48. 发明授权

US06433230B1 Process for conducting an aldol condensation 有权
标题翻译：醛醇缩合的方法
公开(公告)号：US06433230B1
公开(公告)日：2002-08-13
申请号：US09716941
申请日：2000-11-22
申请人： Wilfried Bueschken , Klaus-Diether Wiese , Guido Protzmann
发明人： Wilfried Bueschken , Klaus-Diether Wiese , Guido Protzmann
IPC分类号： C07C49203
CPC分类号： C07C45/75 , C07C45/74 , C07C47/21 , C07C49/203
摘要： &agr;,&bgr;-Unsaturated keto compounds are prepared by base-catalyzed aldol condensation of aldehydes and/or ketones having from 1 to 15 carbon atoms, comprising: reacting the aldehydes and/or ketones with an aqueous catalyst solution under adiabatic reaction conditions; and separating the reaction mixture obtained by rapid distillation into a top product comprising water, aldehyde and/or ketone and a bottom product comprising &agr;,&bgr;-unsaturated keto compounds and aqueous catalyst phase.
摘要翻译： α，β-不饱和酮化合物通过醛和/或具有1至15个碳原子的酮的碱催化醛醇缩合制备，包括：在绝热反应条件下使醛和/或酮与含水催化剂溶液反应; 并将通过快速蒸馏获得的反应混合物分离成包含水，醛和/或酮的顶部产物和包含α，β-不饱和酮化合物和含水催化剂相的底部产物。

49. 发明授权

US06184424B2 Process for the hydrogenation of hydroformylation mixtures 失效
标题翻译：加氢甲酰化混合物氢化的方法
公开(公告)号：US06184424B2
公开(公告)日：2001-02-06
申请号：US09396367
申请日：1999-09-15
申请人： Wilfried Bueschken , Dietmar Gubisch
发明人： Wilfried Bueschken , Dietmar Gubisch
IPC分类号： C07C2916
CPC分类号： C07C31/125 , C07C29/141 , C07C29/16
摘要： A process for the hydrogenation of reaction mixtures from the hydroformylation of C5 to C24 olefins using hydrogen on fixed catalysts at elevated temperature, in which the aldehydes, alcohols, formates and low-boilers are evaporated from the reaction mixture and passed in the vapor state over a support-free Cu/Cr catalyst.
摘要翻译：使用氢气在固定催化剂上升高的温度下从C5加氢甲酰化C5至C24烯烃的反应混合物的氢化方法，其中醛，醇，甲酸酯和低沸点物从反应混合物中蒸发并在蒸汽状态下通过无支撑的Cu / Cr催化剂。

50. 发明授权

US5831135A Process for the catalytic selective hydrogenation of polyunsaturated organic substances 失效
标题翻译：多不饱和有机物催化选择性氢化方法
公开(公告)号：US5831135A
公开(公告)日：1998-11-03
申请号：US944433
申请日：1997-10-06
申请人： Wilfried Bueschken , Juergen Hummel
发明人： Wilfried Bueschken , Juergen Hummel
IPC分类号： B01J19/18 , B01J19/24 , C07B35/02 , C07B61/00 , C07C5/05 , C07C5/08 , C07C11/02 , C07C11/12 , C07C11/21 , C07C45/62 , C07C49/04 , C07C253/30 , C07C255/02 , C07C29/14
CPC分类号： C07C45/62 , B01J19/1862 , B01J19/245 , B01J19/2465 , C07B35/02 , C07C253/30 , B01J2219/00006 , B01J2219/0011 , B01J2219/00182
摘要： The present invention relates to a process for the catalytic selective hydrogenation of a polyunsaturated organic compound, wherein the hydrogenation is carried out in a plurality of two or more series-connected loops, wherein each loop involves the use of one reactor, which comprises: (a) feeding the polyunsaturated organic compound and hydrogen to an upper part of a reactor to catalytically hydrogenate said the polyunsaturated organic compound to produce a hydrogenation product, (b) recycling a portion of said hydrogenation product back into said upper part of said reactor, (c) feeding the remainder of said hydrogenation product from said reactor to an upper part of a subsequent reactor wherein the polyunsaturated organic compound is catalytically hydrogenated to produce a subsequent hydrogenation product, and wherein a portion of said subsequent hydrogenation product has been recycled and is fed with said remainder of said hydrogenation product to said upper part of said subsequent reactor, (d) repeating step (c) until the subsequent reactor is the last reactor, (e) recovering the remainder of said subsequent hydrogenation product from said last reactor, and (f) obtaining the desired compound(s) from the product of step (e).
摘要翻译：本发明涉及多不饱和有机化合物的催化选择性氢化方法，其中氢化在多个两个或多个串联连接的环中进行，其中每个环包括使用一个反应器，其包括：（ a）将多不饱和有机化合物和氢气供给到反应器的上部以催化氢化所述多不饱和有机化合物以产生氢化产物，（b）将一部分所述氢化产物再循环回所述反应器的上部（ c）将剩余的所述氢化产物从所述反应器进料到后续反应器的上部，其中所述多不饱和有机化合物被催化氢化以产生随后的氢化产物，并且其中所述后续氢化产物的一部分已经被再循环并进料所述剩余的所述氢化产物存在于所述后续的所述上部反应器，（d）重复步骤（c），直到后续反应器为最后一个反应器，（e）从所述最后一个反应器中回收剩余的所述后续氢化产物，和（f）从下列反应产物中获得所需化合物：步骤（e）。

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