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41. 发明授权

US5965259A Process of making poy polyester fiber 失效
标题翻译：制造聚酯纤维的工艺
公开(公告)号：US5965259A
公开(公告)日：1999-10-12
申请号：US21611
申请日：1998-02-10
申请人： Heinz-Dieter Schumann , Ulrich Thiele
发明人： Heinz-Dieter Schumann , Ulrich Thiele
IPC分类号： C08K5/5317 , D01F6/84 , D02G3/00 , C08G79/02
CPC分类号： D01F6/84 , C08K5/5317 , Y10T428/2913
摘要： The present invention is a pre-oriented, non-stretched polyester fiber spun with spooling speeds of at least 3,000 m/min., wherein the polyester is a copolymer comprised essentially of ethylene terephthalate units and up to 10 weight % of other dicarboxylic acids or other diols, and carboxy phosphonic acid units of the formula: ##STR1## wherein R is selected from C.sub.1-10 -alkylene, C.sub.1-10 -cycloalkylene or C.sub.6-10 -arylene, in a quantity corresponding to 30 to 500 ppm phosphorus, in relation to polyester. The invention also comprises a process for the production of this fiber.
摘要翻译：本发明是一种预卷取的非拉伸聚酯纤维，其纺丝速度为至少3,000m / min，其中聚酯是基本上由对苯二甲酸乙二醇酯单元和至多10重量％的其它二羧酸组成的共聚物或其它二醇和羧基膦酸单元，其结构式如下：其中R选自C 1-10 - 亚烷基，C 1-10 - 亚环烷基或C 6-10 - 亚芳基，相对于聚酯，其量相当于30-500ppm磷。本发明还包括生产该纤维的方法。

42. 发明授权

US5859173A Process for the production of flame-resistant polyesters 失效
标题翻译：生产耐火聚酯的方法
公开(公告)号：US5859173A
公开(公告)日：1999-01-12
申请号：US968607
申请日：1997-11-13
申请人： Heinz-Dieter Schumann
发明人： Heinz-Dieter Schumann
IPC分类号： C08G63/692 , C08G63/00
CPC分类号： C08G63/6926
摘要： The present invention comprises a process for the production of flame-resistant polyesters with at least 50 mol-% ethylene carboxylate units through esterification or ester interchange and co-polycondensation of at least one diol and a dicarboxylic acid or its dialkyl ester with a carboxyphosphinic acid, whereby the carboxyphosphinic acid, before being added to the co-polycondensation mixture, is dissolved in ethylene glycol of not more than 90.degree. C., and the acid number of this solution is standardized to 50 to 350 mg KOH/g of carboxyphosphinic acid by adding at least one basic alkali metal compound in the absence of oxygen, and said solution is added to the co-polycondensation mixture during the second half of the esterification or ester interchange reaction.
摘要翻译：本发明包括通过酯化或酯交换和至少一种二醇和二羧酸或其二烷基酯与羧基次膦酸的共缩聚生产具有至少50mol％乙烯羧酸酯单元的阻燃聚酯的方法，由此将羧基次膦酸在加入共缩合混合物中之前溶于不超过90℃的乙二醇中，该溶液的酸值标准化为50-350mg KOH / g羧基次膦酸通过在不存在氧的情况下加入至少一种碱式碱金属化合物，并且在酯化或酯交换反应的后半段期间将所述溶液加入到共缩聚混合物中。

43. 发明授权

US5795595A Spinning pack with sand filter 失效
标题翻译：带沙子过滤器的纺纱包装
公开(公告)号：US5795595A
公开(公告)日：1998-08-18
申请号：US698684
申请日：1996-09-09
申请人： Heinz-Dieter Beeck , Bernd Kretschmann , Wilhelm Sprick
发明人： Heinz-Dieter Beeck , Bernd Kretschmann , Wilhelm Sprick
IPC分类号： D01D1/10 , D01D4/00 , D01D4/06
CPC分类号： D01D4/00 , D01D1/106
摘要： A spinning pack with a sand filter for the melt spinning of thermoplastics, whereby at least one perforated plate with evenly distributed D-shaped holes with slanting openings that taper conically in the direction of flow is placed in the direction of flow in front of and/or behind the sand filter. Spinning packs according to the invention surprisingly give highly uniform distribution and flow of thermoplastic melt through the sand filter.
摘要翻译：一种具有用于热塑性塑料熔融纺丝的砂过滤器的纺丝组件，其中至少一个具有均匀分布的D形孔的穿孔板，其具有在流动方向上锥形锥形的倾斜开口朝向在/ 或砂滤器后面。根据本发明的纺丝包令人惊奇地使热塑性熔体的分布和流动高度均匀地通过砂过滤器。

44. 发明授权

US5499652A Distributor for viscous fluids with multiple radial; discharge 失效
标题翻译：多径径粘性流体分配器; 卸货
公开(公告)号：US5499652A
公开(公告)日：1996-03-19
申请号：US356141
申请日：1994-12-15
申请人： Walter Schnaus , Michael Streng , Franz Schoenmeier , Stephan Biller
发明人： Walter Schnaus , Michael Streng , Franz Schoenmeier , Stephan Biller
IPC分类号： B29C31/04 , B29C47/70 , D01D1/06 , F16K49/00
CPC分类号： D01D1/06 , B29C31/04 , B29C47/70 , B29C47/0014 , Y10T137/6579 , Y10T137/85938 , Y10T137/87877
摘要： Distributors for viscous fluids, consisting of a central inlet line and at least two valves that are connected radially to the inlet line, each valve having one valve spindle that moves in the axial direction in the cylindrical valve casing and an outlet opening that opens into an outlet line, whereby a flow displacer having a cylindrical bottom part and a conical top part is inserted centrally into the inlet line at the level of the valves, forming a ring gap, and where the cross section of flow is constricted in the outlet opening and then immediately thereafter is enlarged in the outlet line.
摘要翻译：用于粘性流体的分配器由中心入口管线和至少两个径向连接到入口管线的阀门组成，每个阀门具有一个阀芯，该阀芯轴向在圆柱形阀门壳体中移动，出口开口开口成为出口管线，由此具有圆柱形底部和锥形顶部的流动置换器在阀的水平处中心插入入口管线中，形成环形间隙，并且流体的横截面在出口开口处被收缩，之后立即在出口管线上放大。

45. 发明授权

US5378827A Process for the production of cellulose carbamate 失效
标题翻译：生产纤维素氨基甲酸酯的方法
公开(公告)号：US5378827A
公开(公告)日：1995-01-03
申请号：US122244
申请日：1993-09-16
申请人： Gerhard Keunecke , Adolf Arnold , Sabine Butzke
发明人： Gerhard Keunecke , Adolf Arnold , Sabine Butzke
IPC分类号： C08B15/06 , C08B5/00
CPC分类号： C08B15/06
摘要： A process for the production of cellulose carbamate from cellulose and urea through the conversion of the cellulose with excess urea in an inert liquid organic reaction carrier at a temperature in the range of 130 .degree. to 160.degree. C., separation of the reaction carrier from the reaction mixture and washing of the reaction mixture with water. The cellulose is intimately mixed with an aqueous urea solution. Then the water in the solution is replaced with the organic reaction carrier, and the reaction of urea and cellulose is carried out in the presence of an inert gaseous carrier to remove the by-product ammonia. Thereafter, the organic reaction carrier remaining in the reaction product is replaced with an aqueous urea solution and the resulting suspension of cellulose carbamate in the urea solution is filtered and washed free of urea with water. No liquid ammonia is required in this process.
摘要翻译：在惰性液体有机反应载体中，在130〜160℃的温度范围内，通过纤维素与过量尿素的转化，从纤维素和尿素生产纤维素氨基甲酸酯的方法，将反应载体与反应混合物并用水洗涤反应混合物。纤维素与尿素水溶液紧密混合。然后用有机反应载体代替溶液中的水，尿素和纤维素的反应在惰性气态载体的存在下进行以除去副产物氨。此后，将残留在反应产物中的有机反应载体用尿素水溶液代替，将所得到的尿素溶液中的氨基甲酸纤维素悬浮液过滤并用水洗涤尿素。在这个过程中不需要液氨。

46. 发明授权

US5292865A Process for preparation and after-treatment of polyester pellets 失效
标题翻译：聚酯颗粒的制备和后处理方法
公开(公告)号：US5292865A
公开(公告)日：1994-03-08
申请号：US985842
申请日：1992-12-03
申请人： Hans Kerpes , Ulrich Thiele
发明人： Hans Kerpes , Ulrich Thiele
IPC分类号： C08G63/80 , C08G63/90 , C08F6/10
CPC分类号： C08G63/90 , C08G63/80
摘要： Process for simultaneous removal of aldehyde, solid-phase postcondensation and drying of linear polyesters and copolyesters by after-treating the polyester pellets with a diffusion surface of 1.95 to 2.90 m.sup.2 /kg, an individual pellet weight of 5 to 15 mg and a bulk density of 750 to 900 kg/m.sup.3 at 140.degree. to 210.degree. C. with a flow of a dry gas mixture consisting of 60-90 vol % N.sub.2, 5-21% O.sub.2 and 0.1-25% CO.sub.2 (total 100%) at a quantity ratio of 0.5 to 2.5 kg/h gas mixture per kg/h polyester.
摘要翻译：通过用1.95〜2.90m 2 / kg的扩散表面后处理聚酯粒料，5〜15mg的单个丸粒重量和体积密度的同时去除醛，固相缩聚和干燥线性聚酯和共聚酯的方法在140至210℃下为750至900kg / m 3，在60-90vol％N 2，5-21％O 2和0.1-25％CO 2（总计100％）的干燥气体混合物流中，数量比为0.5〜2.5kg / h混合气/ kg / h聚酯。

47. 发明授权

US5194573A Discontinuous process for polycondensation of terephthalic acid and 1,4-bis(hydroxymethyl)cyclohexane 失效
标题翻译：对苯二甲酸和1,4-双（羟甲基）环己烷缩聚的不连续方法
公开(公告)号：US5194573A
公开(公告)日：1993-03-16
申请号：US853984
申请日：1992-03-20
申请人： Wolfgang Schmidt , Ulrich Thiele
发明人： Wolfgang Schmidt , Ulrich Thiele
IPC分类号： C08G63/199 , C08G63/78 , C08G63/80 , C08G63/85
CPC分类号： C08G63/78 , C08G63/85 , C08G63/199 , C08G63/80
摘要： Process for discontinuous production of polyesters by esterification of terephthalic acid with a definite excess of 1,4-bis(hydroxymethyl)cyclohexane in the presence of a titanium catalyst at 180.degree. to 300.degree. C. and 0.8 to 1.5 bar up to a conversion of 98.0% to 99.6%, then precondensation with the addition of more titanium catalyst at 270.degree. to 300.degree. C. and 500 to 5 mbar up to a conversion of 99.5% to 99.9% and polycondensation at 295.degree. to 310.degree. C. and less than 1.5 mbar up to a conversion corresponding to 40% to 95% of the maximum possible viscosity.
摘要翻译：在180℃至300℃和0.8至1.5巴的钛催化剂存在下，通过使对苯二甲酸与确定过量的1,4-双（羟甲基）环己烷酯化而不连续生产聚酯的方法，直至转化为 98.0％至99.6％，然后在270℃至300℃和500至5毫巴下加入更多的钛催化剂进行预缩合，直至99.5％至99.9％的转化率和295至310℃的缩聚度和较低的超过1.5毫巴，达到相当于最大可能粘度的40％至95％的转化率。

48. 发明授权

US4141231A Machine for applying patterns to a substrate 失效
标题翻译：用于将图案应用于基底的机器
公开(公告)号：US4141231A
公开(公告)日：1979-02-27
申请号：US709550
申请日：1976-07-28
申请人： Hans Kudlich
发明人： Hans Kudlich
IPC分类号： B05B1/30 , D06B11/00 , B05B7/00 , B05C5/00 , D06B1/02
CPC分类号： D06B11/0059 , B05B1/3053
摘要： A substrate to be patterned, such as a textile web, is moved past an array of nozzles with discharge orifices closely spaced from its surface, the substrate being firmly backed at locations confronting the nozzles by being drawn against a supporting conveyor or by being led around rollers. The nozzles are electromagnetically operated by needle valves, the valve needles being carried by membranes under substantially balanced pressures from the printing liquor and from a fluid such as compressed air. The electromagnetic coils are energized by a generator of short current pulses separated by a low holding current, the generator including two complementary power transistors in series with a coil winding. A dyestuff applicator carrying one or more of such nozzles may be transversely displaceable across the substrate, under the control of a programmer, between intermittent advances of the substrate in its longitudinal direction.
摘要翻译：要被图案化的基底，例如织物网，被移动经过具有与其表面紧密间隔开的排出孔的喷嘴阵列，衬底被牢固地支撑在与喷嘴相对的位置处，该位置被拉靠在支撑输送机上或通过被引导在周围滚筒。喷嘴由针阀电磁操作，阀针由来自印刷液体和流体（例如压缩空气）的基本平衡的压力下由膜承载。电磁线圈由短电流脉冲发生器供电，该发电机由低保持电流分开，发电机包括与线圈绕组串联的两个互补功率晶体管。承载一个或多个这样的喷嘴的染料涂布器可以在编程器的控制下横跨基板横向移动，在基板的纵向间歇进给之间。

49. 发明授权

US4119611A Process for the production of linear condensates of phenol and formaldehyde 失效
标题翻译：生产苯酚和甲醛线性缩合物的方法
公开(公告)号：US4119611A
公开(公告)日：1978-10-10
申请号：US845924
申请日：1977-10-27
申请人： Joachim Lobering
发明人： Joachim Lobering
IPC分类号： C08G8/10
CPC分类号： C08G8/10
摘要： A two-stage process for making a linear condensate of phenol and formaldehyde which can be extruded as a film or thread. In the first stage phenol and formaldehyde are reacted at about 90.degree. C to produce a clear low-viscosity phenol-methylol liquid, the pH of which is adjusted to a value greater than 3, say between 3.5 and 7. In the second stage the product of the first stage is added in aliquot portions to molten phenol having a pH of 3 or less, while maintaining the temperature at about 100.degree. C. After all the phenol-methylol has been added the mixture is slowly heated as the viscosity increases up to about 150.degree. C until there is no further increase in viscosity. The highly viscous end product can be extruded as a film or thread.
摘要翻译：用于制造苯酚和甲醛的线性缩合物的两阶段方法，其可以挤出为膜或线。在第一阶段中，苯酚和甲醛在约90℃下反应以产生澄清的低粘度苯酚 - 羟甲基液体，其pH值调节至大于3，例如3.5-7之间。在第二阶段，将第一阶段的产物以等份部分加入到pH为3或更低的熔融酚中，同时保持温度在约100℃。加入所有的酚 - 羟甲基后，随着粘度增加，将混合物缓慢加热至约150℃，直到粘度没有进一步增加。高粘度的最终产品可以挤出成膜或线。

50. 发明授权

US07241855B2 Method for the manufacture of polyesters 有权
标题翻译：制造聚酯的方法
公开(公告)号：US07241855B2
公开(公告)日：2007-07-10
申请号：US11236878
申请日：2005-09-27
申请人： Stefan Deiss , Michael Reisen , Karl-Heinz Heldmann , Eckhard Seidel
发明人： Stefan Deiss , Michael Reisen , Karl-Heinz Heldmann , Eckhard Seidel
IPC分类号： C08G63/02 , C08G63/127 , C08G63/16 , C08G63/78
CPC分类号： C08G63/81 , C08G63/181
摘要： A method is described for the manufacture of polyesters of aromatic dicarboxylic acids with aliphatic and/or cycloaliphatic dials, in which an aromatic dicarboxylic acid in the presence of a monocarboxylic acid or a mixture of a monocarboxylic acid present in a saturated solution with water or another suitable solvent is converted with an aliphatic or cycloaliphatic dial to a dicarboxylic acid alkanediolestercarboxylate and/or its oligomers, which are polycondensed in further process steps to the polyester.
摘要翻译：描述了用脂族和/或脂环族表盘制备芳族二羧酸的聚酯的方法，其中芳族二羧酸在一元羧酸或饱和溶液中存在的单羧酸与水或其它物质的混合物存在下合适的溶剂用脂族或脂环族表盘转化成二羧酸烷二醇酯羧酸酯和/或其低聚物，其在进一步的方法步骤中缩聚成聚酯。

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