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31. 发明授权

US3449080A Device for determining sodium or chloride concentration in body fluids 失效
标题翻译：用于测定体液中钠或氯的浓度的装置
公开(公告)号：US3449080A
公开(公告)日：1969-06-10
申请号：US3449080D
申请日：1964-10-29
申请人： JOHNSON & JOHNSON
发明人： EDWARDS WARREN R
IPC分类号： G01N33/487 , G01N31/04 , G01N33/16
CPC分类号： G01N33/487 , Y10T436/193333

32. 发明授权

US4532216A Use of quaternary ammonium polyelectrolyte salts in test means, test device and method for determining the ionic strength or specific gravity of a liquid sample 失效
标题翻译：在测试手段中使用季铵聚电解质盐，用于测定液体样品的离子强度或比重的测试装置和方法
公开(公告)号：US4532216A
公开(公告)日：1985-07-30
申请号：US453874
申请日：1982-12-27
申请人： Joseph Y. Wang
发明人： Joseph Y. Wang
IPC分类号： G01N9/00 , G01N27/333 , G01N31/00 , G01N31/22 , G01N33/50 , G01N33/52 , G01N9/36 , G01N31/04
CPC分类号： G01N33/52 , G01N33/50 , G01N9/00
摘要： A test means, test device, and method for determining the ionic strength or specific gravity of a test sample as well as a method for making the device, are disclosed. The test means comprises a weakly acidic polyelectrolyte polymer, at least 50 percent of the carboxyl groups of which are present in the form of the salt of a quaternary ammonium ion having the structure ##STR1## in which the R substituents, same or different, are hydrogen, lower alkyl or aryl, with the proviso that at least one of R is other than hydrogen; and an indicator means capable of producing a detectable response to ion exchange between the polyelectrolyte salt and the test sample. The device comprises a carrier matrix incorporated with the test means. The method for determining the ionic strength or specific gravity comprises contacting the test sample with the test means or device and observing a detectable response. The method for making the device comprises the steps of reacting the weakly acidic polyelectrolyte polymer with sufficient quaternary ammonium hydroxide to neutralize at least 50 percent of the carboxyl groups to form a polyelectrolyte salt, and incorporating the salt and a pH indicator with a carrier matrix.
摘要翻译：公开了用于测定试样的离子强度或比重的测试装置，测试装置和方法以及制造该装置的方法。测试装置包括弱酸性聚电解质聚合物，其中羧基的至少50％以具有结构“IMAGE”的季铵离子盐的形式存在，其中R取代基相同或不同氢，低级烷基或芳基，条件是R中的至少一个不是氢; 以及能够产生对聚电解质盐和测试样品之间的离子交换的可检测响应的指示符。该装置包括与测试装置并入的载体矩阵。用于测定离子强度或比重的方法包括使测试样品与测试装置或装置接触并观察可检测的响应。制造该器件的方法包括以下步骤：使弱酸性聚电解质聚合物与足够的氢氧化季铵反应以中和至少50％的羧基以形成聚电解质盐，并将盐和pH指示剂与载体基质结合。

33. 发明授权

US4472354A System for continuously monitoring the ionic content of steam-producing water 失效
标题翻译：用于连续监测蒸汽产生水的离子含量的系统
公开(公告)号：US4472354A
公开(公告)日：1984-09-18
申请号：US385814
申请日：1982-06-07
申请人： Thomas O. Passell , Michel N. Robles , James L. Simpson , Constantine N. Spalaris
发明人： Thomas O. Passell , Michel N. Robles , James L. Simpson , Constantine N. Spalaris
IPC分类号： G01N30/24 , G01N30/46 , G01N30/62 , G01N30/88 , G01N30/96 , G01N33/18 , G01N31/08 , G01N31/04
CPC分类号： G01N30/88 , G01N30/96 , G01N33/18 , G01N2030/626 , G01N2030/8804 , G01N2030/8886 , G01N30/24 , G01N30/466 , Y10T436/117497
摘要： An on-line and continuous sampling system for monitoring the ionic content of steam-producing water in a steam-operated electrical power plant. The monitoring system comprises a plurality of sampling lines and associated apparatus for sampling the steam-producing water at a number of different points in the power plant, an ion chromatographic subsystem for analyzing the sampled water, a calibration subsystem for calibrating the ion chromatographic subsystem, and an automatic control subsystem for operating the monitoring system of the present invention.
摘要翻译：一种在线和连续采样系统，用于监测蒸汽动力电厂中蒸汽产生水的离子含量。监测系统包括多个采样管线和相关联的装置，用于对发电厂中多个不同点的蒸汽产生水进行采样，用于分析采样水的离子色谱子系统，用于校准离子色谱子系统的校准子系统，以及用于操作本发明的监视系统的自动控制子系统。

34. 发明授权

US4403520A Control valve for a direct on-column injector and injection method 失效
标题翻译：用于直接柱上注射器和注射方法的控制阀
公开(公告)号：US4403520A
公开(公告)日：1983-09-13
申请号：US221304
申请日：1980-12-30
申请人： Giorgio Sisti , Bruno Tosi , Sorin Trestianu , Mario Galli
发明人： Giorgio Sisti , Bruno Tosi , Sorin Trestianu , Mario Galli
IPC分类号： G01N30/16 , G01N30/18 , G01N30/20 , G01N31/04
CPC分类号： G01N30/18 , G01N30/20
摘要： An apparatus for controlling the injection passage of on-column injector is disclosed. The apparatus includes a valve having at least one channel inside it and leading to the injection passage for the injection syringe needle. The channel is connected outside the injector to a source for carrier gas introduction, when the valve is open, or to the atmosphere, when the valve is closed, so as to allow a quick-type injection without the drawbacks of this injection type, as well as to have a solvent exhaust after injection.
摘要翻译：公开了一种用于控制柱上喷射器的喷射通道的装置。该装置包括阀，其内部具有至少一个通道并通向注射针头的注射通道。当阀门打开时，通道连接到喷射器外部，用于载气引入源，当阀门关闭时，通道连接到气体源，以便允许快速注射而没有这种注入类型的缺点，如以及注射后有溶剂排出。

35. 发明授权

US4314823A Combination apparatus and method for chromatographic separation and quantitative analysis of multiple ionic species 失效
标题翻译：多种离子物质色谱分离和定量分析的组合仪器和方法
公开(公告)号：US4314823A
公开(公告)日：1982-02-09
申请号：US75260
申请日：1979-09-13
申请人： William E. Rich, Jr. , Frank C. Smith , Janet L. McNeill
发明人： William E. Rich, Jr. , Frank C. Smith , Janet L. McNeill
IPC分类号： G01N30/08 , G01N30/46 , G01N30/60 , G01N30/96 , G01N31/04 , G01N31/08
CPC分类号： G01N30/461 , G01N30/08 , G01N30/96 , G01N2030/085 , G01N2030/965 , Y10T436/15 , Y10T436/25375
摘要： Apparatus and method for chromatographic separation and quantitation of different ions of like charges in a sample, e.g., cations or anions. Referring to anion separation, the sample is directed to a first chromatographic column of the ion exclusion type in which the weak acids (e.g., carboxylic acids) and their salts are partially or totally resolved and separated from a fraction of strong acids (e.g., mineral acids) due to Donnan exclusion. The resolved weak acids may be passed directly to a conductivity cell for quantitative detection. The strong acids may be directed to anion exchange bed with a highly ionized developing reagent and eluted in resolved form with the effluent being passed to a suppressor ion exchange bed wherein the developing reagent is converted to a weakly ionized form without destroying the anion separation. Then, a fraction of the strong acids is detected with the same or a different conductivity cell. Prior to separation, the strong acids are preferably directed through a concentrator column formed of ion exchange resin in which they are retained but not resolved while the remaining solution is removed. Thereafter, the developing agent used for separation of the strong anion is passed through the concentrator column to remove the anions for resolution. The same technique can be employed for cations. In an alternative mode, the system is employed to separate and quantitate weak acids but not the strong ones.
摘要翻译：用于色谱分离和定量样品（例如阳离子或阴离子）中类似电荷的不同离子的装置和方法。关于阴离子分离，样品被引导到离子排斥类型的第一色谱柱，其中弱酸（例如，羧酸）及其盐部分或完全分解并从一部分强酸分离（例如，矿物质酸）由于Donnan排除。分解的弱酸可以直接通过导电池进行定量检测。强酸可以用高度离子化的显影试剂导向阴离子交换床，并以分离形式洗脱，流出物通过抑制离子交换床，其中显影剂转化为弱离子化形式而不破坏阴离子分离。然后，用相同或不同的电导率电池检测一部分强酸。在分离之前，强酸优选通过离子交换树脂形成的浓缩塔，其中它们被保留，但是在除去剩余溶液的同时未分解。此后，用于分离强阴离子的显影剂通过浓缩塔以除去阴离子以进行分辨。阳离子也可采用相同的技术。在替代模式中，该系统用于分离和定量弱酸，而不是强酸。

36. 发明授权

US4272246A Method and apparatus for chromatographic quantitative analysis 失效
标题翻译：色谱定量分析方法和仪器
公开(公告)号：US4272246A
公开(公告)日：1981-06-09
申请号：US67855
申请日：1979-08-20
申请人： James S. Fritz , Douglas T. Gjerde , Gabriella Schmuckler
发明人： James S. Fritz , Douglas T. Gjerde , Gabriella Schmuckler
IPC分类号： G01N30/96 , G01N31/04 , G01N27/08
CPC分类号： G01N30/96 , Y10T436/173076 , Y10T436/18 , Y10T436/193333
摘要： An improved apparatus and method for the quantitative analysis of a solution containing a plurality of anion species by ion exchange chromatography which utilizes a single eluent and a single ion exchange bed which does not require periodic regeneration. The solution containing the anions is added to an anion exchange resin bed which is a low capacity macroreticular polystyrene-divinylbenzene resin containing quarternary ammonium functional groups, and is eluted therefrom with a dilute solution of a low electrical conductance organic acid salt. As each anion species is eluted from the bed, it is quantitatively sensed by conventional detection means such as a conductivity cell.
摘要翻译：一种用于通过离子交换色谱定量分析含有多种阴离子种类的溶液的改进的装置和方法，其利用单一洗脱液和不需要周期性再生的单一离子交换床。将含有阴离子的溶液加入到阴离子交换树脂床中，所述阴离子交换树脂床是含有季铵官能团的低容量大网络聚苯乙烯 - 二乙烯基苯树脂，并用低电导有机酸盐的稀溶液洗脱。由于每个阴离子物质从床上洗脱，所以通过传统的检测手段例如电导池定量地检测。

37. 发明授权

US4268269A Field test method for estimation of concentration of organic materials in water 失效
标题翻译：估算水中有机物浓度的现场试验方法
公开(公告)号：US4268269A
公开(公告)日：1981-05-19
申请号：US115518
申请日：1980-01-25
申请人： Clare B. Proudfoot
发明人： Clare B. Proudfoot
IPC分类号： B01J39/04 , C02F1/28 , G01N30/96 , G01N31/04 , G01N31/08 , G01N33/00
CPC分类号： C02F1/285 , B01J39/04 , G01N30/96 , Y10T436/147777
摘要： This invention relates to use of adsorption resins and ion exchange resins to separate selected organic materials and quantify their concentration in an aqueous solution based upon comparison to a visual standard. This process can be carried out in a relatively short time period and does not require special electronic equipment. Therefore, it can be conveniently used as a field test method to determine concentration of organic materials in aqueous solutions. This invention is especially useful in quantifying the concentration of triazoles in industrial cooling water.
摘要翻译：本发明涉及使用吸附树脂和离子交换树脂来分离所选择的有机材料并根据与视觉标准的比较来定量其在水溶液中的浓度。该过程可以在相对短的时间内进行，并且不需要特殊的电子设备。因此，它可以方便地用作现场测试方法来确定水溶液中有机材料的浓度。本发明特别可用于量化工业冷却水中三唑的浓度。

38. 发明授权

US4171341A Solid state sensor 失效
标题翻译：固态传感器
公开(公告)号：US4171341A
公开(公告)日：1979-10-16
申请号：US841285
申请日：1977-10-12
申请人： Michael J. Morgan
发明人： Michael J. Morgan
IPC分类号： G01N27/62 , G01N31/04
CPC分类号： G01N27/626
摘要： Method and apparatus for selectively sensing the presence of a given constituent within an atmosphere. The apparatus includes a solid state element containing alkali metal ions that react with ions of the given constituent when the two are brought together. The solid state element is housed within a shield that functions as an ion control screen when heated to a predetermined temperature in the presence of a gas or vapor of the given constituent to selectively pass ions of the given constituent into reactive contact with the solid state element housed therein. Circuit means are further provided for detecting a flow of ions through the shield and for producing a discernible signal in response thereto.
摘要翻译：用于选择性地感测大气中给定组分的存在的方法和装置。该装置包括含有碱金属离子的固体元素，当两者被聚集在一起时，该碱金属离子与给定成分的离子反应。固态元件容纳在屏蔽件内，当在给定组分的气体或蒸汽存在下加热至预定温度时，其用作离子控制屏，以选择性地使给定组分的离子与固体元素反应性接触容纳在其中。进一步提供电路装置，用于检测通过屏蔽的离子流，并响应于此产生可识别的信号。

39. 发明授权

US4032293A Preparation of stable strong base cellulosic anion exchangers with red-ox potentials 失效
标题翻译：稳定的强碱性红细胞阴离子交换剂的制备
公开(公告)号：US4032293A
公开(公告)日：1977-06-28
申请号：US504646
申请日：1974-09-09
申请人： Dorothy M. Perrier , Ruth R. Benerito , Richard H. Steele
发明人： Dorothy M. Perrier , Ruth R. Benerito , Richard H. Steele
IPC分类号： B01J47/00 , C08B11/145 , D06M13/08 , D06M13/10 , D06M13/46 , G01N31/04
CPC分类号： B01J47/005 , C08B11/145 , D06M13/085 , Y10S436/904 , Y10T436/25
摘要： Strong base quaternary ammonium cellulose derivatives prepared under anhydrous conditions are further chemically modified in selected organic solvents by a sequential process that produces a partial cellulose ether in fibrous form that can be used in electro-chemical reactions covering a range of oxidation-reduction potentials. These new derivatives can be prepared such that they stabilize a given anion in the cellulose matrix until such time as its oxidation or reduction power is needed in desired chemical reactions. Although prepared in nonaqueous media, these red-ox cellulosic anion exchangers can be used to regulate oxidation-reduction reactions in aqueous media. Some of these new red-ox anion exchangers are dispersible in water and can be reprecipitated by organic solvents without losing their red-ox abilities during the process. Others are water insoluble. Thus these red-ox cellulosic exchangers can be tailor made to specific end uses such as for applications in separation of biochemical or organic mixtures, the identification of reducible or oxidizable chemicals, purification of polluted liquids by oxidation or reduction of contaminants.

40. 发明授权

US4017262A Chromatographic apparatus for analysis of ionic species 失效
标题翻译：用于离子物质分析的色谱仪
公开(公告)号：US4017262A
公开(公告)日：1977-04-12
申请号：US611107
申请日：1975-09-08
申请人： Hamish Small , Timothy S. Stevens
发明人： Hamish Small , Timothy S. Stevens
IPC分类号： B01J39/26 , G01N30/40 , G01N30/46 , G01N30/52 , G01N30/60 , G01N30/96 , G01N27/08 , G01N31/04 , G01N31/08
CPC分类号： G01N30/461 , B01J39/26 , G01N30/96 , G01N2030/402 , G01N2030/525 , G01N2030/965
摘要： Apparatus and method for chromatographic quantitative analysis of a solution containing a plurality of species of cations. A sample of the solution is added to a first ion exchange resin bed containing cation exchange resin and eluted therefrom with a solution of developing reagent consisting of either AgNO.sub.3 or BaCl.sub.2, chromatographic separation of the cationic species being achieved as elution proceeds. The effluent from the first ion exchange resin bed is passed through a second ion exchange resin bed containing anion exchange resin in a form appropriate to the precipitation of whichever metal ion is provided by the developing reagent, i.e., chloride or sulfate forms. As elution proceeds the cations exit from the second ion exchange bed without destroying the ionic separation achieved in the first ion exchange resin bed. Each separated cationic species is quantitatively sensed by a detector such as a conductivity cell on exiting from the second ion exchange resin bed.
摘要翻译：用于色谱定量分析含有多种阳离子的溶液的装置和方法。将溶液样品加入到含有阳离子交换树脂的第一离子交换树脂床上，并用由AgNO 3或BaCl 2组成的显影剂的溶液洗脱，洗脱进行时实现阳离子物质的色谱分离。来自第一离子交换树脂床的流出物通过含有阴离子交换树脂的第二离子交换树脂床，其形式适于沉淀出由显影剂提供的任何金属离子，即氯化物或硫酸盐形式。随着洗脱进行，阳离子从第二离子交换床离开而不破坏在第一离子交换树脂床中实现的离子分离。每个分离的阳离子物质通过诸如从第二离子交换树脂床离开的电导率池的检测器进行定量检测。

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