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1. 发明授权

US4403520A Control valve for a direct on-column injector and injection method 失效
标题翻译：用于直接柱上注射器和注射方法的控制阀
公开(公告)号：US4403520A
公开(公告)日：1983-09-13
申请号：US221304
申请日：1980-12-30
申请人： Giorgio Sisti , Bruno Tosi , Sorin Trestianu , Mario Galli
发明人： Giorgio Sisti , Bruno Tosi , Sorin Trestianu , Mario Galli
IPC分类号： G01N30/16 , G01N30/18 , G01N30/20 , G01N31/04
CPC分类号： G01N30/18 , G01N30/20
摘要： An apparatus for controlling the injection passage of on-column injector is disclosed. The apparatus includes a valve having at least one channel inside it and leading to the injection passage for the injection syringe needle. The channel is connected outside the injector to a source for carrier gas introduction, when the valve is open, or to the atmosphere, when the valve is closed, so as to allow a quick-type injection without the drawbacks of this injection type, as well as to have a solvent exhaust after injection.
摘要翻译：公开了一种用于控制柱上喷射器的喷射通道的装置。该装置包括阀，其内部具有至少一个通道并通向注射针头的注射通道。当阀门打开时，通道连接到喷射器外部，用于载气引入源，当阀门关闭时，通道连接到气体源，以便允许快速注射而没有这种注入类型的缺点，如以及注射后有溶剂排出。

2. 发明授权

US4771628A Chamber for chromatographic analyses 失效
标题翻译：色谱分析室
公开(公告)号：US4771628A
公开(公告)日：1988-09-20
申请号：US465265
申请日：1983-02-09
申请人： Giorgio Sisti , Bruno Tosi , Giovanni Ostan , Fausto Munari , Ermete Riva , Sorin Trestianu
发明人： Giorgio Sisti , Bruno Tosi , Giovanni Ostan , Fausto Munari , Ermete Riva , Sorin Trestianu
IPC分类号： G01N30/54 , G01N30/30 , G01N30/02
CPC分类号： G01N30/30 , G01N2030/3084
摘要： This invention concerns a chamber for chromatographic analyses, in which capillary columns, in particular columns of fused silica, are thermally conditioned. The chamber comprises a thermally insulated space which can be perfectly sealed towards the outside and which houses means for heating the air and at least a fan for air circulation inside said space. In order to make the air flow going to the column(s) within the chamber as homogeneous and stable as possible from the thermal viewpoint the heating means are positioned on the suction side of the fan or of each fan, so to cause a perfect mixing of cold and hot fluid flow threads or lines in correspondence with the fan itself, and thereby obtain a uniform and stable air current from the fan towards the column.
摘要翻译：本发明涉及用于色谱分析的室，其中毛细管柱，特别是熔融二氧化硅柱是热调节的。所述腔室包括可以向外部完美密封的绝热空间，并且该室具有用于加热空气和至少一个用于在所述空间内空气循环的风扇的装置。为了使空气流从室内尽可能均匀且稳定的空气流到风扇或每个风扇的吸入侧，从而使得完全混合冷却和热流体流动线或与风扇本身对应的线，从而获得从风扇朝向柱的均匀和稳定的气流。

3. 发明授权

US4347215A Device for the automation of at least one operation in an injector for gas chromatographic columns 失效
标题翻译：用于自动化气相色谱柱注射器中至少一个操作的装置
公开(公告)号：US4347215A
公开(公告)日：1982-08-31
申请号：US222047
申请日：1981-01-02
申请人： Giorgio Sisti , Bruno Tosi , Sorin Trestianu
发明人： Giorgio Sisti , Bruno Tosi , Sorin Trestianu
IPC分类号： G01N30/16 , G01N30/24 , G01N1/14 , G01N31/08
CPC分类号： G01N30/24
摘要： A device is disclosed for coordinating the position of an injection syringe needle in a gas chromatographic apparatus with at least one other operation of the gas chromatographic apparatus downstream of the device. The device comprises a first channel for introducing the injection syringe. The first channel is substantially aligned with the injection channel of a gas chromatographic injector. The device also includes a position sensor and a lever rotatable around a lever axis substantially perpendicular to the axis of the first channel, wherein the lever has an arm and a shaped appendix, wherein the shaped appendix protrudes into the first channel when the lever is in its rest position, and wherein the appendix is positioned so that, when an injection syringe is introduced into the channel past said point, the injection syringe contacts said appendix and causes rotation of the lever about the lever axis from its rest position so that the arm acts on the position sensor to indicate detection of the presence of the injection syringe in the first channel at said point. The device further includes at least one servomechanism actuatable in response to the detection of the syringe in the channel for controlling the other operation depending on whether or not the injection syringe is detected in the channel.
摘要翻译：公开了一种用于使气相色谱仪器中的注射针头的位置与装置下游的气相色谱装置的至少另一种操作协调的装置。该装置包括用于引入注射器的第一通道。第一通道基本上与气相色谱注射器的注入通道对齐。该装置还包括位置传感器和可围绕基本上垂直于第一通道的轴线的杠杆轴线旋转的杆，其中杠杆具有臂和成形的附件，其中当杠杆处于该状态时，成形的附件突出到第一通道中其静止位置，并且其中所述附件被定位成使得当注射器被引入到通过所述点的通道中时，所述注射注射器接触所述附件并且使所述杠杆绕所述杠杆轴线从其静止位置旋转，使得所述臂作用在位置传感器上以指示在所述点处检测在第一通道中注射注射器的存在。该装置还包括至少一个伺服机构，其响应于通道中的注射器的检测而致动，用于根据在通道中是否检测到注射器来控制另一操作。

4. 发明授权

US4271695A Apparatus for feeding carrier gas to on-column injectors 失效
标题翻译：用于将载气供给柱上喷射器的装置
公开(公告)号：US4271695A
公开(公告)日：1981-06-09
申请号：US82252
申请日：1979-10-05
申请人： Giorgio Sisti , Sorin Trestianu , Mario Galli
发明人： Giorgio Sisti , Sorin Trestianu , Mario Galli
IPC分类号： G01N30/32 , G01N31/08
CPC分类号： G01N30/32
摘要： An apparatus for feeding carrier gas at a constant rate to on-column injectors for capillary and micropacked gas-chromatographic columns. The apparatus includes a constant pressure gas delivering device in operation during the sample injection, and a constant rate gas delivering device in operation during the sample processing stage inside the column. The two devices are connected in parallel and a switch controls the alternative operation of the same.
摘要翻译：用于以恒定速率将载气供给到用于毛细管和微袋气相色谱柱的柱内注射器的装置。该装置包括在样品注入期间操作的恒压气体输送装置，以及在柱内的样品处理阶段期间操作的恒定速率气体输送装置。两个设备并联连接，开关控制其替代操作。

5. 发明授权

US4269608A Method and device for sample injection under controlled conditions of temperature profile into gas chromatographic columns 失效
标题翻译：在温度分布的控制条件下将样品注入的方法和装置进入气相色谱柱
公开(公告)号：US4269608A
公开(公告)日：1981-05-26
申请号：US62927
申请日：1979-08-02
申请人： Giorgio Sisti , Sorin Trestianu , Mario Galli
发明人： Giorgio Sisti , Sorin Trestianu , Mario Galli
IPC分类号： G01N30/16 , G01N30/30
CPC分类号： G01N30/30 , G01N30/16
摘要： A method and device for sample injections into a gas chromatographic column, wherein, in order to achieve sample trapping and solvent effects, the injection zone and an initial portion of the column are kept at a low temperature and then a quick temperature change is performed at the end of said initial portion. The cooling action is preferably performed by a cooling fluid acting outside the injector and column, while said temperature change is obtained by a suitable thermoregulation of the oven wherein said gas chromatographic column is housed.
摘要翻译：一种用于样品注入气相色谱柱的方法和装置，其中为了实现样品捕获和溶剂效应，将注入区和塔的初始部分保持在低温，然后快速进行温度变化所述初始部分的结束。冷却作用优选地通过作用在喷射器和柱外部的冷却流体进行，而所述温度变化是通过适当的温度调节炉，其中容纳所述气相色谱柱。

6. 发明授权

US4383839A Method and device for vaporization injection of a liquid sample for gas chromatographic analysis 失效
标题翻译：用于气相色谱分析的液体样品的蒸发注入方法和装置
公开(公告)号：US4383839A
公开(公告)日：1983-05-17
申请号：US318907
申请日：1981-11-06
申请人： Giorgio Sisti , Mario Galli , Sorin Trestianu
发明人： Giorgio Sisti , Mario Galli , Sorin Trestianu
IPC分类号： G01N30/16 , G01N30/10 , G01N30/12 , G01N30/30 , G01N30/38 , B01D15/08
CPC分类号： G01N30/12 , G01N30/30 , G01N2030/122 , G01N2030/165 , G01N2030/167 , G01N2030/3046 , G01N2030/383 , G01N30/10
摘要： This invention relates to a method and a device for vaporization injection of a liquid sample in a gas chromatographic column housed in an oven comprising a direct on column injector suitable for injecting a liquid sample into the initial zone of a capillary column and capable of pneumatically sealing the injection port at the end of injection. Between the injector and the gas chromatographic column itself an uncoated capillary column length is provided in which vaporization of the injected sample occurs using heat from an oven housing said capillary column length, said oven being the same or separate from the oven containing said gas chromatographic column.
摘要翻译：本发明涉及一种用于在容纳在烘箱中的气相色谱柱中蒸发注入液体样品的方法和装置，该烘箱包括直接在柱式喷射器上的适用于将液体样品注入毛细管柱的初始区域并能够气动密封注射端口在注射结束时。在注射器和气相色谱柱本身之间，提供未涂布的毛细管柱长度，其中使用来自容纳所述毛细管柱长度的烘箱的加热器进行喷射样品的蒸发，所述烘箱与包含所述气相色谱柱的烘箱相同或分离。

7. 发明授权

US4405344A Method and equipment for volumetrically controlled and reproducible introduction of small amounts of liquid samples into chromatographic analysis systems 失效
标题翻译：用于体积控制和可重复地将少量液体样品引入色谱分析系统的方法和设备
公开(公告)号：US4405344A
公开(公告)日：1983-09-20
申请号：US304780
申请日：1981-09-23
申请人： Giorgio Sisti , Sorin Trestianu , Ermete Riva
发明人： Giorgio Sisti , Sorin Trestianu , Ermete Riva
IPC分类号： G01N30/16 , G01N30/91 , G01N35/10 , B01D15/08
CPC分类号： G01N30/91 , G01N30/16 , G01N2035/1041
摘要： A method and apparatus for controllably and reproducibly introducing small amounts of a liquid sample into chromatographic systems, especially high resolution gas chromatographic systems and thin-layer chromatographic systems, order to obtain sampling extremely reduced in volume and presenting maximum reliability and reproducibility, uses a sample container having a pipette-like or nozzle-like outlet neck of very small diameter. The liquid placed in the container is submitted to at least one pressure pulse which is controlled in time and/or amplitude in order to determine emission of a corresponding and controlled quantity of liquid from the outlet neck. The pressure pulse can be a pneumatic pulse directly applied to the liquid sample in the container, or a mechanical pulse applied to the liquid sample through a device acting by magnetostriction or by a piezoelectric system.
摘要翻译：一种用于可控地和可重复地将少量液体样品引入色谱系统，特别是高分辨率气相色谱系统和薄层色谱系统的方法和装置，以获得体积极小并且呈现最大可靠性和再现性的取样，使用样品容器具有非常小直径的移液管状或喷嘴状的出口颈部。放置在容器中的液体被送到至少一个在时间和/或幅度上被控制的压力脉冲，以确定从出口颈部排出相应和受控量的液体。压力脉冲可以是直接施加到容器中的液体样品的气动脉冲，或通过由磁致伸缩作用的装置或通过压电系统施加到液体样品的机械脉冲。

8. 发明授权

US4644779A Method and equipment to perform porosimetric analyses 失效
标题翻译：进行孔隙率分析的方法和设备
公开(公告)号：US4644779A
公开(公告)日：1987-02-24
申请号：US742636
申请日：1985-06-10
申请人： Giorgio Sisti , Pietro Italiano , Ermete Riva , Bruno Tosi
发明人： Giorgio Sisti , Pietro Italiano , Ermete Riva , Bruno Tosi
IPC分类号： G01N15/08
CPC分类号： G01N15/0886
摘要： A method for performing porosimetric analyses and apparatus therefor are disclosed. In particular, a method for performing porosimetric anaylses by the so-called mercury method is disclosed, wherein volumetric variations of mercury placed in a vessel are recorded. These variations are due to mercury penetration into the pores of a solid sample placed in the vessel under the mercury pressure variations. In the method disclosed, additional porosimetric information is obtained by reducing the pressure from a maximum value as a predetermined function of time. For example, the pressure reduction can be at a constant rate. Simultaneously, volume variations of the mercury exiting the sample pores are detected as the pressure decreases. This additional detection, when performed in relation to and/or in addition to the traditional measurement during pressure increase, provides a pressure/volume mercury curve which gives further data on the porosimetric characteristics of the sample, in particular related to the shape of the pores in the sample.
摘要翻译：公开了一种进行孔隙率分析的方法及其装置。特别地，公开了通过所谓的汞法进行孔隙率分析的方法，其中记录放置在容器中的汞的体积变化。这些变化是由于汞在汞压力变化下渗透到容器中的固体样品的孔中。在所公开的方法中，通过将压力从最大值减小为预定的时间函数来获得额外的孔隙度信息。例如，减压可以是恒定的速率。同时，当压力降低时，检测出离开样品孔的汞的体积变化。当在压力增加期间相对于和/或除了传统测量之外执行该附加检测时，提供压力/体积汞曲线，其进一步提供样品的孔隙度特征的数据，特别是与孔的形状有关在样品中。

9. 发明授权

US4343766A Device for sample pickup and washing 失效
标题翻译：用于取样和洗涤的设备
公开(公告)号：US4343766A
公开(公告)日：1982-08-10
申请号：US239175
申请日：1981-03-02
申请人： Giorgio Sisti , Bruno Tosi , Adriano Trisciani
发明人： Giorgio Sisti , Bruno Tosi , Adriano Trisciani
IPC分类号： G01N35/10 , G01N1/12 , G01N1/14
CPC分类号： G01N35/1004
摘要： The invention concerns a device for picking up liquid samples to be analyzed, especially in automatic samplers, said device comprising a needle connected to a sucking pump and supported by a support which moves said needle downwards to pick up the sample from a vial containing same and upwards from said vial. In order to perform a washing step after one aspiration and before the subsequent one, the needle support is designed to perform an oscillating movement when the support is in its upward position with respect to the vial. The oscillating movement is performed by the cooperation of cam means and a control rod having at least a pivot axis controlling the alternative movements. The oscillating movement makes the needle plunge into a sidewardly positioned trough containing a washing liquid.
摘要翻译：本发明涉及一种用于拾取要分析的液体样品的装置，特别是在自动采样器中，所述装置包括连接到吸泵的针并由支撑件支撑，所述支撑将所述针向下移动以从包含其的小瓶中取样，从所述小瓶向上。为了在一次抽吸之后和之后执行洗涤步骤，针支撑件被设计成当支撑件相对于小瓶处于其向上位置时执行摆动运动。振荡运动通过凸轮装置和至少具有控制替代运动的枢转轴线的控制杆的配合来执行。振荡运动使针头插入含有洗涤液体的侧面定位的槽中。

10. 发明授权

US4526686A Apparatus for chromatographic sample injection 失效
标题翻译：色谱注射装置
公开(公告)号：US4526686A
公开(公告)日：1985-07-02
申请号：US533899
申请日：1983-09-20
申请人： Giorgio Sisti , Sorin Trestiano , Ermete Riva
发明人： Giorgio Sisti , Sorin Trestiano , Ermete Riva
IPC分类号： G01N30/16 , G01N30/91 , G01N35/10 , B01D15/08
CPC分类号： G01N30/91 , G01N30/16 , G01N2035/1041
摘要： An apparatus for controllably and reproducibly introducing, small amounts of a liquid sample into chromatographic systems, especially high resolution gas chromatographic systems with cold injection, thin-layer chromatographic systems and high resolution liquid chromatographic systems, in order to obtain sampling extremely reduced in volume and presenting maximum reliability and reproducibility, uses a sample container having a pipette-like or nozzle-like outlet neck of very small diameter. The liquid placed in the container is submitted to at least one pressure pulse which is controlled in duration and/or amplitude in order to determine emission of a corresponding and controlled quantity of liquid from the outlet neck.

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