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31. 发明申请

US20080132731A1 Synthesis of Fluorinated Ethers 有权
标题翻译：氟化醚的合成
公开(公告)号：US20080132731A1
公开(公告)日：2008-06-05
申请号：US11813785
申请日：2006-01-06
申请人： Joel Swinson , Barry Jones , Danny Graham , Neville Pavri
发明人： Joel Swinson , Barry Jones , Danny Graham , Neville Pavri
IPC分类号： C07C41/22
CPC分类号： C07C43/123 , C07C41/22
摘要： A process for preparing fluorinated ethers, such as desflurane, comprises reacting the corresponding chlorinated ether, such as isoflurane, with anhydrous hydrogen fluoride in the vapor phase in the presence of chromia catalyst. It is emphasized that this abstract is provided to comply with the rules requiring an abstract which will allow a searcher or other reader quickly to ascertain the subject matter of the technical disclosure. It is submitted with the understanding that it will not be used to interpret or limit the scope or meaning of the appended issued claims.
摘要翻译：制备氟代醚的方法，如地氟烷，包括在铬酸催化剂存在下，使气相中的相应的氯化醚如异氟烷与无水氟化氢反应。要强调的是，该摘要被提供以符合要求抽象的规则，这将允许搜索者或其他读者快速地确定技术公开的主题。提交它的理解是，它不会用于解释或限制所附权利要求的范围或含义。

32. 发明申请

US20080054232A1 PREPARATION OF HIGH ASSAY DECABROMODIPHENYL OXIDE 审中-公开
标题翻译：高分析十溴烷基氧化物的制备
公开(公告)号：US20080054232A1
公开(公告)日：2008-03-06
申请号：US11843734
申请日：2007-08-23
申请人： Bonnie Gary McKinnie
发明人： Bonnie Gary McKinnie
IPC分类号： C09K21/08 , C07C25/00
CPC分类号： C07C41/22 , C07C43/29 , C08K5/06
摘要： Process technology for producing very pure reaction-derived decabromodiphenyl oxide is described. Diphenyl oxide or partially brominated diphenyl oxide or a mixture of either or both of these is fed substantially continuously over a period of about 2 to about 12 hours into a reactor containing an excess of refluxing bromine containing Lewis acid bromination catalyst, and substantially concurrently reducing the content of hydrogen bromide present in the reactor whereby a decabromodiphenyl oxide product having a purity of over 99%, preferably 99.5% or more, is formed in the reactor.
摘要翻译：描述了用于生产非常纯的反应衍生的十溴二苯醚的工艺技术。将二苯基氧化物或部分溴化二苯醚或其中的一种或两种的混合物在约2至约12小时的时间内基本上连续进料至含有过量含回流溴的路易斯酸溴化催化剂的反应器中，并且基本上同时还原存在于反应器中的溴化氢含量在反应器中形成具有超过99％，优选99.5％或更高纯度的十溴二苯醚产物。

33. 发明授权

US07297822B2 1-bromo-4-(4′-bromophenoxy)-2-pentadecyl benzene and preparation thereof 有权
标题翻译： 1-溴-4-（4'-溴苯氧基）-2-十五烷基苯及其制备
公开(公告)号：US07297822B2
公开(公告)日：2007-11-20
申请号：US11394144
申请日：2006-03-30
申请人： More Arvind Sudhakar , Wadgaonkar Prakash Purushottam
发明人： More Arvind Sudhakar , Wadgaonkar Prakash Purushottam
IPC分类号： C07C43/205 , C07C41/09
CPC分类号： C07C41/22 , C07C41/16 , C07C43/29 , C07C43/275
摘要： The present invention relates to novel brominated phenoxy compounds and to process for their preparation. More particularly, the present invention relates to synthesis of novel dibromodiphenyl ether starting from Cashew Nut Shell Liquid (CNSL);—a renewable resource material. The present invention particularly relates to novel 1-bromo-4-(4′-bromophenoxy)-2-pentadecylbenzene and to a method for it's preparation.
摘要翻译：本发明涉及新型溴化苯氧基化合物及其制备方法。更具体地说，本发明涉及从腰果壳液（CNSL）开始的新型二溴二苯醚的合成; - 可再生资源材料。本发明特别涉及新的1-溴-4-（4'-溴苯氧基）-2-十五烷基苯及其制备方法。

34. 发明申请

US20040087817A1 Method for the preparation of sevoflurane 失效
标题翻译：七氟醚的制备方法
公开(公告)号：US20040087817A1
公开(公告)日：2004-05-06
申请号：US10644500
申请日：2003-08-20
申请人： Medeva Pharmaceuticals PA, Inc.
发明人： Ross C. Terrell
IPC分类号： C07C041/00
CPC分类号： C07C41/22 , C07C43/123
摘要： A method for the preparation of sevoflurane which comprises (a) providing a liquid mixture of (CF3)2CHOCH2Cl, hydrogen fluoride, and an amine and (b) reacting the mixture, to form (CF3)2CHOCH2F.
摘要翻译：一种制备七氟醚的方法，其包括（a）提供（CF 3）2 CHOCH 2 Cl，氟化氢和胺的液体混合物，和（b）使该混合物反应以形成（CF 3）2 CHOCH 2 F。

35. 发明申请

US20040024250A1 Perfluoropolyether primary bromides and lodides 有权
标题翻译：全氟聚醚一级溴化物和卤化物
公开(公告)号：US20040024250A1
公开(公告)日：2004-02-05
申请号：US10626972
申请日：2003-07-25
发明人： Jon L. Howell , Erik W. Perez , Alfred Waterfeld , Chadron Mark Friesen , Joseph Stuart Thrasher , Ireneusz Nowak
IPC分类号： C07C051/58
CPC分类号： C07C41/14 , C07C41/18 , C07C41/22 , C07C43/126
摘要： A perfluoropolyether and a composition comprising the perfluoropolyether are provided in which the perfluoropolyether comprises at least one bromine or iodine atom at the primary position of the perfluoropolyether. Also provided is a process for producing the composition in which the process comprises contacting a perfluoropolyether acid fluoride moiety with a metal bromide or metal iodide or a suitable polyether secondary iodide under a condition sufficient to effect the production of a perfluoropolyether comprising at least one bromine or iodine at the primary position.
摘要翻译：提供全氟聚醚和包含全氟聚醚的组合物，其中全氟聚醚在全氟聚醚的主要位置包含至少一个溴或碘原子。还提供了一种制备组合物的方法，其中该方法包括使全氟聚醚酰氟部分与金属溴化物或金属碘化物或适当的聚醚二碘化物在足以产生包含至少一种溴或全氟聚醚的全氟聚醚的条件下接触碘在主要位置。

36. 发明授权

US06635760B2 Ring fluorination of non-activated aromatic compounds 失效
标题翻译：非活化芳香族化合物的环氟化
公开(公告)号：US06635760B2
公开(公告)日：2003-10-21
申请号：US10044082
申请日：2001-10-23
申请人： Ronald Eric. Banks , Mohamed Khalifa Besheesh
发明人： Ronald Eric. Banks , Mohamed Khalifa Besheesh
IPC分类号： C07D25124
CPC分类号： C07D251/28 , C07B39/00 , C07C17/12 , C07C41/22 , C07C201/12 , C07D251/24 , C07C25/13 , C07C205/12 , C07C43/225
摘要： Aromatic compounds having one or more electron-withdrawing substituents are fluorinated, preferably in a nitromethane solvent, by contact with tri(halo- or trifluoromethyl) substituted N-fluorotriazinium salts of the following Formula I: wherein three A moieties are independently CR, where each R is independently halogen or trifluoromethyl; two A moieties are independently Z, where each Z is independently nitrogen or a quaternary nitrogen atom and Y is a counterion or group of counterions which are inert to chemical attack by fluorine. Preferably the cation of the salt is 2,4,6-trichloro-1,3,5-triazinium.
摘要翻译：具有一个或多个吸电子取代基的芳族化合物优选通过与下式I的三（卤代或三氟甲基）取代的N-氟代三嗪鎓盐接触来氟化，优选在硝基甲烷溶剂中：其中三个A部分独立地为CR，其中每个 R独立地为卤素或三氟甲基; 两个A部分独立地为Z，其中每个Z独立地为氮或季氮原子，Y为对氟化学侵蚀呈惰性的抗衡离子的抗衡离子。优选的盐的阳离子是2,4,6-三氯-1,3,5-三嗪鎓。

37. 发明授权

US06596907B1 Process for the preparation of 4,4′-dihalogen-o-hydroxydiphenyl compounds 失效
标题翻译：制备4,4'-二卤代-O-羟基二苯基化合物的方法
公开(公告)号：US06596907B1
公开(公告)日：2003-07-22
申请号：US09806668
申请日：2001-04-03
申请人： Armando Di Teodoro , Werner Hölzl , Dieter Reinehr , Rudolf Zink
发明人： Armando Di Teodoro , Werner Hölzl , Dieter Reinehr , Rudolf Zink
IPC分类号： C07C4100
CPC分类号： C07C41/16 , C07C41/22 , C07C41/26 , C07C43/23 , C07C43/29 , C07C43/295
摘要： A description is given of a three-step process for the preparation of 4,4′-dihalogen-o-hydroxydiphenyl compounds of formula (1) which comprises: a) hologenating an alkoxyphenol of formula (6) (=a1), reacting the resulting halogenated phenol compound of formula (5) with p-dihalobenzene of formula (4a) in the presence of copper and/or copper salts to the diphenyl ether compound of formula (2) (=a2) and subsequent ether fission to the diphenyl ether compound of formula (1) (=a3); or b) reacting an alkoxyphenol of formula (6) with the halophenol of formula (4b) to the compound of formula (3) (=b1), then halogenating this compound (=b2) and subsequent ether fission of the resulting compound of formula (2) to the diphenyl ether compound of formula (1) (=b3). The compounds of formula (1) are used for protecting organic materials and objects against microorganisms.
摘要翻译：给出了制备式（1）的4,4'-二卤代邻羟基二苯基化合物的三步法，其包括：a）使式（6）的烷氧基酚（= a1）氢化，使得到式（5）的卤代酚化合物与式（4a）的对二卤苯在铜和/或铜盐存在下与式（2）（= a2）的二苯基醚化合物反应，随后醚裂解成二苯基醚式（1）化合物（= a3）; 或b）使式（6）的烷氧基酚与式（4b）的卤代酚反应到式（3）的化合物（= b1），然后将该化合物（= b2）卤化，随后将所得的式（2）到式（1）的二苯醚化合物（= b3）。式（1）化合物用于保护有机材料和物体免受微生物侵害。

38. 发明授权

US06528692B2 Process for producing bromo-aromatic condensed ring compound 失效
标题翻译：溴芳香稠环化合物的制备方法
公开(公告)号：US06528692B2
公开(公告)日：2003-03-04
申请号：US10021071
申请日：2001-12-19
申请人： Takahiro Ueoka , Hideyuki Ikehira
发明人： Takahiro Ueoka , Hideyuki Ikehira
IPC分类号： C07C1700
CPC分类号： C07C43/225 , C07C17/12 , C07C25/22 , C07C41/22 , C07C43/1745 , C07C2603/44 , C07C25/24 , C07C43/1747
摘要： Provided is a process for producing a bromo-aromatic condensed ring compound which comprises reacting an aromatic condensed ring compound in which the number of carbon atom constituting the aromatic condensed ring is 15 or more with a N-bromo carboxylic acid amide in the presence of a chlorinated hydrocarbon compound and sulfuric acid to brominate said aromatic condensed ring compound.
摘要翻译：本发明提供一种溴 - 芳族稠环化合物的制备方法，该方法包括使构成芳族稠合环的碳原子数为15以上的芳香族稠环化合物与N-溴羧酸酰胺在氯化烃化合物和硫酸溴化所述芳族稠环化合物。

39. 发明申请

US20030013924A1 Perfluoropolyether primary bromides and iodides 有权
公开(公告)号：US20030013924A1
公开(公告)日：2003-01-16
申请号：US10237345
申请日：2002-09-09
发明人： Jon L. Howell , Erik W. Perez , Alfred Waterfeld , Chadron Mark Friesen , Joseph Stuart Thrasher , Ireneusz Nowak
IPC分类号： C09K003/00 , C07C043/12
CPC分类号： C07C41/14 , C07C41/18 , C07C41/22 , C07C43/126
摘要： A perfluoropolyether and a composition comprising the perfluoropolyether are provided in which the perfluoropolyether comprises at least one bromine or iodine atom at the primary position of the perfluoropolyether. Also provided is a process for producing the composition in which the process comprises contacting a perfluoropolyether acid fluoride moiety with a metal bromide or metal iodide or a suitable polyether secondary iodide under a condition sufficient to effect the production of a perfluoropolyether comprising at least one bromine or iodine at the primary position.

40. 发明申请

US20020177739A1 Method for the preparation of sevoflurane 审中-公开
标题翻译：七氟醚的制备方法
公开(公告)号：US20020177739A1
公开(公告)日：2002-11-28
申请号：US10193786
申请日：2002-07-11
申请人： Medeva Pharmaceuticals PA, Inc.
发明人： Ross C. Terrell
IPC分类号： C07C043/00
CPC分类号： C07C41/22 , C07C43/123
摘要： A method for the preparation of sevoflurane which comprises (a) providing a liquid mixture of (CF3)2CHOCH2Cl, hydrogen fluoride, and an amine and (b) reacting the mixture, to form (CF3)2CHOCH2F.
摘要翻译：一种制备七氟醚的方法，其包括（a）提供（CF 3）2 CHOCH 2 Cl，氟化氢和胺的液体混合物和（b）使该混合物反应以形成（CF 3）2 CHOCH 2 F。

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