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31. 发明申请

US20100029832A1 COMPOSITES COMPRISING POLYMER AND MESOPOROUS SILICATE 审中-公开
标题翻译：包含聚合物和多孔硅酸盐的复合材料
公开(公告)号：US20100029832A1
公开(公告)日：2010-02-04
申请号：US12520960
申请日：2008-01-07
申请人： Thomas J. Pinnavaia , In Park , Siqi Xue
发明人： Thomas J. Pinnavaia , In Park , Siqi Xue
IPC分类号： C08K3/36
CPC分类号： C08K7/26 , C08K3/013 , C08K3/34 , C08K3/346 , C08K3/36
摘要： Surfactant-templated mesoporous silicates and mesoporous layered silicate clays having certain porosity parameters are used as reinforcing agents for polymers to make composites. The combination of porosity parameters that allows mesoporous silicates to be competitive with organoclays for the reinforcement of engineering polymers include an average mesopore size of at least 4 nm for surfactant-templated mesoporous silicates and least 2 nm for mesoporous layered silicate clays.
摘要翻译：具有一定孔隙率参数的表面活性剂模板的中孔硅酸盐和介孔层状硅酸盐粘土被用作制备复合材料的聚合物的增强剂。允许介孔硅酸盐与有机粘土竞争加强工程聚合物的孔隙度参数的组合包括表面活性剂模板的介孔硅酸盐的平均中孔尺寸至少为4nm，并且介孔层状硅酸盐粘土至少为2nm。

32. 发明申请

US20090123734A1 Synthetic layered silicate nanolayers 失效
标题翻译：合成层状硅酸盐纳米层
公开(公告)号：US20090123734A1
公开(公告)日：2009-05-14
申请号：US12228383
申请日：2008-08-12
申请人： Thomas J. Pinnavaia , Mihai Polverejan
发明人： Thomas J. Pinnavaia , Mihai Polverejan
IPC分类号： B32B5/16
CPC分类号： B01J39/14 , B01J20/10 , B01J20/28007 , B82Y30/00 , C02F1/42 , C02F2001/425 , Y10T428/259
摘要： Nanolayered layered silicate materials of octahedrally arranged units with divalent metal ions at centers of the units covalently linked above and below to tetrahedrally arranged oxygen and hydroxyl units with silicon atoms. The silicate materials contain silanol groups which are reactive to form derivative compositions useful for water purification to remove heavy meal cations.
摘要翻译：在上下共价连接的单元的中心具有二价金属离子的八面体排列单元的纳米级层状硅酸盐材料到具有硅原子的四面体排列的氧和羟基单元。硅酸盐材料含有硅烷醇基团，其对形成用于水净化以除去重金属阳离子的衍生物组合物具有反应性。

33. 发明授权

US07423132B2 Method for the enrichment and characterization of phosphorylated peptides or proteins 失效
标题翻译：磷酸化肽或蛋白质的富集和表征方法
公开(公告)号：US07423132B2
公开(公告)日：2008-09-09
申请号：US11147073
申请日：2005-06-07
申请人： Jetze J. Tepe , Thomas J. Pinnavaia
发明人： Jetze J. Tepe , Thomas J. Pinnavaia
IPC分类号： C07K1/14
CPC分类号： G01N33/6842 , B82Y30/00 , C07K1/22 , C07K1/36 , G01N33/543 , G01N33/6803
摘要： A method for the separation and assay of phosphorylated peptides or proteins from complex mixtures of proteins and peptides is described. The method uses a diazo moiety linked by an organic group to a substrate. Kits for performing the assay are also described. The method and kits are particularly useful for detecting changes in phosphorylates produced in living cells.
摘要翻译：描述了从蛋白质和肽的复杂混合物中分离和测定磷酸化肽或蛋白质的方法。该方法使用通过有机基团连接到底物的重氮基团。还描述了用于进行测定的试剂盒。该方法和试剂盒特别适用于检测活细胞中产生的磷酸化酶的变化。

34. 发明授权

US07067687B2 Ultrastable organofunctional microporous to mesoporous silica compositions 失效
标题翻译：超声波有机功能微孔与介孔二氧化硅组合物
公开(公告)号：US07067687B2
公开(公告)日：2006-06-27
申请号：US10795546
申请日：2004-03-08
申请人： Thomas J. Pinnavaia , Yutaka Mori
发明人： Thomas J. Pinnavaia , Yutaka Mori
IPC分类号： C07F7/04
CPC分类号： C01B37/02 , B01J29/0308 , B01J31/125 , B01J35/002 , B01J2231/32 , B01J2231/70
摘要： Mesostructured and microporous to mesoporous organofunctionalized silica compositions are described. The compositions incorporate the organofunctional group L as part of a LSiO3 unit in the framework of the compositions. In addition the compositions incorporate the organofunctional group R as part of a O3Si—R—siO3 unit in the framework of the compositions. The compositions are useful as molecular sieves, supports for catalysts and numerous other applications requiring an organo group on surfaces of a silica.
摘要翻译：描述介孔结构和微孔至介孔有机官能化二氧化硅组合物。组合物在组合物的框架中掺入有机官能团L作为LSiO 3 N 3单元的一部分。此外，组合物在组合物的框架中加入作为O 3 Si-R-SiO 3 N 3单元的一部分的有机官能团R。该组合物可用作分子筛，用于催化剂的载体和需要二氧化硅表面上的有机基团的许多其它应用。

35. 发明授权

US06261640B1 Method for the preparation of homostructured mixed proton and organic layered silicates 失效
标题翻译：均质混合质子和有机层状硅酸盐的制备方法
公开(公告)号：US06261640B1
公开(公告)日：2001-07-17
申请号：US09518355
申请日：2000-03-03
申请人： Thomas J. Pinnavaia , Zhen Wang
发明人： Thomas J. Pinnavaia , Zhen Wang
IPC分类号： B05D100
CPC分类号： C01B33/44 , B01J20/10 , C04B14/206
摘要： Homostructured, cation exchanged, layered compositions containing mixed onium and protonated hydronium ions and mixtures thereof are described. Particulate concentrates formed by intercalation of a polymer component into the galleries of the layered inorganic and organic homostructured layered cation exchange composition and to the use of the particulate concentrates for the preparation of cured polymer-inorganic nanolayer hybrid composite compositions are described. In the most preferred embodiment of the invention the layered inorganic composition is selected from the family of 2:1 layered silicate clays.
摘要翻译：描述了同构结构的，阳离子交换的，含有混合的鎓和质子化的水合氢离子的层状组合物及其混合物。描述了通过将聚合物组分嵌入到层状无机和有机均相层状阳离子交换组合物的凝结物中以及使用颗粒浓缩物制备固化的聚合物 - 无机纳米层混合复合材料组合物而形成的颗粒状浓缩物。在本发明的最优选实施方案中，层状无机组合物选自2:1层状硅酸盐粘土的族。

36. 发明授权

US6096803A Methods of preparation of organic-inorganic hybrid nanocomposites 有权
标题翻译：有机 - 无机杂化纳米复合材料的制备方法
公开(公告)号：US6096803A
公开(公告)日：2000-08-01
申请号：US136939
申请日：1998-08-20
申请人： Thomas J. Pinnavaia , Tie Lan
发明人： Thomas J. Pinnavaia , Tie Lan
IPC分类号： C08K9/08 , B32B5/16 , C08J3/34
CPC分类号： C08K9/08 , Y10T428/2991 , Y10T428/2993 , Y10T428/2998
摘要： The present invention relates to particulate concentrate compositions formed by intercalation of a polymer polymerizing component into the galleries of a layered inorganic cation exchange composition initially in proton exchanged form and to the use of the particulate concentrates for the preparation of cured polymer-inorganic nanolayer hybrid composite compositions. The polymer polymerizing component comprising the particulate concentrate contains a basic group for reaction with the protons of the inorganic cation exchanger. Also, the polymer polymerizing component contains a functional group for polymerization reaction with a polymer precursor, a mixture of polymer precursors, or a polymer melt which is introduced into the galleries of the inorganic cation exchanger and reacts with the polymer polymerizing component to form a cured polymer-inorganic nanolayer hybrid composite. In the most preferred embodiment of the invention the layered inorganic composition is selected from the family of 2:1 layered silicate cation exchangers.
摘要翻译：本发明涉及通过将聚合物聚合组分嵌入最初质子交换形式的层状无机阳离子交换组合物的凝结物中形成的颗粒状浓缩物组合物以及使用颗粒浓缩物制备固化的聚合物 - 无机纳米层混合复合材料组合物。包含颗粒浓缩物的聚合物聚合组分含有用于与无机阳离子交换剂的质子反应的碱性基团。此外，聚合物聚合组分含有用于与聚合物前体，聚合物前体的混合物或聚合物熔体的聚合反应的官能团，其被引入无机阳离子交换剂的凝结物中并与聚合物聚合组分反应以形成固化聚合物 - 无机纳米层混合复合材料。在本发明的最优选实施方案中，层状无机组合物选自2:1层状硅酸盐阳离子交换剂族。

37. 发明授权

US5800799A Porous inorganic oxide materials prepared by non-ionic surfactant and fluoride ion 失效
标题翻译：由非离子表面活性剂和氟离子制备的多孔无机氧化物材料
公开(公告)号：US5800799A
公开(公告)日：1998-09-01
申请号：US641802
申请日：1996-05-02
申请人： Thomas J. Pinnavaia , Eric P. Prouzet
发明人： Thomas J. Pinnavaia , Eric P. Prouzet
IPC分类号： C01B37/00 , C01B37/02 , C01B39/04
CPC分类号： C01B37/00 , C01B37/02
摘要： A method for the preparation of new quasi-crystalline, porous inorganic oxide compositions formed in the presence of fluoride ion possessing a disordered assembly of worm-like channels. The method uses an interaction between various nonionic polyethylene oxide based surfactants (N.degree.) and neutral inorganic oxide precursors (I.degree.) in an aqueous solution and then the formation of dispersed particles in the aqueous solution in the presence of fluoride. This (N.degree. I.degree. F.sup.-) templating approach introduces several new concepts to mesostructure synthesis. The application of the low-cost, non-toxic and biodegradable surfactants and ambient reaction temperatures, introduces environmentally clean synthetic techniques to the formation of mesostructures. Recovery of the template can be achieved through solvent extraction where the solvent may be water or ethanol.
摘要翻译：在氟离子存在下形成的具有蠕虫状通道无序组合的新型准晶体，多孔无机氧化物组合物的制备方法。该方法在水溶液中使用各种非离子聚环氧乙烷基表面活性剂（N DEG）和中性无机氧化物前体（I DEG）之间的相互作用，然后在氟化物存在下在水溶液中形成分散的颗粒。这种（N DEG I DEG F-）模板方法为介观结构合成引入了几个新概念。低成本，无毒和可生物降解的表面活性剂和环境反应温度的应用，引入了环境清洁的合成技术来形成介观结构。模板的回收可以通过溶剂萃取来实现，其中溶剂可以是水或乙醇。

38. 发明授权

US5726113A Porous clay heterostructures prepared by gallery templated synthesis 失效
标题翻译：通过画廊模板合成制备的多孔粘土异质结构
公开(公告)号：US5726113A
公开(公告)日：1998-03-10
申请号：US618317
申请日：1996-03-19
申请人： Thomas J. Pinnavaia , Anne H. Galarneau , Anis F. Barodawalla
发明人： Thomas J. Pinnavaia , Anne H. Galarneau , Anis F. Barodawalla
IPC分类号： B01J21/16 , B01J29/04 , C01B33/44
CPC分类号： B01J29/049 , B01J21/16
摘要： A porous clay heterostructure of a 2:1 layered silicate prepared by a gallery templated synthesis method is described. The method uses an inorganic oxide, a neutral amine surfactant and a quaternary onium ion surfactant in the galleries of the 2:1 layered silicate. The structure is then calcined to remove the surfactants which act as a template to produce the porous clay heterostructure. The structure is useful for cracking catalysts, molecular sieves and adsorbents.
摘要翻译：描述了通过画廊模板合成方法制备的2:1层状硅酸盐的多孔粘土异质结构。该方法在2:1层状硅酸盐的画廊中使用无机氧化物，中性胺表面活性剂和季铵离子表面活性剂。然后将该结构物煅烧以除去用作模板以产生多孔粘土异质结构的表面活性剂。该结构可用于裂化催化剂，分子筛和吸附剂。

39. 发明授权

US5116587A Layered double hydroxide sorbents for the removal of SO.sub.x from flue gas resulting from coal combustion 失效
标题翻译：用于从煤炭燃烧中排出的烟气中去除SOX的层状双氢氧化物分子
公开(公告)号：US5116587A
公开(公告)日：1992-05-26
申请号：US466984
申请日：1990-01-18
申请人： Thomas J. Pinnavaia , Jayantha Amarasekera , Christine A. Polansky
发明人： Thomas J. Pinnavaia , Jayantha Amarasekera , Christine A. Polansky
IPC分类号： B01D53/02 , B01D53/50 , B01J20/06 , B01J20/08 , B01J20/28 , C01F7/00 , C01G1/00 , C01G49/00
CPC分类号： B01D53/508 , B01J20/06 , C01F7/002 , C01G1/00 , C01G49/009 , C01P2002/22 , C01P2002/78
摘要： Processes for removing noxious oxides from gas streams, particularly from flue gases of coal-burning power plants, using heated layered double hydroxide (LDH) sorbents are described. The sorbent compositions contain metal components, incorporated into the sorbents either by isomorphous replacement of all or part of M.sup.II and /or M.sup.III ions in layers of LDH structures or by impregnation as a metal salt, to promote the oxidation of sulfur dioxide.
摘要翻译：描述了使用加热的层状双氢氧化物（LDH）吸附剂从燃气流，特别是燃煤发电厂的烟道气中除去有害氧化物的方法。吸附剂组合物含有金属组分，其通过在LDH结构层中的全部或部分MII和/或MIII离子的同晶取代或通过浸渍作为金属盐同时置换到吸附剂中，以促进二氧化硫的氧化。

40. 发明授权

US4629712A Delaminated clay materials 失效
标题翻译：分层粘土材料
公开(公告)号：US4629712A
公开(公告)日：1986-12-16
申请号：US641912
申请日：1984-08-17
申请人： Thomas J. Pinnavaia , Rasik H. Raythatha
发明人： Thomas J. Pinnavaia , Rasik H. Raythatha
IPC分类号： B01J21/16 , B01J23/26 , B01J29/04
CPC分类号： B01J29/049 , B01J21/16 , B01J23/26
摘要： Delaminated trioctahedral smectite clay compositions are provided having a substantially delaminated interlayer structure with a face-to-edge and edge-to-edge association of the clay layers and an inorganic metal oxide intercalated between the clay layers. A process for preparing delaminated smectite clay compositions comprises reacting an admixture of a trioctahedral smectite clay having an average particle size up to about 500 angstroms and a polymeric cationic hydroxy metal complex in an aqueous medium and recovering the reacted clay solids.
摘要翻译：提供分层的三八面体绿土粘土组合物，其具有基本上分层的层间结构，其中粘土层与粘土层之间插入的无机金属氧化物具有面对边和边缘到边缘的关联。一种制备分层蒙脱石粘土组合物的方法包括使平均粒径达500埃的三八面体绿土粘土和聚合物阳离子羟基金属络合物在水性介质中的混合物反应并回收反应的粘土固体。

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