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31. 发明申请

US20120091394A1 BLUE LIGHT EMITTING GLASS AND PREPARATION METHOD THEREOF 有权
标题翻译：蓝光发光玻璃及其制备方法
公开(公告)号：US20120091394A1
公开(公告)日：2012-04-19
申请号：US13377569
申请日：2009-06-25
申请人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi
发明人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi
IPC分类号： C09K11/79 , C03B32/00
CPC分类号： C03C3/095 , C03B32/00 , C03C3/062 , C03C4/12 , C09K11/7721
摘要： Blue light emitting glass and the preparation method thereof are provided. The blue light emitting glass has the following composition: aCaO.bAl2O3.cSiO2.xCeO2, wherein a, b, c and x are, by mol part, 15-55, 15-35, 20-60 and 0.01-5 respectively. The preparation method comprises: weighing the raw materials according to the composition of the blue light emitting glass; mixing the raw materials uniformly and melting the raw materials to obtain glass melt; moulding the glass melt to obtain transparent glass; thermally treating the transparent glass under reducing atmosphere, and thereafter obtaining the finished product. The blue light emitting glass obtained has intense broadband excitation spectrum in ultraviolet region and emits intense blue light under the excitation of ultraviolet light. It is suitable for using as luminescent medium material.
摘要翻译：提供蓝色发光玻璃及其制备方法。蓝色发光玻璃具有以下组成：aCaO.bAl2O3.cSiO2.xCeO2，其中a，b，c和x分别为15-55,15-35,20-60和0.01-5。制备方法包括：根据蓝色发光玻璃的成分称量原料; 均匀混合原料，熔化原料，得到玻璃熔体; 将玻璃熔体成型得到透明玻璃; 在还原气氛下对透明玻璃进行热处理，然后得到成品。获得的蓝色发光玻璃在紫外线区域具有强烈的宽带激发光谱，并在紫外光的激发下发出强烈的蓝光。适合用作发光介质材料。

32. 发明申请

US20120061615A1 Rare Earth Ion Doped Silicate Luminescence Glass and Preparation Method Thereof 有权
标题翻译：稀土离子掺杂硅酸盐发光玻璃及其制备方法
公开(公告)号：US20120061615A1
公开(公告)日：2012-03-15
申请号：US13320753
申请日：2009-05-19
申请人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi , Yanbo Qiao , Qingtao Li
发明人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi , Yanbo Qiao , Qingtao Li
IPC分类号： C09K11/79
CPC分类号： C03C4/12 , C03C3/062 , C03C3/095
摘要： A rare earth ion doped silicate luminescence glass and preparation method thereof are provided. The luminescence glass is the material with the following formula: aM2O.bM′2O3.cSiO2.dRE2O3, wherein M is at least one of Na, K and Li, M′ is at least one of Y, Gd, La, Sc and Lu, RE is at least one of Ce, Tm, Tb, Ho, Dy, Er, Nd, Sm, Eu and Pr. The preparation method is: grinding the raw material until mixed uniformly, calcining the raw material at 1200-1500° C. for 1-5 h, cooling to room temperature, annealing at 600-1100° C. for 0.5-24 h, cooling to room temperature again, molding then getting the product. The performance of the product is stable. The product is homogenous, and the luminescence performance is good. The light transmittance is high. The process of the preparation method is simple and with low cost.
摘要翻译：提供了一种稀土离子掺杂硅酸盐发光玻璃及其制备方法。发光玻璃是具有下式的材料：aM2O.bM'2O3.cSiO2.dRE2O3，其中M是Na，K和Li中的至少一种，M'是Y，Gd，La，Sc和Lu中的至少一种，RE为Ce，Tm，Tb，Ho，Dy，Er，Nd，Sm，Eu和Pr中的至少一种。制备方法为：研磨原料直至混合均匀，在1200-1500℃下煅烧原料1-5小时，冷却至室温，在600-1100℃退火0.5-24小时，冷却再到室温，成型然后得到产品。产品性能稳定。产品均匀，发光性能好。透光率高。制备方法简单，成本低。

33. 发明授权

US09000667B2 Luminescent element, preparation method thereof and luminescence method 有权
标题翻译：发光元件及其制备方法和发光方法
公开(公告)号：US09000667B2
公开(公告)日：2015-04-07
申请号：US13392495
申请日：2009-08-26
申请人： Mingjie Zhou , Wenbo Ma , Yugang Liu , Qingtao Li , Jing Tang , Xi Luo
发明人： Mingjie Zhou , Wenbo Ma , Yugang Liu , Qingtao Li , Jing Tang , Xi Luo
IPC分类号： H01J23/24 , C03C17/09 , C03C3/068 , C03C3/15 , C03C4/12 , H01J63/04 , H01J63/06 , H01J29/20 , H01J29/28 , C09K11/77
CPC分类号： C03C17/09 , C03C3/068 , C03C3/15 , C03C4/12 , C03C2217/252 , C03C2217/254 , C03C2217/255 , C03C2217/256 , C03C2217/261 , C03C2217/268 , C03C2217/27 , C03C2218/15 , C03C2218/32 , C09K11/778 , H01J29/20 , H01J29/28 , H01J63/04 , H01J63/06 , H01J2329/28 , Y10T428/24355
摘要： A luminescent element includes a luminescent glass and a metal layer with a metal microstructure formed on a surface of the luminescent glass; wherein the luminescent glass has a chemical composition: bY2O3.cAl2O3.dB2O3.yTb2O3, wherein bY2O3.cAl2O3.dB2O3.yTb2O3. A preparation method of a luminescent element and a luminescence method are also provided. The luminescent element has good luminescence homogeneity, high luminescence efficiency, good luminescence stability and simple structure, and can be used in luminescent device with ultrahigh brightness.
摘要翻译：发光元件包括发光玻璃和在发光玻璃的表面上形成有金属微结构的金属层; 其中发光玻璃具有化学组成：bY2O3.cAl2O3.dB2O3.yTb2O3，其中bY2O3.cAl2O3.dB2O3.yTb2O3。还提供了发光元件的制备方法和发光方法。发光元件具有良好的发光均匀性，发光效率高，发光稳定性好，结构简单，可用于超高亮度发光装置。

34. 发明授权

US08562866B2 Preparation method of zinc manganese silicate 有权
标题翻译：锌硅酸锌的制备方法
公开(公告)号：US08562866B2
公开(公告)日：2013-10-22
申请号：US13640353
申请日：2010-04-27
申请人： Mingjie Zhou , Shuxin Lu , Wenbo Ma
发明人： Mingjie Zhou , Shuxin Lu , Wenbo Ma
IPC分类号： C09K11/70
CPC分类号： C09K11/595
摘要： A preparation method of zinc manganese silicate is provided. The method includes the following steps: step 1, preparing silicon dioxide sol with distilled water, anhydrous ethanol and tetraethyl orthosilicate; step 2, preparing a mixture solution of a zinc salt and a manganese salt; step 3, adjusting the silicon dioxide sol to be neutral or acidic; step 4, adding the mixture solution of the zinc salt and the manganese salt into the silicon dioxide sol to form a gelatin; step 5, drying the gelatin, keeping the temperature, grinding, reducing with keeping the temperature in a reductive atmosphere to obtain zinc manganese silicate. The preparation method has simple technique and low equipment requirement. The particles of the zinc manganese silicate phosphor prepared by the method have a regular size, uniform shape and good luminescent performance.
摘要翻译：提供了一种硅酸锌的制备方法。该方法包括以下步骤：步骤1，用蒸馏水，无水乙醇和原硅酸四乙酯制备二氧化硅溶胶; 步骤2，制备锌盐和锰盐的混合溶液; 步骤3，调节二氧化硅溶胶为中性或酸性; 步骤4，将锌盐和锰盐的混合溶液加入到二氧化硅溶胶中以形成明胶; 步骤5，干燥明胶，保持温度，研磨，还原，保持温度在还原气氛中，得到硅酸锌锰。制备方法技术简单，设备要求低。通过该方法制备的硅酸锌锰粉末的颗粒具有规则的尺寸，均匀的形状和良好的发光性能。

35. 发明申请

US20130240785A1 HALO-BORATE LUMINESCENT MATERIALS AND PREPARATION METHODS THEREOF 有权
标题翻译：低硼酸盐光致发光材料及其制备方法
公开(公告)号：US20130240785A1
公开(公告)日：2013-09-19
申请号：US13885275
申请日：2010-12-14
申请人： Mingjie Zhou , Qiurong Liao , Wenbo Ma
发明人： Mingjie Zhou , Qiurong Liao , Wenbo Ma
IPC分类号： C09K11/87 , C09K11/77
CPC分类号： C09K11/87 , C09K11/774
摘要： Halo-borate luminescent materials and preparation methods thereof are provided. The said luminescent materials are represented by the following general formula: Ca2-xBO3Cl1-yFy:xEu2+, zM0, wherein M0 is selected from one of Ag, Au, Pt, Pd or Cu metal nano-particles; 0.001≦x≦0.1, 0≦y≦0.2, 0≦z≦0.01. The said luminescent materials have excellent chemical stability and high luminous intensity. The said preparation methods have simple technique, no pollution, manageable process conditions and low equipment requirement, and are beneficial to industry production.
摘要翻译：提供卤硼酸盐发光材料及其制备方法。所述发光材料由以下通式表示：Ca2-xBO3Cl1-yFy：xEu2 +，zM0，其中M0选自Ag，Au，Pt，Pd或Cu金属纳米颗粒之一; 0.001 @ x @ 0.1,0 @ y @ 0.2,0 @ z @ 0.01。所述发光材料具有优异的化学稳定性和高发光强度。所述制备方法技术简单，无污染，工艺条件可控，设备要求低，有利于工业生产。

36. 发明申请

US20130214206A1 TUNGSTATE FLUORESCENT MATERIALS AND PREPARATION METHODS THEREOF 有权
标题翻译：黄铁矿荧光材料及其制备方法
公开(公告)号：US20130214206A1
公开(公告)日：2013-08-22
申请号：US13881683
申请日：2010-12-14
申请人： Mingjie Zhou , Jun Liu , Wenbo Ma
发明人： Mingjie Zhou , Jun Liu , Wenbo Ma
IPC分类号： C09K11/87 , C09K11/68
CPC分类号： C09K11/87 , C09K11/025 , C09K11/58 , C09K11/68 , C09K11/684 , C09K11/873
摘要： Tungstate luminescent materials and preparation methods thereof are provided. The said luminescent materials are represented by the following general formula: RWO4:xM, wherein R is selected from one or two of Ca, Sr or Ba, M is selected from one or two of Ag, Au, Pt or Pd metal nano-particles; 0
摘要翻译：提供了钨酸盐发光材料及其制备方法。所述发光材料由以下通式表示：RWO4：xM，其中R选自Ca，Sr或Ba中的一种或两种，M选自Ag，Au，Pt或Pd金属纳米颗粒中的一种或两种 ; 0

37. 发明申请

US20130169143A1 FIELD EMISSION LIGHT SOURCE DEVICE AND MANUFACTURING METHOD THEREOF 有权
标题翻译：场发射光源装置及其制造方法
公开(公告)号：US20130169143A1
公开(公告)日：2013-07-04
申请号：US13821512
申请日：2010-09-20
申请人： Mingjie Zhou , Wenbo Ma , Qingtao Li
发明人： Mingjie Zhou , Wenbo Ma , Qingtao Li
IPC分类号： H01J1/90 , H01J9/38
CPC分类号： H01J1/90 , H01J9/24 , H01J9/38 , H01J61/30 , H01J63/02 , H01J63/06
摘要： A field emission light source device, comprising: cathode plate comprising substrate and cathode conductive layer disposed on surface of substrate, and anode plate comprising base formed from transparent ceramic material and anode conductive layer disposed on one surface of base, and insulating support member by which cathode plate and anode plate are integrally fixed, and vacuum-tight chamber formed with anode plate, cathode plate and insulating support member; anode conductive layer and the cathode plate are disposed opposite each other. Because of advantages of good electrical conductivity, high light transmittance, stable electron-impact resistance performance and uniform luminescence, using transparent ceramic as the base of the anode plate in the field emission light source device can increase electron beam excitation efficiency effectively, increase light extraction efficiency of the field emission light source device, and finally increase its luminous efficiency. A manufacturing method of the field emission light source device is also provided.
摘要翻译：一种场发射光源装置，包括：阴极板，包括设置在基板表面上的基板和阴极导电层，以及阳极板，其包括由透明陶瓷材料形成的基底和设置在基底的一个表面上的阳极导电层，以及绝缘支撑构件，阴极板和阳极板一体固定，真空室形成阳极板，阴极板和绝缘支撑构件; 阳极导电层和阴极板彼此相对设置。由于导电性好，透光率高，电子撞击性能稳定，发光均匀，采用透明陶瓷作为场致发射光源装置的阳极板底座，可有效提高电子束激发效率，增加光提取场发射光源器件的效率，最终提高其发光效率。还提供了场发射光源装置的制造方法。

38. 发明授权

US08446088B2 Field emission device for emitting white light 有权
标题翻译：用于发射白光的场发射装置
公开(公告)号：US08446088B2
公开(公告)日：2013-05-21
申请号：US13514951
申请日：2009-12-29
申请人： Mingjie Zhou , Wenbo Ma
发明人： Mingjie Zhou , Wenbo Ma
IPC分类号： H01J63/06
CPC分类号： H01J63/06 , C09K11/0883 , C09K11/565 , C09K11/584 , C09K11/7702 , C09K11/7718 , C09K11/7734 , C09K11/7771 , C09K11/7774 , H01J29/20 , H01J63/04 , Y02B20/181
摘要： A field emission device for emitting white light is provided. The device includes a cathode plate assembly (1), an anode plate assembly (2) which is opposite to and spaced from the cathode plate assembly (1), and a supporting body (3) for tight coupling the cathode plate assembly (1) with the anode plate assembly (2). The anode plate assembly (2) includes a transparent substrate (203) which can emit yellow light when excited by blue light. An anode (202) and a blue cathode ray luminescent material layer (201) are provided on the surface of the transparent substrate (203). The blue cathode ray luminescent material layer (201) contains blue cathode ray luminescent material.
摘要翻译：提供了用于发射白光的场发射装置。该装置包括阴极板组件（1），与阴极板组件（1）相对并间隔开的阳极板组件（2）和用于紧密耦合阴极板组件（1）的支撑体（3）与阳极板组件（2）。阳极板组件（2）包括透明基板（203），当由蓝光激发时可以发出黄光。在透明基板（203）的表面上设置阳极（202）和蓝色阴极射线发光材料层（201）。蓝色阴极射线发光材料层（201）含有蓝色阴极射线发光材料。

39. 发明申请

US20130112919A1 White Light Emitting Glass-Ceramic and Production Method Thereof 有权
标题翻译：白光发射玻璃陶瓷及其制作方法
公开(公告)号：US20130112919A1
公开(公告)日：2013-05-09
申请号：US13809679
申请日：2010-07-22
申请人： Mingjie Zhou , Wenbo Ma , Fangyi Weng
发明人： Mingjie Zhou , Wenbo Ma , Fangyi Weng
IPC分类号： C09K11/77
CPC分类号： C09K11/7774 , C03B32/00 , C03B32/02 , C03C3/112 , C03C4/12 , C03C10/0009 , C03C10/16 , C09K11/7766 , H01L33/502 , Y02B20/181
摘要： A white light emitting glass-ceramic. The chemical formula of the glass-ceramic is aSiO2.bAl2O3.cNaF.dCeF3.nDyF3.mAg, wherein a, b, c, d, n and m are, by mol part, 25-50, 15-30, 10-30, 10-25, 0.01-1 and 0.01-1, respectively, and a+b+c+d-100. A method for producing said glass-ceramic is also provided. Silver ion is doped in the glass-ceramic in the form of silver particles by means of sintering and reduction annealing treatment, and thus the luminescence properties of rare earth ion is improved.
摘要翻译：白色发光玻璃陶瓷。玻璃陶瓷的化学式为SiO2.bAl2O3.cNaF.dCeF3.nDyF3.mAg，其中a，b，c，d，n和m分别为25-50,15-30,10-30 ，10-25,0.01-1和0.01-1，a + b + c + d-100。还提供了制造所述玻璃 - 陶瓷的方法。通过烧结和还原退火处理将银离子以银颗粒的形式掺杂在玻璃陶瓷中，从而提高稀土离子的发光性能。

40. 发明申请

US20130112654A1 PREPARATION METHOD OF FLUORESCENT POWDER LAYER 有权
标题翻译：荧光粉层的制备方法
公开(公告)号：US20130112654A1
公开(公告)日：2013-05-09
申请号：US13810058
申请日：2010-07-14
申请人： Mingjie Zhou , Wenbo Ma , Yugang Liu
发明人： Mingjie Zhou , Wenbo Ma , Yugang Liu
IPC分类号： C23F13/02 , B29D11/00
CPC分类号： H05B33/14 , H01L33/501 , H01L33/505 , H01L2933/0041 , H05B33/10
摘要： A preparation method of the fluorescent powder layer (108, 208) is provided. The said preparation method is carried out as following steps: step 1, a fluorescent powder layer (102, 202) is coated on one surface of a flat transparent substrate (101, 201); step 2, the surface of a board (103, 203) is shaped into a curved surface (104, 204); step 3, the board (103, 203) of step 2 is arranged on the substrate (101, 201) coated with the fluorescent powder layer (102, 202) of step 1; the curved surface (104, 204) of the board (103, 203) faces the substrate (101, 201), and the fluorescent powder layer (102, 202) is sandwiched between the substrate (101, 201) and the board (103, 203); step 4, the substrate (101, 201) is softened by heating, a pressure is then applied to the board (103, 203) so that the fluorescent powder layer (102, 202) sandwiched between the substrate (101, 201) and the board (103, 203) forms the fluorescent powder layer (108, 208) having the same curved shape as the curved surface (104, 204) of the board (103, 203) by the pressure, and the fluorescent powder layer (108, 208) on the substrate (101, 201) is completed after cooling.
摘要翻译：提供了荧光粉层（108,208）的制备方法。所述制备方法如下步骤：步骤1，在平坦的透明基材（101,201）的一个表面上涂布荧光粉末层（102,202）; 步骤2，将板（103,203）的表面成形为弯曲表面（104,204）; 步骤3，步骤2的板（103,203）布置在涂覆有步骤1的荧光粉层（102,202）的基板（101,201）上; 基板（103,203）的曲面（104,204）面向基板（101,201），荧光粉层（102,202）夹在基板（101,201）和基板（103）之间，203）; 步骤4，通过加热软化基板（101,201），然后将压力施加到基板（103,203），使得夹在基板（101,201）和基板（101,201）之间的荧光粉末层（102,202）板（103,203）通过压力形成具有与板（103,203）的弯曲表面（104,204）相同的弯曲形状的荧光粉末层（108,208），荧光粉末层（108,208） 208）在冷却后完成。

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