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31. 发明授权

US07328733B2 Inner tube compositions having improved heat resistance characteristics 失效
标题翻译：具有改善的耐热特性的内管组合物
公开(公告)号：US07328733B2
公开(公告)日：2008-02-12
申请号：US10635382
申请日：2003-08-06
申请人： Donald Sheley Tracey , Ilan Duvdevani , Hsien-Chang Wang
发明人： Donald Sheley Tracey , Ilan Duvdevani , Hsien-Chang Wang
IPC分类号： B60C5/02
CPC分类号： C08L23/16 , B60C1/00 , B60C1/0008 , B60C5/02 , C08L21/00 , C08L23/22 , C08L23/283 , C08L2312/00 , C08L2666/04 , C08L2666/06
摘要： Halogenated isobutylene-co-alkylstyrene polymer, preferably halogenated isobutylene-co-methylstyrene polymer, even more preferably brominated isobutylene-co-paramethylstyrene polymer (BIMS), blends thereof, and blends with a second rubber, show improved heat resistance compared to butyl inner tube compositions, and retain the superior barrier properties of butyl inner tube compositions versus inner tube compositions with butyl/EP blends.
摘要翻译：卤代异丁烯 - 共 - 烷基苯乙烯聚合物，优选卤代异丁烯 - 共 - 甲基苯乙烯聚合物，甚至更优选溴化异丁烯 - 共 - 对甲基苯乙烯聚合物（BIMS），其共混物和与第二橡胶的共混物与丁基内管相比显示改进的耐热性并且保持丁基内管组合物与丁基/ EP共混物的内管组合物的优异的阻隔性能。

32. 发明授权

US06907911B2 Thermoplastic blend 有权
公开(公告)号：US06907911B2
公开(公告)日：2005-06-21
申请号：US10879820
申请日：2004-06-29
申请人： Hsien-Chang Wang
发明人： Hsien-Chang Wang
IPC分类号： B60C5/14 , B29D30/00 , C08J5/18 , C08L9/00 , C08L23/22 , C08L23/28 , C08L25/06 , C08L25/18 , C08L29/04 , C08L67/00 , C08L69/00 , C08L71/02 , C08L71/12 , C08L77/00 , C08L77/02 , C08L77/06 , C08L81/06 , C08L101/00
CPC分类号： C08L77/06 , C08L9/00 , C08L23/22 , C08L23/283 , C08L25/06 , C08L25/18 , C08L29/04 , C08L67/00 , C08L69/00 , C08L71/02 , C08L71/123 , C08L77/00 , C08L77/02 , C08L81/06 , C08L101/00 , Y10T152/10 , Y10T152/10495 , Y10T152/10855 , C08L2666/20 , C08L2666/02 , C08L2666/04 , C08L2666/14 , C08L2666/08 , C08L25/00
摘要： The invention generally relates to thermoplastic blends having improved properties. Optionally, these blends may be dynamically vulcanized. More specifically, this invention is directed to a composition comprising a blend of chloromethylated(styrene-isobutylene) polymer and a thermoplastic resin selected from the group consisting of polyamides, polyesters, polycarbonates, polysulfones, polyacetals, polyacetones, acrylonitrile-butadiene styrene resins, polyphenylene oxide, polyphenylene sulfide, styrene-acrylonitrile resins, styrene-maleic anhydride resins, polyamides, aromatic polyketones, ethylene vinyl alcohol polymer and mixtures thereof. Tires and tire components such as air permeation prevention films comprising these compositions are also provided.

33. 发明授权

US06875813B2 Isobutylene-based elastomer blends 失效
标题翻译：异丁烯基弹性体共混物
公开(公告)号：US06875813B2
公开(公告)日：2005-04-05
申请号：US10258008
申请日：2001-04-26
申请人： Andy H. Tsou , Ilan Duvdevani , Hsien-Chang Wang
发明人： Andy H. Tsou , Ilan Duvdevani , Hsien-Chang Wang
IPC分类号： C08L23/08 , C08L23/22 , C08F8/00 , C08L9/00 , C08L23/04 , C08L27/06 , C08L45/00
CPC分类号： C08L23/0815 , C08L23/22 , C08L2666/06
摘要： The improved green strength, green elongation, and green relaxation properties of isobutylene-based elastomers at elevated temperatures along with improved aging and barrier properties are achieved by blending semi-compatible, semi-crystalline copolymers with the isobutylene elastomers. The semi-crystalline copolymers are typically copolymers of ethylene and an alpha-olefin having from 4 to 16 carbon atoms. The improved properties are maintained in subsequent rubber compounds containing said blends and are particularly useful in tire and pharmaceutical container applications.
摘要翻译：通过将半相容的半结晶共聚物与异丁烯弹性体共混，可以提高异丁烯基弹性体在升高的温度下改善的生坯强度，绿色伸长率和绿色松弛性能以及改善的老化和阻隔性能。半结晶共聚物通常是乙烯和具有4至16个碳原子的α-烯烃的共聚物。在随后的包含所述共混物的橡胶化合物中维持改进的性能，并且在轮胎和药物容器应用中特别有用。

34. 发明授权

US06300431B1 Phase transfer process with catalyst recovery 失效
标题翻译：催化剂回收相转移过程
公开(公告)号：US06300431B1
公开(公告)日：2001-10-09
申请号：US09466520
申请日：1999-12-17
申请人： Hsien-Chang Wang , Chia Shian Chee , W. S. Winston Ho
发明人： Hsien-Chang Wang , Chia Shian Chee , W. S. Winston Ho
IPC分类号： C08F208
CPC分类号： B01D61/362 , B01J14/00 , B01J19/2475
摘要： A process for catalytic recovery in a phase transfer process wherein heterogeneous reactions in a liquid-liquid two phase reaction systems using a phase transfer catalyst is improved by separating the two liquid phases with a membrane which retains the catalyst while passing the aqueous polar liquid thereby allowing easy recovery of the phase transfer catalyst. The reaction is carried out between reactants selectively soluble in the different phases, one of the reactants being transferred into the other phase by means of a phase transfer catalyst which is soluble in said polar liquid phase with the one reactant. The phases are separated after completion of the reactions by adding water to the two-phase reaction system to dissolve out the polar liquid phase containing the phase transfer catalyst into an aqueous phase. Further, the phase transfer catalyst is separated from the polar liquid phase by passing the aqueous polar liquid phase through a membrane that retains the transfer catalyst while passing the polar liquid.
摘要翻译：在相转移过程中催化回收的方法，其中使用相转移催化剂的液 - 液两相反应体系中的非均相反应通过用保留催化剂的膜分离两个液相而改善，所述膜通过极性极性液体从而允许容易回收相转移催化剂。该反应在选择性溶于不同相的反应物之间进行，其中一种反应物通过相转移催化剂转移到另一相中，所述相转移催化剂可溶于所述极性液相中的一种反应物。通过向两相反应体系中加入水以将含有相转移催化剂的极性液相溶出到水相中，在反应完成后分离各相。此外，通过使极性液相通过保持转移催化剂的膜，同时通过极性液体，将相转移催化剂与极性液相分离。

35. 发明授权

US6140424A Multiple component thermoplastic elastomer compositions 有权
标题翻译：多组分热塑性弹性体组合物
公开(公告)号：US6140424A
公开(公告)日：2000-10-31
申请号：US280802
申请日：1999-03-26
申请人： Raman Patel , Sabet Abdou-Sabet , Hsien-Chang Wang
发明人： Raman Patel , Sabet Abdou-Sabet , Hsien-Chang Wang
IPC分类号： C08L9/02 , C08L21/00 , C08L23/00 , C08L23/02 , C08L23/04 , C08L23/08 , C08L23/10 , C08L23/12 , C08L23/16 , C08L23/20 , C08L23/22 , C08L23/28 , C08L33/08 , C08L67/00 , C08L67/02 , C08L71/00 , C08L71/10 , C08L71/12 , C08L77/00 , C08L77/02 , C08L77/06 , C08L33/18
CPC分类号： C08L77/02 , C08L21/00 , C08L23/02 , C08L23/08 , C08L23/10 , C08L23/12 , C08L23/16 , C08L23/22 , C08L23/283 , C08L67/02 , C08L77/00 , C08L77/06 , C08L9/02 , C08L2205/02 , C08L2205/035 , C08L23/04 , C08L23/20 , C08L2312/04
摘要： Thermoplastic elastomer compositions which have good high temperature end use and good oil swell resistance are made by blending a high melting thermoplastic polymer containing a non-polar rubber and a polar rubber. Alternatively, a high melting thermoplastic polymer containing a non-polar rubber or a polar rubber or both is blended with a polyolefin thermoplastic polymer containing a non-polar rubber, or a polar rubber, or both. The composition is dynamically vulcanized. The cured multi-component thermoplastic elastomer compositions exhibit good end use properties such as hardness, tensile strength, modulus, flexibility.
摘要翻译：通过混合含有非极性橡胶和极性橡胶的高熔点热塑性聚合物制备具有良好的高温最终用途和良好耐油溶胀性的热塑性弹性体组合物。或者，将含有非极性橡胶或极性橡胶或两者的高熔点热塑性聚合物与含有非极性橡胶或极性橡胶或两者的聚烯烃热塑性聚合物共混。组合物被动态硫化。固化的多组分热塑性弹性体组合物表现出良好的最终用途性质，例如硬度，拉伸强度，模量，柔韧性。

36. 发明授权

US6060563A Graft copolymers containing ionomer units 失效
标题翻译：含离聚物单元的接枝共聚物
公开(公告)号：US6060563A
公开(公告)日：2000-05-09
申请号：US862630
申请日：1997-05-23
申请人： Dennis G. Peiffer , Hsien-Chang Wang , Pamela Jean Wright , Joseph A. Sissano , Lewis J. Fetters , Louise M. Wheeler , Rebecca L. Rucker
发明人： Dennis G. Peiffer , Hsien-Chang Wang , Pamela Jean Wright , Joseph A. Sissano , Lewis J. Fetters , Louise M. Wheeler , Rebecca L. Rucker
IPC分类号： C08G81/02 , C08F257/00 , C08F257/02 , C08F259/00 , C08F259/02
CPC分类号： C08G81/021
摘要： Graft copolymers having cationic units pendant to the backbone chain are disclosed. These polymers are prepared by reacting a polymer containing halogenated paramethylstyrene units in the chain, e.g., a brominated copolymer of isobutylene and para-methylstyrene, with an anionically polymerized polymer made using an organolithium initiator compound having the formula R.sub.1 R.sub.2 Z R.sub.3 --Li where R.sub.1 and R.sub.2 are alkyl radicals, R.sub.3 is a direct link or an organic radical and Z is nitrogen or phosphorous. Reaction of the anionically polymerized polymer having an R.sub.1 R.sub.2 Z R.sub.3 --end group with the halogenated polymer leads to graft polymers coupled by a quaternary ammonium or phosphonium groups.
摘要翻译：公开了具有垂直于主链的阳离子单元的接枝共聚物。这些聚合物通过使链中含有卤代对甲基苯乙烯单元的聚合物例如异丁烯和对甲基苯乙烯的溴化共聚物与使用具有式R1 R2 Z R3-Li的有机锂引发剂化合物制成的阴离子聚合聚合物反应制备，其中R 1 R2为烷基，R3为直链或有机基团，Z为氮或磷。具有R1R2Z R3-端基的阴离子聚合聚合物与卤化聚合物的反应导致通过季铵或鏻基团偶联的接枝聚合物。

37. 发明授权

US5631316A Tire innerliner comprising ester-functionalized elastomeric interpolymers of C4-C7 isomonoolefin and para-alkylstyrene 失效
标题翻译：轮胎内衬层包括C4-C7异单烯烃和对 - 烷基苯乙烯的酯官能化弹性共聚体
公开(公告)号：US5631316A
公开(公告)日：1997-05-20
申请号：US472373
申请日：1995-06-07
申请人： Bernard J. Costemalle , James V. Fusco , Pierre T. Hous , Hsien-Chang Wang
发明人： Bernard J. Costemalle , James V. Fusco , Pierre T. Hous , Hsien-Chang Wang
IPC分类号： B60C5/14 , B29C33/02 , B29C35/02 , B29D30/06 , B29K21/00 , B29K105/24 , B29L30/00 , B60C1/00 , C08J3/24 , C08L21/00 , C08L23/20 , C08L23/22 , C08L23/26 , C08L25/16 , C08K3/04
CPC分类号： B60C1/0008 , C08L21/00 , C08L23/22 , C08L23/26 , Y02T10/862 , Y10S525/912 , Y10T152/10495
摘要： Vulcanizable tire innerliner compositions are described which are essentially free of halogen atoms or contain a reduced halogen content. The innerliners contain a saturated elastomeric interpolymer of a C.sub.4 -C.sub.7 isomonoolefin, e.g., isobutylene and a para-alkylstyrene e.g., para-methylstyrene, which contains benzylic ester functionality having the structure: ##STR1## wherein R.sub.2 and R.sub.3 are independently selected from hydrogen or C.sub.1 to C.sub.6 alkyl, and R.sub.4 is selected from hydrogen, C.sub.1, to C.sub.28 alkyl, aryl or C.sub.2 to C.sub.28 alkenyl.Innerliners of the invention provide excellent impermeability to air, heat aging properties and good adhesion to tire carcass stock required for tire innerliners, and are also essentially free of halogen or contain low halogen content thereby reducing environmental concerns occasioned by the incineration of used tires.
摘要翻译：描述了基本上不含卤素原子或含有降低的卤素含量的可硫化轮胎内衬组合物。内衬含有C4-C7异单烯烃的饱和弹性互聚物，例如异丁烯和对 - 烷基苯乙烯，例如对甲基苯乙烯，其含有具有以下结构的苄基酯官能团：其中R2和R3独立地选自氢或 C1至C6烷基，R4选自氢，C1至C28烷基，芳基或C2至C28烯基。本发明的内衬对轮胎内衬所需的轮胎胎体材料提供优异的空气不透气性，热老化性能和良好的粘附性，并且也基本上不含卤素或含有低卤素含量，从而减少了废旧轮胎焚烧引起的环境问题。

38. 发明授权

US5597866A Propylene polymer compositions having improved impact strength 失效
标题翻译：丙烯聚合物组合物具有改善的冲击强度
公开(公告)号：US5597866A
公开(公告)日：1997-01-28
申请号：US497486
申请日：1995-06-30
申请人： Donald A. White , Hsien-Chang Wang , Dongming Li
发明人： Donald A. White , Hsien-Chang Wang , Dongming Li
IPC分类号： C08L23/10 , C08L23/28 , C08L51/06 , C08L23/22
CPC分类号： C08L23/10 , C08L23/283 , C08L51/06
摘要： Crystalline propylene polymer compositions having improved impact strength and improved clarity are disclosed. The composition is prepared by melt blending a propylene polymer, e.g., polypropylene, and from about 1 to 35 wt % of an elastomeric interpolymer of a C.sub.4 to C.sub.8 isomonoolefin, e.g., isobutylene, and a para alkystyrene comonomer, e.g., para-methylstyrene. The interpolymer preferably contains a benzylic functional group such as halogen (bromine). The composition may also contain from about 0.5 to 15 wt % of the amide reaction product of an organic acid-grafted propylene polymer, e.g., maleic anhydride grafted polypropylene, and a polyfunctional primary amine.
摘要翻译：公开了具有改进的冲击强度和改进的透明度的结晶丙烯聚合物组合物。该组合物通过熔融共混丙烯聚合物如聚丙烯和约1至35重量％的C4至C8异单烯烃（例如异丁烯）和对甲氧基苯乙烯共聚单体例如对甲基苯乙烯的弹性互聚物来制备。互聚物优选含有苄基官能团如卤素（溴）。组合物还可以含有约0.5至15wt％的有机酸接枝的丙烯聚合物例如马来酸酐接枝聚丙烯和多官能伯胺的酰胺反应产物。

39. 发明授权

US5473017A Intervulcanized elastomer blends 失效
标题翻译：互相硫化弹性体共混物
公开(公告)号：US5473017A
公开(公告)日：1995-12-05
申请号：US305547
申请日：1994-09-14
申请人： Hsien-Chang Wang
发明人： Hsien-Chang Wang
IPC分类号： C08K3/22 , B60C1/00 , C08C19/20 , C08F8/00 , C08K5/14 , C08K5/40 , C08L7/00 , C08L9/00 , C08L11/00 , C08L21/00 , C08L23/16 , C08L23/20 , C08L23/22 , C08L23/26 , C08L13/00
CPC分类号： C08L21/00 , B60C1/0008 , C08L23/22 , C08L23/26 , Y10S525/912
摘要： Intervulcanized compositions having improved curing efficiency are prepared by the free radical curing of a mixture of an ethylenically unsaturated diolefin polymer such as natural or synthetic rubber and a saturated or low unsaturation polymer such as an isobutylene/para-methylstyrene copolymer which contains functional groups pendant to the polymer chain. These functional groups contain an olefinic or vinyl double bond positioned alpha, beta to a substituent group which activates the double bond towards free radical addition reactions with the diolefin polymer. Preferred functionality includes benzylic ester functionality represented by the structure: ##STR1## wherein R.sub.2 and R.sub.3 are independently selected from hydrogen or C.sub.1 to C.sub.6 alkyl, and R.sub.4 is selected from hydrogen, C.sub.1 to C.sub.28 alkyl, aryl or C.sub.2 to C.sub.28 alkenyl.
摘要翻译：具有改进的固化效率的硫化组合物通过烯属不饱和二烯烃聚合物如天然或合成橡胶和饱和或低不饱和聚合物如异丁烯/对甲基苯乙烯共聚物的混合物的自由基固化来制备，所述异丁烯/对甲基苯乙烯共聚物含有垂饰于聚合物链。这些官能团含有与取代基α，β的烯属或乙烯基双键，其活化与二烯烃聚合物的自由基加成反应的双键。优选的功能包括由以下结构表示的苄酯官能团：其中R2和R3独立地选自氢或C1至C6烷基，R4选自氢，C1至C28烷基，芳基或C2至C28烯基。

40. 发明授权

US5451647A Living carbocationic polymerization process 失效
标题翻译：活性碳阳离子聚合工艺
公开(公告)号：US5451647A
公开(公告)日：1995-09-19
申请号：US958406
申请日：1992-10-08
申请人： Rudolf Faust , Hsien-Chang Wang , Miklos Gyor
发明人： Rudolf Faust , Hsien-Chang Wang , Miklos Gyor
IPC分类号： C08F4/16 , C08F4/60 , C08F4/64 , C08F10/00 , C08F12/00 , C08F12/08 , C08F297/00 , C08F10/10
CPC分类号： C08F297/00 , C08F10/00 , Y10S526/912
摘要： An olefin polymerization process is provided wherein an olefin chargestock is contacted with an organic compound polymerization initiator, a Lewis acid coinitiator and a pyridine compound such as 2,6-di-tert-butylpyridine to produce homopolymers, copolymers or block copolymers having a narrow molecular weight distribution.
摘要翻译：提供了一种烯烃聚合方法，其中烯烃装料与有机化合物聚合引发剂，路易斯酸共引发剂和吡啶化合物如2,6-二叔丁基吡啶接触以制备具有窄分子量的均聚物，共聚物或嵌段共聚物体重分布。

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