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31. 发明申请

US20130068139A1 Silica gel comprising guanidine carbonate 审中-公开
标题翻译：含有碳酸胍的硅胶
公开(公告)号：US20130068139A1
公开(公告)日：2013-03-21
申请号：US13617807
申请日：2012-09-14
申请人： Lothar Puppe , Dietrich Pantke
发明人： Lothar Puppe , Dietrich Pantke
IPC分类号： C08K3/28
CPC分类号： C08K3/28 , C01B33/148 , D21H17/68 , D21H21/10
摘要： A process of preparing a silica sol is described. The process involves reacting a fresh sol with guanidine carbonate. The reaction may be conducted in the presence of a base (e.g., sodium water glass), and at a pH of from 8 to 12. The process of the present invention may also include concentrating steps. The silica sol prepared by the method of the present invention has a BET surface area of greater than or equal to 100 m2/g, and contains from 0.05 to 15% by weight of gaunidinium ions, based on the total weight of the silica gel.
摘要翻译：描述了制备二氧化硅溶胶的方法。该方法包括使新鲜的溶胶与碳酸胍反应。反应可以在碱（例如钠水玻璃）存在下进行，pH为8〜12。本发明的方法还可以包括浓缩步骤。通过本发明的方法制备的二氧化硅溶胶具有大于或等于100m 2 / g的BET表面积，并且基于硅胶的总重量含有0.05至15重量％的高锰酸根离子。

32. 发明授权

US08299131B2 Silica gel comprising guanidine carbonate 失效
标题翻译：含有碳酸胍的硅胶
公开(公告)号：US08299131B2
公开(公告)日：2012-10-30
申请号：US10520574
申请日：2003-07-07
申请人： Lothar Puppe , Dietrich Pantke
发明人： Lothar Puppe , Dietrich Pantke
IPC分类号： C01B33/12 , C01B33/141
CPC分类号： C08K3/28 , C01B33/148 , D21H17/68 , D21H21/10
摘要： A process of preparing a silica sol is described. The process involves reacting a fresh sol with guanidine carbonate. The reaction may be conducted in the presence of a base (e. g. , sodium water glass), and at a pH of from 8 to 12. The process of the present invention may also include concentrating steps. The silica sol prepared by the method of the present invention has a BET surface area of greater than or equal to 100 m2/g, and contains from 0.05 to 15% by weight of gaunidinium ions, based on the total weight of the silica gel.
摘要翻译：描述了制备二氧化硅溶胶的方法。该方法包括使新鲜的溶胶与碳酸胍反应。反应可以在碱（例如钠水玻璃）存在下进行，pH为8〜12。本发明的方法还可以包括浓缩步骤。通过本发明的方法制备的二氧化硅溶胶具有大于或等于100m 2 / g的BET表面积，并且基于硅胶的总重量含有0.05至15重量％的高锰酸根离子。

33. 发明授权

US06710217B1 Method for producing 4-chlorobiphenyl and 4-chlorobiphenyl-specific specifications 失效
标题翻译：制备4-氯联苯和4-氯联苯的具体规格的方法
公开(公告)号：US06710217B1
公开(公告)日：2004-03-23
申请号：US10009536
申请日：2001-11-13
申请人： Reinhard Langer , Alexander Klausener , Paul Wagner , Lothar Puppe
发明人： Reinhard Langer , Alexander Klausener , Paul Wagner , Lothar Puppe
IPC分类号： C07C1700
CPC分类号： C07C25/18 , B01J27/10 , B01J29/60 , C07C17/12 , C07C17/383
摘要： The invention relates to a process for preparing 4-chlorobiphenyl by (a) reacting biphenyl and chlorine in the presence of one or more ring-chlorination catalysts, and (b) subjecting the reaction mixture obtained in step (a) to fractional distillation to obtain 4-chlorobiphenyl.
摘要翻译：本发明涉及一种通过（a）在一种或多种环氯化催化剂存在下使联苯和氯反应制备4-氯联苯的方法，和（b）将步骤（a）中获得的反应混合物进行分馏，得到 4-氯联苯。

34. 发明授权

US5885331A Process for the adsorption of nitrogen from gas mixtures by means of pressure swing adsorption with zeolites 失效
标题翻译：通过利用沸石的变压吸附从气体混合物中吸附氮的方法
公开(公告)号：US5885331A
公开(公告)日：1999-03-23
申请号：US690415
申请日：1996-07-25
申请人： Gerhard Reiss , Lothar Puppe , Bruno Hees
发明人： Gerhard Reiss , Lothar Puppe , Bruno Hees
IPC分类号： B01D53/04 , B01D53/047 , B01J20/18 , C01B13/02 , C01B21/04
CPC分类号： C01B13/027 , B01D53/047 , B01D2253/108 , B01D2256/12 , B01D2257/102 , B01D2259/40052 , B01D53/0446 , B01D53/0476 , C01B2210/0046 , Y10S95/902
摘要： In the pressure swing adsorption of nitrogen from gas mixtures with less polar gas components at temperatures of between 20.degree. and 50.degree. C., wherein the gas mixture is passed through an adsorber which is filled with packings of zeolite pellets and has an inlet zone and an outlet zone, the improvement which comprises providing at least two packings in the adsorber, a packing of Li-zeolite X in the inlet zone of the adsorber and a packing of at least one of Ca-zeolite A and Ca-zeolite X in the outlet zone of the adsorber.
摘要翻译：在20至50℃的温度下，在具有极性较小的气体组分的气体混合物的氮气的变压吸附中，其中气体混合物通过填充有沸石颗粒的填料的吸附器，并具有入口区和出口区，其改进包括在吸附器中提供至少两个填料，在吸附器的入口区域中包含Li-沸石X，并且在该吸附器的至少一个Ca-沸石A和Ca-沸石X的填料中吸附器的出口区。

35. 发明授权

US5386067A Process for separating mixtures of m- and p-dichlorobenzene 失效
标题翻译：分离对 - 二氯苯混合物的方法
公开(公告)号：US5386067A
公开(公告)日：1995-01-31
申请号：US252154
申请日：1994-06-01
申请人： Ursula Pentling , Hans-Josef Buysch , Lothar Puppe , Kai Rohlk , Rolf Grosser , Hans-Ingolf Paul
发明人： Ursula Pentling , Hans-Josef Buysch , Lothar Puppe , Kai Rohlk , Rolf Grosser , Hans-Ingolf Paul
IPC分类号： B01D15/00 , B01D15/04 , C07C17/38 , C07C17/389 , C07C25/08
CPC分类号： C07C17/389
摘要： Mixtures of m- and p-dichlorobenzene can be separated by treating such mixtures in the liquid phase with a pentasil zeolite at from 20.degree. to 250.degree. C., a filtrate enriched in m-dichlorobenzene being removed and the p-dichlorobenzene being obtained by desorption of the pentasil zeolite. The pentasil zeolites may contain, as exchangeable cations, protons, cations of the first or second main group of the Mendeleev Periodic System, cations of the rare earth metals or a mixture of a plurality thereof. In order to prepare the liquid phase a solvent is used that belongs to the group of cyclic saturated hydrocarbons having 5 to 15 carbon atoms, alkyl-substituted aromatic hydrocarbons having 8 to 12 carbon atoms, and halogen-substituted aromatic hydrocarbons having 6 to 10 carbon atoms and 1 to 3 halogen atoms. The solvents ethylbenzene, chlorobenzene, p-xylene, p-chlorotoluene and dichlorobenzene are excepted. A mixture of a plurality of these solvents may also be used.
摘要翻译：可以通过在20至250℃下用pentasil沸石处理液相中的这种混合物来分离对 - 二氯苯的混合物，除去富含间二氯苯的滤液，将对二氯苯由五硅沸石的解吸。戊二烯沸石可以包含作为可交换阳离子的质子，门多列夫周期系统的第一或第二主要组分的阳离子，稀土金属的阳离子或其多个混合物。为了制备液相，使用属于具有5至15个碳原子的环状饱和烃基团，具有8至12个碳原子的烷基取代的芳族烃和具有6至10个碳原子的卤素取代的芳族烃的溶剂原子和1至3个卤素原子。溶剂乙苯，氯苯，对二甲苯，对氯甲苯和二氯苯除外。也可以使用多种这些溶剂的混合物。

36. 发明授权

US5360922A Process for the preparation of dialkyl carbonates 失效
标题翻译：制备碳酸二烷基酯的方法
公开(公告)号：US5360922A
公开(公告)日：1994-11-01
申请号：US23302
申请日：1993-02-26
申请人： Erich Wolters , Heinz Landscheidt , Alexander Klausener , Lothar Puppe
发明人： Erich Wolters , Heinz Landscheidt , Alexander Klausener , Lothar Puppe
IPC分类号： B01J29/064 , C07C68/00 , C07C69/96
CPC分类号： B01J29/064 , C07C68/00 , Y02P20/582
摘要： Dialkyl carbonates can be prepared by the reaction of carbon monoxide with alkyl nitrites in a continuous gas phase reaction, using a platinum group metal catalyst on an alumosilicate zeolite having acidic centers, preferably in the H.sup.+ form, as a support, which catalyst may optionally comprise additional material of a compound of antimony, bismuth, aluminum, copper, vanadium, niobium, tantalum, tin, iron, cobalt, nickel or a mixture of a plurality of these, and hydrogen halide being added in the course of the reaction intermittently or continuously. In this reaction, the dialkyl carbonates are formed with almost quantitative selectivity; the corresponding dialkyl oxalates cannot be detected in most cases.
摘要翻译：碳酸二烷基酯可以通过在连续气相反应中使用一氧化碳与烷基亚硝酸盐的反应来制备，使用铂族金属催化剂在具有酸性中心的铝硅酸盐沸石，优选以H +形式作为载体，该催化剂可任选地包含锑，铋，铝，铜，钒，铌，钽，锡，铁，钴，镍或它们中的多种的混合物的化合物的附加材料和在反应过程中间歇或连续地加入的卤化氢。在该反应中，以几乎定量的选择性形成碳酸二烷基酯; 在大多数情况下不能检测到相应的草酸二烷基酯。

37. 发明授权

US5098448A Process for the production of molecular sieve granulates 失效
标题翻译：生产分子筛颗粒的方法
公开(公告)号：US5098448A
公开(公告)日：1992-03-24
申请号：US680601
申请日：1991-04-01
申请人： Lothar Puppe , Gunter Ulisch
发明人： Lothar Puppe , Gunter Ulisch
IPC分类号： B01J2/14 , B01J2/28 , B01J20/18 , C01B39/18 , C01B39/22 , C01B39/24 , C01B39/26 , C01B39/30 , C01B39/38
CPC分类号： B01J2/14 , B01J2/28 , B01J20/183
摘要： A process for the production of silica-bound zeolite granulates is disclosed, wherein zeolite to be formed into a granulate is mixed with silica sol. The process is carried out by adding aqueous alkali metal silicate to the silica sol immediately before the silica sol is mixed with the solid zeolite to be granulated. By the described process, granulates of various grain sizes can be obtained, and the resultant granulates can have a narrow grain size distribution.
摘要翻译：公开了一种生产二氧化硅结合的沸石颗粒的方法，其中将形成颗粒的沸石与硅溶胶混合。该方法是在将二氧化硅溶胶与要造粒的固体沸石混合之前，向二氧化硅溶胶中加入碱金属硅酸盐。通过所述方法，可以获得各种粒径的颗粒，并且所得到的颗粒可以具有窄的粒度分布。

38. 发明授权

US5072017A Process for the preparation of P-substituted O-benzylphenols 失效
标题翻译：制备O-取代的苄氧基苯酚的方法
公开(公告)号：US5072017A
公开(公告)日：1991-12-10
申请号：US505799
申请日：1990-04-06
申请人： Hans-Josef Buysch , Gunter Klug , Peter Mues , Lothar Puppe
发明人： Hans-Josef Buysch , Gunter Klug , Peter Mues , Lothar Puppe
IPC分类号： C07C43/23 , B01J29/08 , C07B61/00 , C07C27/00 , C07C37/11 , C07C37/16 , C07C37/18 , C07C39/15 , C07C41/00 , C07C41/30 , C07C67/00 , C07C67/343 , C07C69/76 , C07C69/92 , C07C255/53 , C07C313/00 , C07C319/20 , C07C323/20 , C07C323/62
CPC分类号： B01J29/08 , C07C37/16 , C07C37/18
摘要： Para-substituted o-benzylphenols are prepared by reacting p-substituted phenols with benzylating agents in the presence of zeolites of the faujasite type at elevated temperature.
摘要翻译：对位取代的邻 - 苄基苯酚是通过在升高的温度下在八面沸石型沸石存在下使对取代的酚与苄化剂反应来制备的。

39. 发明授权

US4990687A Preparation of 4-methyl-2-cyclohexylphenol 失效
标题翻译：制备4-甲基-2-环己基苯酚
公开(公告)号：US4990687A
公开(公告)日：1991-02-05
申请号：US436156
申请日：1989-11-13
申请人： Alfons Klein , Helmut Fiege , Lothar Puppe , Werner Jeblick
发明人： Alfons Klein , Helmut Fiege , Lothar Puppe , Werner Jeblick
IPC分类号： C07C37/11 , C07B61/00 , C07C37/14 , C07C37/16 , C07C39/15
CPC分类号： C07C37/16 , C07C37/14 , B01J2229/183 , B01J29/084 , B01J29/088 , C07C2101/14
摘要： 4-Methyl-2-cyclohexylphenol can be prepared by alkylation of p-cresol with cyclohexanol or cyclohexene by performing the reaction in the liquid phase in the presence of 1-10% by weight, based on the amount of p-cresol, of a large pore, acidic zeolite.
摘要翻译： 4-甲基-2-环己基苯酚可以通过使对甲酚与环己醇或环己烯烷基化来制备，通过在1-10％（重量）的对甲苯酚的存在下，在液相中进行反应，大孔，酸性沸石。

40. 发明授权

US4913850A Process for the removal of iodine and organic iodine compounds from gases and vapors using silver-containing zeolite of the faujasite type 失效
标题翻译：使用八面沸石类的含银沸石从气体和蒸气中除去碘和有机碘化合物的方法
公开(公告)号：US4913850A
公开(公告)日：1990-04-03
申请号：US318841
申请日：1989-03-06
申请人： Lothar Puppe , Jurgen Wilhelm
发明人： Lothar Puppe , Jurgen Wilhelm
IPC分类号： B01D53/68
CPC分类号： B01D53/68
摘要： Iodine and organic iodine compounds which may be radioactive and which may be found in waste gases or vapors from nuclear reactors can be removed from such gases or vapors by passing the iodine or organic iodine compound-containing gases or vapors through a layer of binder-free silver-exchanged molecular sieve granulates of the faujasite type.
摘要翻译：可以通过使含碘或有机碘化合物的气体或蒸汽通过一层无粘合剂的物质，可以从这种气体或蒸气中除去可能是放射性的并且可能存在于来自核反应堆的废气或蒸汽中的碘和有机碘化合物银盐交换分子筛颗粒的八面沸石型。

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