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31. 发明授权

US08318889B2 Organic polyurethane shape memory material and a preparation method thereof 有权
标题翻译：有机聚氨酯形状记忆材料及其制备方法
公开(公告)号：US08318889B2
公开(公告)日：2012-11-27
申请号：US11889867
申请日：2007-08-17
申请人： Wen-Chiung Su , Cheng-Che Tsai , Ching-Shiang Yu , Shenghong A Dai , Ru-Jong Jeng
发明人： Wen-Chiung Su , Cheng-Che Tsai , Ching-Shiang Yu , Shenghong A Dai , Ru-Jong Jeng
IPC分类号： C08G18/00
CPC分类号： C08G18/4277 , C08G18/2825 , C08G18/3275 , C08G18/714 , C08G18/7671 , C08G83/003 , C08G2280/00
摘要： An organic polyurethane shape memory material includes a C10 chain or C18 chain and consists of hard segment and soft segment. The material is produced by reacting the single-chain type dendrimer with diethylenetriamine to produce dendrimer. Then dendrimer reacts with N-(3-aminopropyl)diethanolamine to produce dendritic diols. Next, polymer HO(C6H10O2)xC2H4OC2H4(C6H10O2)yOH, where x+y=25˜26, reacts with methylenedi-p-phenyl diisocyanate, and at least one type of dendritic diols is added to produce the organic polyurethane shape memory material.
摘要翻译：有机聚氨酯形状记忆材料包括C10链或C18链，由硬链段和软链段组成。该材料通过使单链型树枝状聚合物与二亚乙基三胺反应制备树枝状聚合物而制备。然后树枝状大分子与N-（3-氨基丙基）二乙醇胺反应产生枝状二醇。接下来，将聚合物HO（C6H10O2）xC2H4OC2H4（C6H10O2）yOH（其中x + y = 25〜26）与亚甲基二苯基二异氰酸酯反应，并加入至少一种类型的树枝状二醇以制备有机聚氨酯形状记忆材料。

32. 发明申请

US20110213114A1 DENDRON, POLYURETHANE WITH SIDE-CHAIN REGULAR DENDRON, AND PRODUCING METHODS THEREOF 有权
标题翻译： DENDRON，具有侧链常规聚苯乙烯的聚氨酯及其生产方法
公开(公告)号：US20110213114A1
公开(公告)日：2011-09-01
申请号：US12714515
申请日：2010-02-28
申请人： WEN-CHIUNG SU , Wei-Ho Ting , Chun-Ming Yeh , Chia-Cheng Chang , Sheng-Hong Dai , Ru-Jong Jeng
发明人： WEN-CHIUNG SU , Wei-Ho Ting , Chun-Ming Yeh , Chia-Cheng Chang , Sheng-Hong Dai , Ru-Jong Jeng
IPC分类号： C08G18/32 , C08G18/24 , C07C271/06
CPC分类号： C07C275/40 , C08G18/10 , C08G18/2825 , C08G18/2895 , C08G18/3228 , C08G18/3275 , C08G18/4825 , C08G18/4854 , C08G18/3831
摘要： A dendron with hydrophobic functional of end group, a polyurethane with the dendron, and producing methods thereof are disclosed. The dendron with hydrophobic functional of end group in the polyurethane systems, and the honeycomb-like structure thin films were obtained by a breath-figure process. The structures of dendron and dendritic side-chain polyurethanes are respectively expressed in the following. Therein, the end-groups (R) of the dendron are long alkyl chains or perfluoroalkyl derivatives.
摘要翻译：公开了具有端基疏水功能的树枝状突起，具有树突的聚氨酯及其制造方法。在聚氨酯体系中具有端基疏水功能的树枝状体，蜂窝状结构薄膜通过呼吸图法得到。树枝状和枝状侧链聚氨酯的结构分别表示如下。其中，树枝状结构基团（R）是长烷基链或全氟烷基衍生物。

33. 发明授权

US07741505B2 Bisbiphenylacylphosphine oxide and preparation method therefore 有权
标题翻译：二苯基酰基氧化膦及其制备方法
公开(公告)号：US07741505B2
公开(公告)日：2010-06-22
申请号：US12141354
申请日：2008-06-18
申请人： Wen-Chiung Su , Chang-Chih Lin , Ching-Shang Sheng
发明人： Wen-Chiung Su , Chang-Chih Lin , Ching-Shang Sheng
IPC分类号： C07F9/02
CPC分类号： C07F9/657172
摘要： A bisbiphenylacylphosphine oxide of formula (I) and its preparation method are provided. The formula of —Ar— is First, 10-chloro-9,10-dihydro-9-oxa-10-phosphaphenanthrene (CDOP) is prepared by using 2-phenylphenol, and then is esterified to synthesize 6-methoxy-(6H)-dibenz[c,e][1,2]oxa-phosphorin (MDOP). Next, acid chloride compounds are added for performing the Arbuzov reaction to synthesize bisbiphenylacylphosphine oxide. CDOP is hydrolyzed to be derived into 9,10-dihydro-9-oxa-10-phosphaphen-anthrene-10-oxide (DOPO), and then DOPO reacts with arylaldehyde to form secondary alcohol. Therefore, bisbiphenylacylphosphine oxide is prepared by using secondary alcohol under oxidation. Also, under a coupling reaction, DOPO reacts with the acid chloride compounds by using a Lewis acid as a catalyst to prepare bisbiphenylacylphosphine oxide.
摘要翻译：提供式（I）的双联苯酰基氧化膦及其制备方法。 -Ar-的配方是通过使用2-苯基苯酚制备10-氯-9,10-二氢-9-氧杂-10-磷杂菲（CDOP），然后酯化合成6-甲氧基 - （6H） - - 二苯并[c，e] [1,2]氧杂 - 磷杂（MDOP）。接下来，加入酰氯化合物进行Arbuzov反应以合成双联苯基酰基氧化膦。将CDOP水解成9,10-二氢-9-氧杂-10-磷杂蒽-10-氧化物（DOPO），然后DOPO与芳基醛反应形成仲醇。因此，通过使用仲醇在氧化下制备双联苯基酰基氧化膦。此外，在偶联反应中，DOPO通过使用路易斯酸作为催化剂与酰基氯化合物反应以制备双联苯基酰基氧化膦。

34. 发明申请

US20080287701A1 BISBIPHENYLACYLPHOSPHINE OXIDE AND PREPARATION METHOD THEREFORE 有权
标题翻译：二苯基乙基氧化膦及其制备方法
公开(公告)号：US20080287701A1
公开(公告)日：2008-11-20
申请号：US12141380
申请日：2008-06-18
申请人： Wen-Chiung Su , Chang-Chih Lin , Ching-Shang Sheng
发明人： Wen-Chiung Su , Chang-Chih Lin , Ching-Shang Sheng
IPC分类号： C07F9/6571
CPC分类号： C07F9/657172
摘要： A bisbiphenylacylphosphine oxide of formula (I) and its preparation method are provided. The formula of —Ar— is First, 10-chloro-9,10-dihydro-9-oxa-10-phosphaphenanthrene (CDOP) is prepared by using 2-phenylphenol, and then is esterified to synthesize 6-methoxy-(6H)-dibenz[c,e][1,2]oxa-phosphorin (MDOP). Next, acid chloride compounds are added for performing the Arbuzov reaction to synthesize bisbiphenylacylphosphine oxide. CDOP is hydrolyzed to be derived into 9,10-dihydro-9-oxa-10-phosphaphen-anthrene-10-oxide (DOPO), and then DOPO reacts with arylaldehyde to form secondary alcohol. Therefore, bisbiphenylacylphosphine oxide is prepared by using secondary alcohol under oxidation. Also, under a coupling reaction, DOPO reacts with the acid chloride compounds by using a Lewis acid as a catalyst to prepare bisbiphenylacylphosphine oxide.
摘要翻译：提供式（I）的双联苯酰基氧化膦及其制备方法。 -Ar-的配方是通过使用2-苯基苯酚制备10-氯-9,10-二氢-9-氧杂-10-磷杂菲（CDOP），然后酯化合成6-甲氧基 - （6H） - 二苯并[c，e] [1,2]氧杂 - 磷杂（MDOP）。接下来，加入酰氯化合物进行Arbuzov反应以合成双联苯基酰基氧化膦。将CDOP水解成9,10-二氢-9-氧杂-10-磷杂蒽-10-氧化物（DOPO），然后DOPO与芳基醛反应形成仲醇。因此，通过使用仲醇在氧化下制备双联苯基酰基氧化膦。此外，在偶联反应中，DOPO通过使用路易斯酸作为催化剂与酰基氯化合物反应以制备双联苯基酰基氧化膦。

35. 发明申请

US20050101793A1 Method for preparing a biphenylphosphonate compound 有权
标题翻译：联苯膦酸盐化合物的制备方法
公开(公告)号：US20050101793A1
公开(公告)日：2005-05-12
申请号：US10972396
申请日：2004-10-26
申请人： Wen-Chiung Su , Chin-Shang Sheng
发明人： Wen-Chiung Su , Chin-Shang Sheng
IPC分类号： C07F9/02 , C07F9/6571
CPC分类号： C07F9/657163
摘要： A method for preparing a biphenylphosphonate compound of the following formula (I): wherein n is 2 or 3; Ar is a C6-C16 aromatic group; which comprising (a) reacting an o-phenylphenol with a phosphorus trichloride in the presence of a zinc chloride catalyst to form a 6-chloro-6H-dibenz [c,e][1,2] oxaphosphorin of the following formula (II); (b) reacting a polyhydroxybenzene compound of the formula (III) (HO)n—Ar (III) wherein n and Ar are defined the same as the above, with the compound of formula (II) to form a compound of the following formula (IV) wherein n and Ar are defined the same as the above; and (c) oxidizing the compound of formula (IV) in the presence of water and ozone to form the compound of formula (I).
摘要翻译：一种制备下式（I）的联苯膦酸酯化合物的方法：其中n为2或3; Ar是C 6 -C 16芳基; 其包括（a）在氯化锌催化剂存在下使邻苯基苯酚与三氯化磷反应以形成下式（II）的6-氯-6H-二苯并[c，e] [1,2]氧杂磷杂环戊烯， ; （b）使式（III）的多羟基苯化合物<？in-line-formula description =“In-line Formulas”end =“lead”→（HO）n -Ar（III ）其中n和Ar与上述定义相同，与式（II）的化合物反应形成下列化合物：式（Ⅳ）其中n和Ar定义与上述相同; 和（c）在水和臭氧存在下氧化式（Ⅳ）化合物以形成式（I）化合物。

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