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21. 发明授权

US6060617A Contaminant free organometallic amide compositions and processes for making same 失效
标题翻译：污染物游离有机金属酰胺组合物及其制备方法
公开(公告)号：US6060617A
公开(公告)日：2000-05-09
申请号：US670348
申请日：1996-06-25
申请人： Randy W. Hall , Bobby J. McElroy , James A. Schwindeman , Conrad W. Kamienski , Terry L. Rathman , Robert C. Morrison
发明人： Randy W. Hall , Bobby J. McElroy , James A. Schwindeman , Conrad W. Kamienski , Terry L. Rathman , Robert C. Morrison
IPC分类号： C07C211/65 , C07F7/10
CPC分类号： C07F7/10 , C07C211/65
摘要： Organometallic amide compositions and processes for preparing the same, for example, by: reacting an alkali metal, alkali metal hydride, or alkali metal amide with a substituted amine in the absence of an electron carrier; reacting an alkali metal with a substituted amine in the presence of an electron carrier in a hydrocarbon solvent; distilling a composition which includes an alkali metal amide and a reduced electron carrier to recover the alkali metal amide; reacting an alkali metal with a substituted amine in the presence of an alkyl halide; and reacting a substituted amine capable of reacting with an alkali metal to form a hydrocarbon insoluble alkali metal amide with an alkali metal in the presence of a substituted amine capable of reacting with an alkali metal to form a hydrocarbon soluble alkali metal amide.
摘要翻译：有机金属酰胺组合物及其制备方法，例如：在不存在电子载体的情况下使碱金属，碱金属氢化物或碱金属氨化物与取代的胺反应; 在电子载体存在下在烃溶剂中使碱金属与取代的胺反应; 蒸馏包含碱金属氨化物和还原电子载体以回收碱金属胺的组合物; 在烷基卤存在下使碱金属与取代的胺反应; 并使能够与碱金属反应的取代的胺与能够与碱金属反应形成烃溶性碱金属氨化物的取代胺存在下与碱金属形成不溶于烃的碱金属胺。

22. 发明授权

US5882548A Luminescent organic-inorganic perovskites with a divalent rare earth metal halide framework 失效
标题翻译：发光有机 - 无机钙钛矿与二价稀土金属卤化物框架
公开(公告)号：US5882548A
公开(公告)日：1999-03-16
申请号：US852894
申请日：1997-05-08
申请人： Kangning Liang , David Brian Mitzi
发明人： Kangning Liang , David Brian Mitzi
IPC分类号： C07C211/63 , C07C211/65 , C07F5/00 , C07F7/22 , C07F7/24 , C07F7/30 , C09K11/06 , H01L51/50 , H05B33/12 , H05B33/14 , C07C291/00
CPC分类号： C09K11/06 , C07C211/65 , C07F5/003 , H01L51/001 , H01L51/0089
摘要： There is disclosed herein novel organic-inorganic layered perovskites of the general formula A.sub.2 MX.sub.4 where A is an organic ammonium cation, M is a divalent rare earth metal and X is a halogen. These compounds can be made by a low temperature (about 100.degree.-160.degree. C.) solid state reaction between the organic ammonium salt with the appropriate hydrogen halide and MX.sub.2 where M is a divalent rare earth metal and X is a halogen). A specific example is (C.sub.4 H.sub.9 NH.sub.3).sub.2 EuI.sub.4 which has been made through a reaction at about 140.degree.-160 C. between C.sub.4 H.sub.9 NH.sub.2. HI and EuI.sub.2. This new compound produces intense blue photoluminescence at room temperature, with a peak wavelength of 460 nm and a fairly narrow peak width (FWHM=24 nm). In addition to the simple aliphatic ammonium cations of the form C.sub.n H.sub.2n+1 NH.sub.3.sup.+, e.g., propylammonium (C.sub.3 H.sub.7 NH.sub.3) and butylammonium (C.sub.4 H.sub.9 NH.sub.3), a wide range of organic cations including those based on aliphatic amines, simple aromatic amines and more complex organic cations will substitute into the "A" sites of the current family of novel organic-inorganic perovskites. There is also disclosed a novel perovskite of the general formula AMX.sub.3, CH.sub.3 NH.sub.3 EuI.sub.3, having a photoluminescence peak at 448 nm. Both families of compounds are expected to be useful in devices such as organic/inorganic light emitting diodes.
摘要翻译：公开了通式A2MX4的新型有机 - 无机层状钙钛矿，其中A为有机铵阳离子，M为二价稀土金属，X为卤素。这些化合物可以通过有机铵盐与合适的卤化氢和MX2（其中M是二价稀土金属，X是卤素）的低温（约100-116℃）固态反应来制备。一个具体实例是（C4H9NH3）2EuI4，它们是通过C4H9NH2之间约140-160℃的反应制成的。 HI和EuI2。这种新化合物在室温下产生强烈的蓝色光致发光，峰值波长为460nm，峰宽相当窄（FWHM = 24nm）。除了CnH2n + 1NH3 +形式的简单的脂族铵阳离子，例如丙基铵（C 3 H 7 NH 3）和丁基铵（C 4 H 9 NH 3）外，包括基于脂族胺，简单芳香胺和更复杂的有机阳离子的有机阳离子范围广泛，将取代进入目前新型有机 - 无机钙钛矿家族的“A”场。还公开了在448nm处具有光致发光峰的通式为AMX3，CH3NH3Eu3的新型钙钛矿。预期这两种化合物族可用于诸如有机/无机发光二极管的器件中。

23. 发明授权

US5856079A Preparation and use of a dimethylamine silver bromo-iodide complex as a single source precursor for iodide incorporation in silver bromide crystals 失效
标题翻译：制备和使用二甲胺碘溴化银络合物作为溴化银晶体中碘化物掺入的单一来源前体
公开(公告)号：US5856079A
公开(公告)日：1999-01-05
申请号：US865753
申请日：1997-05-30
申请人： Tommie L. Royster, Jr. , Seshadri Jagannathan , David E. Fenton , Samuel Chen
发明人： Tommie L. Royster, Jr. , Seshadri Jagannathan , David E. Fenton , Samuel Chen
IPC分类号： C07C209/68 , C07C211/65 , C07F1/00 , C07F5/06 , G03C1/015 , G03C1/005 , C01G5/00 , C01G5/02 , C07F1/10
CPC分类号： C07F1/005 , G03C1/015
摘要： A dimeitylarnine silver bromo-iodide complex is used as a single source precursor for iodide incorporation in silver bromide crystals.
摘要翻译：碘化银碘化银络合物用作溴化银晶体中碘化物掺入的单一来源前体。

24. 发明授权

US5847227A Method for producing aryl alkyl hydroperoxides 失效
标题翻译：芳基烷基氢过氧化物的制备方法
公开(公告)号：US5847227A
公开(公告)日：1998-12-08
申请号：US607496
申请日：1996-02-27
申请人： Terunori Fujita , Shigekazu Matsui , Toshihiro Takai , Hideto Matsuoka , Akifumi Kagayama , Hiroshi Kuroda , Masayasu Ishibashi , Hiroshi Iwasaki , Nobuya Hirokane
发明人： Terunori Fujita , Shigekazu Matsui , Toshihiro Takai , Hideto Matsuoka , Akifumi Kagayama , Hiroshi Kuroda , Masayasu Ishibashi , Hiroshi Iwasaki , Nobuya Hirokane
IPC分类号： C07F13/00 , C07C211/65 , C07C215/14 , C07C219/06 , C07C229/16 , C07C233/36 , C07C251/24 , C07C251/74 , C07C251/76 , C07C251/86 , C07C255/24 , C07C407/00 , C07C409/08 , C07C409/10 , C07C409/12 , C07D255/02 , C07D257/02 , C07D259/00 , C07F1/08 , C07F15/00 , C07C45/32 , C07C45/33
CPC分类号： C07C233/36 , C07C211/65 , C07C215/14 , C07C219/06 , C07C229/16 , C07C251/24 , C07C251/74 , C07C251/76 , C07C251/86 , C07C255/24 , C07C407/00 , C07C409/08 , C07C409/10 , C07C409/12 , C07D255/02 , C07D257/02 , C07D259/00
摘要： A method for producing aryl alkyl hydroperoxides which comprises selectively oxidizing an aryl alkyl hydrocarbon having the formula: ##STR1## wherein P and Q are hydrogen or an alkyl and may be the same or different from each other; x is an integer of 1-3; and Ar is an aromatic hydrocarbon group having a valence of x, with an oxygen-containing gas in the presence of a transition metal complex which contains, as a ligand, a cyclic polyfunctional amine compound having at least three nitrogen atoms in the ring forming molecular chain or an open chain polyfunctional amine compound having at least three nitrogen atoms in the main chain of the molecule.
摘要翻译：一种制备芳基烷基氢过氧化物的方法，其包括选择性氧化具有下式的芳基烷基烃：其中P和Q是氢或烷基并且可以彼此相同或不同; x是1-3的整数; 并且在具有含氧气体的过渡金属络合物存在下，Ar是具有x价的芳族烃基，其中所述过渡金属络合物在环形成分子中含有至少三个氮原子的环状多官能胺化合物链或在分子主链中具有至少三个氮原子的开链多官能胺化合物。

25. 发明授权

US5681790A Catalyst for preparing methacrylic acid 失效
标题翻译：用于制备甲基丙烯酸的催化剂
公开(公告)号：US5681790A
公开(公告)日：1997-10-28
申请号：US565712
申请日：1995-11-30
申请人： Young Chul Kim , Ki Hwa Lee , Eun Hee Jin
发明人： Young Chul Kim , Ki Hwa Lee , Eun Hee Jin
IPC分类号： B01J31/36 , B01J27/199 , B01J31/02 , C07B61/00 , C07C51/235 , C07C57/055 , C07C211/65 , B01J31/00
CPC分类号： B01J23/002 , B01J27/199 , B01J31/0239 , B01J31/0254 , C07C211/65 , B01J2231/70 , B01J2231/76 , B01J2523/00
摘要： This invention relates to a novel catalyst for preparing methacrylic acid by gas phase oxidation of methacrolein obtained by gas phase catalytic oxidation of isobutylene or t-butanol. The catalyst is represented by the formula: P.sub.a Mo.sub.11 V.sub.b Du.sub.c X.sub.d Q.sub.e Z.sub.f O.sub.g wherein X is at least one of potassium, rubium, cessium, and thallium; Z is at least one of lead, antimony, chromium, iron, bismuth, cerium, and zinc; Q is at least one of organic quaternary ammonium cations consisting of ##STR1## in which R, R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are each independently selected from the group consisting of C.sub.1 -C.sub.5 alkyl or C.sub.1 -C.sub.5 substituted alkyl having functional groups; a is a number from 0.8 to 1.6; b is a number from 0.6 to 2; c is a number from 0.1 to 0.8; d is a number from 0.7 to 2.2; e is a number from 0.01 to 0.1; f is a number from 0 to 0.5; and g is a number of oxygens required to satisfy the valence requirements of the other elements present.
摘要翻译：本发明涉及一种用于通过气相氧化异丁烯或异丁烯通过气相催化氧化获得的甲基丙烯醛来制备甲基丙烯酸的新型催化剂。该催化剂由下式表示：其中X是钾，铷，铯和铊中的至少一种：PaMo11VbDucXdQeZfOg; Z是铅，锑，铬，铁，铋，铈和锌中的至少一种; Q是由以下组成的至少一种有机季铵阳离子：其中R，R 1，R 2，R 3和R 4各自独立地选自具有官能团的C 1 -C 5烷基或C 1 -C 5取代的烷基; a是从0.8到1.6的数字; b是从0.6到2的数字; c为0.1〜0.8的数; d是从0.7到2.2的数字; e为0.01〜0.1的数; f是从0到0.5的数字; 并且g是满足其它元素的化合价要求所需的数量的氧。

26. 发明授权

US5380897A Tri(platinum) complexes 失效
标题翻译：三（铂）复合物
公开(公告)号：US5380897A
公开(公告)日：1995-01-10
申请号：US66581
申请日：1993-05-25
申请人： James D. Hoeschele , Yun Qu , Nicholas Farrell
发明人： James D. Hoeschele , Yun Qu , Nicholas Farrell
IPC分类号： A61K31/555 , A61K31/282 , A61K33/24 , A61P33/00 , A61P35/00 , C07C211/65 , C07F15/00 , A61K31/28 , A61K31/66
CPC分类号： C07F15/008
摘要： Novel tri(platinum) complexes containing three platinum coordination spheres coupled via diamine or triamine bridging agents are taught as well as methods for their preparation. These complexes are to be used as pharmaceutical agents, e.g., for the treatment of cancer and parasitic diseases.
摘要翻译：教导了含有通过二胺或三胺桥连剂偶联的三个铂配位球的新型三（铂）配合物及其制备方法。这些复合物用作药剂，例如用于治疗癌症和寄生虫病。

27. 发明授权

US5290961A Platinum compound and process of preparing same 失效
标题翻译：铂化合物及其制备方法
公开(公告)号：US5290961A
公开(公告)日：1994-03-01
申请号：US3306
申请日：1993-01-12
申请人： Koji Okamoto , Yuko Hoshi , Chihiro Nakanishi
发明人： Koji Okamoto , Yuko Hoshi , Chihiro Nakanishi
IPC分类号： A61K31/28 , C07C209/68 , C07C211/65 , C07F15/00
CPC分类号： C07F15/0093
摘要： Disclosed herein are a platinum compound employed as raw material of medicines having carcinostatic effects, and a process of preparing the platinum compound. The platinum compound (I) substantially free from impurities can be prepared through a reaction between the corresponding dihalogen compound and an organic dibasic acid employing an iodine compound utilizing the difference of solubilities between the desired compound and the iodine compounds.
摘要翻译：本文公开了作为具有制癌作用的药物的原料的铂化合物，以及铂化合物的制备方法。基本上不含杂质的铂化合物（I）可以通过使用碘化合物的相应二卤化合物和有机二元酸之间的反应，利用所需化合物和碘化合物之间的溶解度的差异来制备。

28. 发明授权

US5023335A 1,2-bis (aminomethyl) cyclobutane-platinum complexes 失效
标题翻译： 1,2-二（氨基甲基）环丁烷 - 铂络合物
公开(公告)号：US5023335A
公开(公告)日：1991-06-11
申请号：US590610
申请日：1990-09-25
申请人： Wolfgang Schumacher , Johannes Respondek , Jurgen Engel , Jorg Pohl , Rainer Voegeli , Peter Hilgard
发明人： Wolfgang Schumacher , Johannes Respondek , Jurgen Engel , Jorg Pohl , Rainer Voegeli , Peter Hilgard
IPC分类号： A61K31/28 , A61K31/282 , A61K33/24 , A61P35/00 , C07C211/65 , C07C215/42 , C07C217/44 , C07C217/74 , C07C219/24 , C07C219/28 , C07F15/00
CPC分类号： C07F15/0093
摘要： 1,2-Bis(aminomethyl)-cyclobutane-platinum complexes having an anti-tumor activity.
摘要翻译：具有抗肿瘤活性的1,2-双（氨基甲基） - 环丁烷 - 铂络合物。

29. 发明授权

US4562275A Antitumor platinum complexes 失效
标题翻译：抗肿瘤铂复合物
公开(公告)号：US4562275A
公开(公告)日：1985-12-31
申请号：US592987
申请日：1984-03-23
申请人： Robert J. Speer , David P. Stewart
发明人： Robert J. Speer , David P. Stewart
IPC分类号： A61K31/69 , A61K31/28 , A61K31/282 , A61K31/66 , A61K31/70 , A61K31/7135 , A61P35/00 , C07C211/65 , C07F9/38 , C07F15/00 , C07H23/00 , C07F11/00
CPC分类号： C07F15/0093
摘要： Novel platinum(II) complexes of 1,2-diaminocyclohexane, 1-aminomethylcyclooctylamine and 1,2-diamino-2,4-dimethylpentane are provided. Such complexes are of use in inhibiting the growth of certain mammalian tumors.

30. 发明授权

US4235821A Hydrogenation of aliphatic nitriles to primary amines 失效
标题翻译：将脂族腈氢化成伯胺
公开(公告)号：US4235821A
公开(公告)日：1980-11-25
申请号：US8315
申请日：1979-02-01
申请人： Walter A. Butte, Jr. , William J. Murtaugh , Richard E. Mitchell
发明人： Walter A. Butte, Jr. , William J. Murtaugh , Richard E. Mitchell
IPC分类号： C07B61/00 , B01J23/00 , B01J23/46 , B01J23/74 , C07C67/00 , C07C209/00 , C07C209/44 , C07C209/48 , C07C211/03 , C07C211/65 , C07C213/00 , C07C213/02 , C07C217/08 , C07C87/14 , C07C85/12
CPC分类号： C07C209/48
摘要： In the process of hydrogenating aliphatic nitriles to primary amines whereby the nitrile is hydrogenated in a solvent system containing added ammonia using a cobalt or ruthenium catalyst, the improvement of employing an ether as solvent and carrying out the hydrogenation in the presence of water in an amount of from about 5% to about 15% by volume of the ether solvent whereby the rate of reaction is increased, and selectivity to primary amine products is increased.
摘要翻译：在将脂族腈氢化成伯胺的过程中，使用钴或钌催化剂在含有氨的溶剂体系中氢化腈，改进使用醚作为溶剂并在水存在下进行氢化为约5％至约15体积％的醚溶剂，由此反应速率增加，对伯胺产物的选择性增加。

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