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21. 发明授权

US5580994A Preparation of tetrahydropyran-4-carboxylic acid and its esters 失效
标题翻译：制备四氢吡喃-4-羧酸及其酯
公开(公告)号：US5580994A
公开(公告)日：1996-12-03
申请号：US403769
申请日：1995-03-24
申请人： Rolf Fischer , Werner Schnurr , Norbert Goetz , Thomas Kuekenhoehner
发明人： Rolf Fischer , Werner Schnurr , Norbert Goetz , Thomas Kuekenhoehner
IPC分类号： B01J21/04 , B01J21/06 , B01J23/08 , B01J23/14 , B01J23/16 , C07D309/08 , C07D493/10 , C07D309/06
CPC分类号： C07D309/08
摘要： A process for preparing tetrahydropyran-4-carboxylic acid and its esters of the formula I ##STR1## (R=H, C.sub.1 -C.sub.8 -alkyl, C.sub.3 -C.sub.8 -cycloalkyl, aryl, C.sub.7 -C.sub.12 -alkylphenyl and C.sub.7 -C.sub.12 -phenylalkyl) by reacting 2,7-dioxaspiro[4.4]nonane-1,6-dione II ##STR2## with water or alcohols IIIR--OH (III),in the presence of acidic catalysts at from 150.degree. to 350.degree. C. and from 0.01 to 100 bar.
摘要翻译： PCT No.PCT / EP93 / 03670 Sec。 371日期：1995年3月24日 102（e）1995年3月24日PCT 1993年12月23日PCT公布。第WO94 / 15931号公报日期：1994年7月21日制备四氢吡喃-4-羧酸及其式I的酯的方法（I）（R = H，C 1 -C 8 - 烷基，C 3 -C 8 - 环烷基，芳基，C 7 -C 12 - 烷基苯基和C 7 -C 12 - 苯基烷基），通过使二,7-二氧杂螺[4.4]壬烷-1,6-二酮IIIII）在酸性催化剂存在下，在150至350℃和0.01至100巴。

22. 发明授权

US5414097A Purification of esters of tetrahydro-pyran-4-carboxylic acid 失效
标题翻译：四氢 - 吡喃-4-羧酸酯的纯化
公开(公告)号：US5414097A
公开(公告)日：1995-05-09
申请号：US185179
申请日：1994-01-24
申请人： Rolf Fischer , Norbert Goetz , Thomas Kuekenhoehner , Harald Rust , Werner Schnurr
发明人： Rolf Fischer , Norbert Goetz , Thomas Kuekenhoehner , Harald Rust , Werner Schnurr
IPC分类号： C07D309/08
CPC分类号： C07D309/08
摘要： A process for purifying esters of tetrahydropyran-4-carboxylic acid of the formula I ##STR1## where R.sup.1 to R.sup.3 are each C.sub.1 -C.sub.4 -alkyl, and R.sup.2 and R.sup.3 are each additionally hydrogen, from mixtures produced in the reaction of butyrolactones of the formula II ##STR2## where R.sup.2 and R.sup.3 have the abovementioned meanings, and R.sup.4 is hydrogen, alkyl of 1-6 carbons or acyl of the formula --CO--R.sup.2, with alcohols of the formula R.sup.1 OH in the presence of oxide catalysts, by distillation, which entailsa) removing overhead, in a first column with 5-25 theoretical plates with a distillate pressure of 700-1100 mbar and a distillate temperature of 50.degree.-80.degree. C., an alcohol and up to 10% of the water,b) transferring the bottom product from the first column into a second column with 18-40 theoretical plates, into which a water entrainer is metered between plates 15 and 30, and is circulated, and which operates with a distillate pressure of 35-350 mbar and a distillate temperature of 18.degree.-70.degree. C., with the esters of tetrahydropyran-4-carboxylic acid being removed between plates 8 and 18 at 90.degree.-150.degree. C., and, where appropriate,c) feeding the bottom product from the second column into a third column with 5-25 theoretical plates, and returning the overhead products at a distillate pressure of 1-100 mbar and a distillate temperature of 90.degree.-140.degree. C. to the synthesis of the esters of tetrahydropyran-4-carboxylic acid.
摘要翻译：用于纯化式I的四氢吡喃-4-羧酸的酯的方法，其中R 1至R 3各自为C 1 -C 4 - 烷基，R 2和R 3各自为氢，其中R 2和R 3具有上述含义，R 4是氢，1-6个碳的烷基或式-CO-R 2的酰基，其中式R 1 OH的醇在存在下氧化物催化剂，通过蒸馏，其需要a）在具有5-25理论塔板的第一塔中，馏出物压力为700-1100毫巴，馏出物温度为50-80℃，醇和升高至10％的水，b）将底部产物从第一塔转移到具有18-40理论塔板的第二塔中，其中在15和30之间计量水夹带剂，并循环，并且其以馏出液压力为35-350毫巴，馏出物温度为18-70℃，其中四氢吡喃-4-羧酸的酯在90℃-150℃下在板8和18之间除去，并且在适当的情况下，c）将底部产物从第二塔进料到具有5-25理论值的第三塔将塔顶馏出物返回到馏出物压力为1-100毫巴，馏出液温度为90-140℃，以合成四氢吡喃-4-羧酸酯。

23. 发明授权

US5294639A .alpha.-arylacrylic acid derivatives, their preparation and their use for controlling pests and fungi 失效
标题翻译： α-芳基丙烯酸衍生物，它们的制备及其用于防治害虫和真菌的用途
公开(公告)号：US5294639A
公开(公告)日：1994-03-15
申请号：US754850
申请日：1991-09-04
申请人： Reinhard Kirstgen , Albrecht Harreus , Uwe Kardorff , Thomas Kuekenhoehner , Harald Rang , Gisela Lorenz , Eberhard Ammermann , Christoph Kuenast
发明人： Reinhard Kirstgen , Albrecht Harreus , Uwe Kardorff , Thomas Kuekenhoehner , Harald Rang , Gisela Lorenz , Eberhard Ammermann , Christoph Kuenast
IPC分类号： A01N37/36 , A01N37/38 , A01N43/10 , A01N43/40 , A01N43/50 , C07C69/734 , C07C69/736 , C07C205/56 , C07C255/54 , C07C255/57 , C07C323/20 , C07C323/62 , C07D213/55 , C07D233/60 , C07D237/08 , C07D237/16 , C07D239/54 , C07D241/12 , C07D241/24 , C07D249/00 , C07D249/06 , C07D261/08 , C07D277/20 , C07D277/30 , C07D307/54 , C07D333/24 , C07C69/612 , A01N37/10 , A01N37/34 , C07C69/618
CPC分类号： A01N43/40 , A01N37/36 , A01N37/38 , A01N43/10 , A01N43/50 , C07C69/734 , C07C69/736
摘要： Abstract of the Disclosure: .alpha.-Arylacrylic acid derivatives of the general formula I ##STR1## where X is ethylene or ethenylene;Y is a direct bond or oxygen;R.sup.1 is an unsubstituted or substituted mononuclear or dinuclear aromatic or heteroaromatic system;R.sup.2 is cyano, nitro, halogen, alkyl, haloalkyl, alkoxy, haloalkoxy, alkylthio or haloalkylthio;n is 1 or 2, and the radicals may be different if n is 2, and(c m is 0, 1 or 2, and the radicals may be different if m is 2,with the proviso that R.sup.1 is not phenyl when n is 1 and m is 0, their preparation, insecticides and fungicides containing them and methods for their use.
摘要翻译：公开的摘要：通式Ⅰ的α-丙烯酸衍生物（I）其中X是亚乙基或亚乙烯基; Y是直接键或氧; R1是未取代或取代的单核或双核芳族或杂芳族体系; R 2是氰基，硝基，卤素，烷基，卤代烷基，烷氧基，卤代烷氧基，烷硫基或卤代烷硫基; n为1或2，如果n为2，则基团可以不同，（cm为0,1或2，如果m为2，则基团可以不同，条件是当n为1时R1不为苯基） m为0，其制备方法，含有杀虫剂和杀真菌剂及其使用方法。

24. 发明授权

US5250553A Methyl .alpha.-arylacrylates substituted by a heterocyclic radical and their use 失效
标题翻译：被杂环基取代的α-芳基丙烯酸甲酯及其用途
公开(公告)号：US5250553A
公开(公告)日：1993-10-05
申请号：US921765
申请日：1992-07-30
申请人： Franz Schuetz , Hans-Juergen Neubauer , Thomas Kuekenhoehner , Ulrich Schirmer , Peter Hofmeister , Christoph Kuenast , Eberhard Ammermann , Gisela Lorenz , Uwe Kardorff
发明人： Franz Schuetz , Hans-Juergen Neubauer , Thomas Kuekenhoehner , Ulrich Schirmer , Peter Hofmeister , Christoph Kuenast , Eberhard Ammermann , Gisela Lorenz , Uwe Kardorff
IPC分类号： A01N43/36 , A01N43/80 , C07D207/32 , C07D207/337 , C07D261/08 , C07D261/12
CPC分类号： C07D207/337 , A01N43/36 , A01N43/80 , C07D261/08
摘要： Methyl .alpha.-arylacrylates substituted by a heterocyclic radical and having the general formula ##STR1## where R is alkyl, alkenyl, haloalkyl, cycloalkyl, alkoxy, alkylcarbonyl, alkoxycarbonyl, halogen or aryl, the aromatic ring being unsubstituted or substituted, Het is a five-membered heteroaromatic ring which is unsubstituted or substituted and has from one to three heteroatoms, and A is ethenylene, ethylene, methyleneoxy or methylenethio, and fungicides and pesticides containing these compounds.
摘要翻译：由杂环基取代并具有通式（I）的α-芳基丙烯酸甲酯，其中R是烷基，烯基，卤代烷基，环烷基，烷氧基，烷基羰基，烷氧基羰基，卤素或芳基，芳环是未取代或取代的，Het 是未被取代或被取代并具有一至三个杂原子的五元杂芳环，A是亚乙烯基，乙烯基，亚甲基氧基或亚甲硫基，以及包含这些化合物的杀真菌剂和农药。

25. 发明授权

US5194438A .alpha.-arylacrylates substituted by a trifluoromethylpyrimidinyloxy radical, fungicidal compositions and methods 失效
标题翻译：被三氟甲基嘧啶氧基取代的α-芳基丙烯酸酯，杀真菌剂和方法
公开(公告)号：US5194438A
公开(公告)日：1993-03-16
申请号：US645604
申请日：1991-01-25
申请人： Franz Schuetz , Thomas Kuekenhoehner , Jochen Wild , Hubert Sauter , Eberhard Ammermann , Gisela Lorenz
发明人： Franz Schuetz , Thomas Kuekenhoehner , Jochen Wild , Hubert Sauter , Eberhard Ammermann , Gisela Lorenz
IPC分类号： A01N43/40 , A01N43/42 , A01N43/54 , C07D213/64 , C07D213/68 , C07D213/70 , C07D213/79 , C07D213/80 , C07D213/85 , C07D215/22 , C07D215/227 , C07D215/233 , C07D215/26 , C07D215/28 , C07D215/36 , C07D215/54 , C07D239/34 , C07D239/36 , C07D239/38 , C07D239/56
CPC分类号： C07D239/56 , A01N43/40 , A01N43/42 , A01N43/54 , C07D213/64 , C07D213/68 , C07D213/70 , C07D213/79 , C07D213/80 , C07D213/85 , C07D215/227 , C07D215/233 , C07D215/26 , C07D215/28 , C07D215/36 , C07D215/54 , C07D239/34 , C07D239/36 , C07D239/38
摘要： .alpha.-Arylacrylates substituted by a heterocyclic radical and of the general formula I ##STR1## where R.sup.1 is alkoxy or alkylthio R.sup.2 is alkyl, Het is pyridyl, pyridone, quinolyl, pyrimidinyl, pyrimidinone, the heterocyclic ring system being unsubstituted or substituted, A is carbonyloxy, oxygen or sulfur, and n is 0 or 1, and their plant-tolerated acid addition salts and metal complexes, and the N-oxides of the heterocyclic compounds, and fungicides containing these compounds.
摘要翻译：由杂环基和通式I的取代基的α-丙烯酸酯，其中R1是烷氧基或烷硫基R2是烷基，Het是吡啶基，吡啶酮，喹啉基，嘧啶基，嘧啶酮，该杂环体系是未取代的或取代的，A 是羰氧基，氧或硫，n是0或1，以及它们的植物耐受酸加成盐和金属络合物，杂环化合物的N-氧化物和含有这些化合物的杀真菌剂。

26. 发明授权

US5132318A Azolymethylcycloalkyloxiranes and therir use as crop protection agents 失效
标题翻译： AZOLYMETHYLCYCLOALKYLOXIRANES并且作为作物保护剂使用
公开(公告)号：US5132318A
公开(公告)日：1992-07-21
申请号：US483279
申请日：1990-02-20
申请人： Rainer Seele , Stefan Karbach , Thomas Kuekenhoehner , Hubert Sauter , Gisela Lorenz , Eberhard Ammermann
发明人： Rainer Seele , Stefan Karbach , Thomas Kuekenhoehner , Hubert Sauter , Gisela Lorenz , Eberhard Ammermann
IPC分类号： A61L2/16 , A01N43/50 , A01N43/653 , C07D233/58 , C07D249/08 , C07D405/06 , C07D405/14 , C07D521/00
CPC分类号： C07D249/08 , A01N43/50 , A01N43/653 , C07D231/12 , C07D233/56 , C07D405/06 , C07D405/14
摘要： Azolylmethyloxiranes of the general formula I ##STR1## where A and B are cycloalkyl, tetrahydropyranyl, tetrahydrofuranyl, dioxanyl, norbornyl, cycloalkenyl or phenyl, each of these radicals being unsubstituted or substituted, with the proviso that A and B are not simultaneously phenyl, D is O, X is CH or N, and their plant-tolerated acid addition salts or metal complexes, and fungicides containing these compounds.
摘要翻译：其中A和B是环烷基，四氢吡喃基，四氢呋喃基，二恶烷基，降冰片基，环烯基或苯基，其中每个基团是未取代的或取代的，条件是A和B不同时为苯基， D是O，X是CH或N，以及它们的植物耐受酸加成盐或金属络合物，以及含有这些化合物的杀真菌剂。

27. 发明授权

US5073563A Alkoxycoumarins substituted by a heterocyclic radical, their preparation and therapeutic agents containing these compounds 失效
标题翻译：由其他化合物取代的烷氧基化物，其制备和含有这些化合物的治疗剂
公开(公告)号：US5073563A
公开(公告)日：1991-12-17
申请号：US417451
申请日：1989-10-05
申请人： Fritz-Frieder Frickel , Thomas Kuekenhoehner , Beatrice Rendenbach-Mueller , Harald Weifenbach , Hans-Juergen Teschendorf
发明人： Fritz-Frieder Frickel , Thomas Kuekenhoehner , Beatrice Rendenbach-Mueller , Harald Weifenbach , Hans-Juergen Teschendorf
IPC分类号： A61K31/335 , A61K31/41 , A61K31/44 , A61K31/443 , A61K31/4433 , A61P25/00 , C07D405/12 , C07D407/12 , C07D409/12 , C07D413/12 , C07D417/12 , C07D419/12
CPC分类号： C07D405/12 , C07D407/12 , C07D409/12 , C07D413/12 , C07D417/12
摘要： An alkoxycoumarin substituted by a heterocyclic radical, of the formula ##STR1## Het is one of the following heterocyclic radicals: where X is oxygen or sulfur.
摘要翻译：由下式杂环基取代的烷氧基香豆素：下列杂环基：其中X是氧，或者其中X是氧或硫。

28. 发明授权

US4943584A (p-Phenoxyphenoxy)-methyl-five-membered hetaryls 失效
标题翻译：（对苯氧基苯氧基） - 甲基五元杂芳基
公开(公告)号：US4943584A
公开(公告)日：1990-07-24
申请号：US184122
申请日：1988-04-20
申请人： Hans Theobald , Christoph Kuenast , Peter Hofmeister , Hans-Juergen Neubauer , Thomas Kuekenhoehner , Wolfgang Krieg , Joachim Leyendecker , Uwe Kardorff
发明人： Hans Theobald , Christoph Kuenast , Peter Hofmeister , Hans-Juergen Neubauer , Thomas Kuekenhoehner , Wolfgang Krieg , Joachim Leyendecker , Uwe Kardorff
IPC分类号： C07D233/64 , A01N43/80 , C07D207/333 , C07D207/34 , C07D231/12 , C07D231/20 , C07D231/22 , C07D233/28 , C07D233/54 , C07D249/08 , C07D261/08 , C07D261/10 , C07D261/12 , C07D263/32 , C07D263/38 , C07D271/06 , C07D271/10 , C07D275/02 , C07D277/24 , C07D307/42 , C07D333/16 , C07D333/28 , C07D333/32
CPC分类号： C07D231/12 , C07D233/28 , C07D233/64 , C07D249/08 , C07D261/08 , C07D261/10 , C07D261/12 , C07D271/06 , C07D271/10 , C07D275/02 , C07D277/24 , C07D307/42 , C07D333/16
摘要： Novel (p-phenoxyphenoxy)-methyl-five-membered heeroaromatic radicals of the formula ##STR1## where the substituents have the following meanings: R.sup.1, R.sup.2, R.sup.3 hydrogen, halogen, C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.8 -alkoxy, C.sub.1 -C.sub.4 -haloalkyl, C.sub.1 -C.sub.4 -haloalkoxy, C.sub.3 -C.sub.10 -cycloalkyl, nitro or cyano,R.sup.4 hydrogen or C.sub.1 -C.sub.4 -alkyl, and a five-membered heteroaromatic ring, and their use for combating pests.
摘要翻译：式（I）的新型（对苯氧基苯氧基） - 甲基五元环芳族基团，其中取代基具有以下含义：R 1，R 2，R 3氢，卤素，C 1 -C 8 - 烷基，C 1 -C 8 - 烷氧基，C 1 -C 4卤代烷基，C 1 -C 4卤代烷氧基，C 3 -C 10 - 环烷基，硝基或氰基，R 4氢或C 1 -C 4 - 烷基和5元杂芳环，以及它们用于防治害虫的用途。

29. 发明授权

US5378711A .alpha.-arylacrylates substituted by a heterocyclic radical, and fungicides which contain these compounds 失效
标题翻译：被杂环基取代的α-芳基丙烯酸酯和含有这些化合物的杀真菌剂
公开(公告)号：US5378711A
公开(公告)日：1995-01-03
申请号：US997521
申请日：1992-12-28
申请人： Franz Schuetz , Thomas Kuekenhoehner , Jochen Wild , Hubert Sauter , Eberhard Ammermann , Gisela Lorenz
发明人： Franz Schuetz , Thomas Kuekenhoehner , Jochen Wild , Hubert Sauter , Eberhard Ammermann , Gisela Lorenz
IPC分类号： A01N43/40 , A01N43/42 , A01N43/54 , C07D213/64 , C07D213/68 , C07D213/70 , C07D213/79 , C07D213/80 , C07D213/85 , C07D215/22 , C07D215/227 , C07D215/233 , C07D215/26 , C07D215/28 , C07D215/36 , C07D215/54 , C07D239/34 , C07D239/36 , C07D239/38 , C07D239/56 , A61K31/505 , C07D239/02
CPC分类号： C07D239/56 , A01N43/40 , A01N43/42 , A01N43/54 , C07D213/64 , C07D213/68 , C07D213/70 , C07D213/79 , C07D213/80 , C07D213/85 , C07D215/227 , C07D215/233 , C07D215/26 , C07D215/28 , C07D215/36 , C07D215/54 , C07D239/34 , C07D239/36 , C07D239/38
摘要： .alpha.-Arylacrylates substituted by a heterocyclic radical and of the general formula I ##STR1## where R.sup.1 is alkoxy or alkylthio, R.sup.2 is alkyl, Het is quinolyl, which is unsubstituted or substituted, A is oxygen and n is 1, and their plant-tolerated acid addition salts and metal complexes, and the N-oxides of the heterocyclic compounds, and fungicides containing these compounds.
摘要翻译：由杂环基和通式I的取代基的α-丙烯酸酯，其中R1是烷氧基或烷硫基，R2是烷基，Het是未被取代或取代的喹啉基，A是氧，n是1，它们的植物过硫酸加成盐和金属络合物，以及杂环化合物的N-氧化物和含有这些化合物的杀真菌剂。

30. 发明授权

US5374642A Hydroquinone diethers, their preparation and their use 失效
标题翻译：氢醌二醚，其制备及其用途
公开(公告)号：US5374642A
公开(公告)日：1994-12-20
申请号：US34649
申请日：1993-03-22
申请人： Uwe Kardorff , Christoph Nuebling , Hans Theobald , Thomas Kuekenhoehner , Hans-Juergen Neubauer , Joachim Leyendecker , Christoph Kuenast , Peter Hofmeister , Wolfgang Krieg
发明人： Uwe Kardorff , Christoph Nuebling , Hans Theobald , Thomas Kuekenhoehner , Hans-Juergen Neubauer , Joachim Leyendecker , Christoph Kuenast , Peter Hofmeister , Wolfgang Krieg
IPC分类号： A01N31/14 , A01N43/00 , A01N43/48 , A01N43/50 , A01N43/72 , A01N43/80 , A01N43/82 , A01N43/836 , C07D231/12 , C07D233/64 , C07D249/08 , C07D261/08 , C07D263/32 , C07D271/06 , C07D271/10 , C07D275/02 , C07D277/24 , C07D285/08 , C07D285/12 , C07D403/12 , C07D405/12 , C07D409/12 , C07D413/12 , C07D417/12
CPC分类号： C07D271/06 , A01N43/50 , A01N43/80 , A01N43/82 , C07D261/08 , C07D285/12 , C07D409/12 , C07D413/10 , C07D417/12
摘要： Hydroquinone diethers of the general formula I ##STR1## where R.sup.1 is hydrogen, halogen or C.sub.1 -C.sub.6 -alkyl, A and B are each unsubstituted or substituted methylene, ethylene or propylene and X and Y are each unsubstituted or substituted hetaryl, processes for their preparation and pesticides.
摘要翻译：其中R 1为氢，卤素或C 1 -C 6 - 烷基，A和B各自为未取代或取代的亚甲基，亚乙基或亚丙基，X和Y各自为未取代或取代的杂芳基的通式I的对苯二酚二醚，他们的准备和农药。

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