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21. 发明授权

US08633334B2 Method for preparing trifluoromethanesulphinic acid 有权
标题翻译：三氟甲磺酸的制备方法
公开(公告)号：US08633334B2
公开(公告)日：2014-01-21
申请号：US12744875
申请日：2008-11-25
申请人： Vincent Schanen , Olivier Buisine , François Metz , Bernard Besson
发明人： Vincent Schanen , Olivier Buisine , François Metz , Bernard Besson
IPC分类号： C07C313/04
CPC分类号： C07C313/04
摘要： The present invention relates to a method for preparing a highly pure trifluoromethanesulphinic acid. The method of the invention for preparing a highly pure trifluoromethanesulphinic acid, starting from an aqueous mixture comprising a trifluoromethanesulphinic acid salt, a trifluoroacetic acid salt and saline impurities resulting from the method for preparing same, is characterized in that said mixture is subjected to the following operations: —acidification such that the trifluoroacetic acid salt and the triflinic acid salt are released in an acid form, —separation of the trifluoroacetic acid and trifluoromethanesulphinic acid by distillation enabling the trifluoroacetic acid to be recovered at the top of the distillation and the trifluoromethanesulphinic acid to be recovered at the bottom of the distillation, —separation by distillation of the trifluoromethanesulphinic acid present in the distillation residue previously obtained.
摘要翻译：本发明涉及一种制备高纯度三氟甲磺酸的方法。本发明制备高纯度三氟甲磺酸的方法，其特征在于，由包含三氟甲磺酸盐，三氟乙酸盐和由其制备方法得到的盐水杂质的含水混合物开始，将所述混合物进行以下步骤操作：酸化使得三氟乙酸盐和三氟甲磺酸盐以酸的形式释放，通过蒸馏分离三氟乙酸和三氟甲磺酸，使得三氟乙酸在蒸馏顶部回收，并且三氟甲亚磺酸在蒸馏的底部回收，通过蒸馏先前获得的蒸馏残余物中存在的三氟甲亚磺酸分离。

22. 发明申请

US20140012033A1 METHOD FOR PREPARING DIFLUOROACETONITRILE AND THE DERIVATIVES THEREOF 有权
标题翻译：制备二氟乙酸乙酯及其衍生物的方法
公开(公告)号：US20140012033A1
公开(公告)日：2014-01-09
申请号：US14003118
申请日：2012-03-08
申请人： Olivier Buisine
发明人： Olivier Buisine
IPC分类号： C07C253/14 , C07C51/08
CPC分类号： C07C253/14 , C07C51/08 , C07C255/10
摘要： The present invention relates to a method for preparing difluoracetonitrile and the derivatives thereof. The method for preparing difluoroacetonitrile according to the invention is characterized in that it includes reacting halogenodifluoromethane and a source of cyanide anions in an alkaline medium. The invention also relates to the use of difluoroacetonitrile as an intermediate in the manufacture of difluoroacetic acid and the salts, esters, or amide thereof
摘要翻译：本发明涉及二氟乙腈及其衍生物的制备方法。根据本发明的制备二氟乙腈的方法的特征在于其包括在碱性介质中使卤代二氟甲烷和氰化物阴离子源反应。本发明还涉及二氟乙腈作为制备二氟乙酸及其盐，酯或酰胺的中间体的用途

23. 发明授权

US08524935B2 Method for preparing fluoroalkanesulphinic acid esters 有权
标题翻译：氟烷基亚磺酸酯的制备方法
公开(公告)号：US08524935B2
公开(公告)日：2013-09-03
申请号：US13266260
申请日：2010-04-29
申请人： Olivier Buisine
发明人： Olivier Buisine
IPC分类号： C07C313/04
CPC分类号： C07C313/04
摘要： A method for preparing fluoroalkanesulphinic acid esters is described. The preparation of esters of trifluoromethanesulphinic acid, commonly referred to as “triflinic acid,” is also described. A method for preparing a fluoroalkanesulphinic acid ester is also described wherein the method includes reacting a fluoroalkanesulphinic acid with an organic carbonate leading to the formation of a fluoroalkanesulphinic acid ester and carbon dioxide, which is removed during the reaction.
摘要翻译：描述了制备氟烷基亚磺酸酯的方法。还描述了通常称为“三氟酸”的三氟甲磺酸的酯的制备。还描述了制备氟烷基亚磺酸酯的方法，其中所述方法包括使氟烷基亚磺酸与有机碳酸酯反应，导致形成氟烷基亚磺酸酯和二氧化碳，其在反应期间被除去。

24. 发明申请

US20080097064A1 Method for Preparing Polyorganosiloxanes (Pos) by Ring (S) - Opening Polymerization and/or Pos Redistribution in the Presence of Carbene (S) and Pos Compounds Produced by Said Method 有权
标题翻译：在由所述方法生产的碳（S）和Pos化合物存在下通过环（S） - 开环聚合和/或位置再分布制备聚有机硅氧烷（Pos）的方法
公开(公告)号：US20080097064A1
公开(公告)日：2008-04-24
申请号：US10584774
申请日：2004-12-08
申请人： Delphine Blanc-Magnard , Sebastien Sterin , Etienne Fleury , Olivier Buisine , Antoine Baceiredo
发明人： Delphine Blanc-Magnard , Sebastien Sterin , Etienne Fleury , Olivier Buisine , Antoine Baceiredo
IPC分类号： C08G77/08
CPC分类号： C08G77/08
摘要： A method for preparing polyorganosiloxanes (POS) by a ring-opening polymerization and/or linear, non-linear or cyclic POS redistribution in the presence of a nucleophilic carbene. The initial efficiency of the POS conversion is substantially increased at low temperature, resulting in less residual content of initial POS.
摘要翻译：一种通过在亲核卡宾的存在下通过开环聚合和/或线性，非线性或循环POS再分布制备聚有机硅氧烷（POS）的方法。 POS转换的初始效率在低温下显着增加，导致初始POS的残留量较少。

25. 发明授权

US07019145B2 Method for preparing metallic carbene-based catalysts for hydrosilylation of unsaturated compounds and resulting catalysts 有权
标题翻译：制备用于不饱和化合物和所得催化剂的氢化硅烷化的金属卡宾催化剂的方法
公开(公告)号：US07019145B2
公开(公告)日：2006-03-28
申请号：US10479808
申请日：2002-06-04
申请人： Olivier Buisine , Istvan Marko , Sebastien Sterin
发明人： Olivier Buisine , Istvan Marko , Sebastien Sterin
IPC分类号： C07F15/00 , C07F7/08 , B01J31/00
CPC分类号： C07F7/1876 , C07F7/14 , C07F15/0086
摘要： The invention concerns an improved method for preparing catalysts for hydrosilylation reactions of compounds with ethylene or acetylene unsaturation (for example olefins or acetylene derivatives), in particular but not exclusively those involving polyorganosiloxanes (POS) bearing Si—H units and POS bearing Si-(ethylene or acetylene unsaturation) units. Said preparation corresponds to the following synthesis (I), wherein: A=B=carbon: T1, T2=cyclohexyl, t-butyl or methyl; T3, T4=H; DVTMS=divinyltetramethylsiloxane; t-BuOK=potassium tert-butylate; T.A=room temperature. The invention is characterised in that it consists in carrying out said synthesis in a single step by bringing together salt (III) above, Karstedt (IV) in the presence of a solvent (V) (THF) and a base (VI) (t-BuOK) at room temperature.
摘要翻译：本发明涉及一种用于制备具有乙烯或乙炔不饱和键（例如烯烃或乙炔衍生物）的化合物的氢化硅烷化反应的催化剂的改进方法，特别但不仅限于涉及含有Si-H单元的聚有机硅氧烷（POS）和承载Si-（乙烯或乙炔不饱和度）单元。所述制备对应于以下合成（I），其中：A = B =碳：T 1，T 2 =环己基，叔丁基或甲基; T 3，T 4 = H; DVTMS =二乙烯基四甲基硅氧烷; t-BuOK =叔丁醇钾; T.A =室温。本发明的特征在于其包括在溶剂（V）（THF）和碱（VI）（t）存在下将上述盐（III），Karstedt（Ⅳ） -BuOK）在室温下。

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