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21. 发明授权

US5403693A Toner aggregation and coalescence processes 失效
标题翻译：调色剂聚集和聚结过程
公开(公告)号：US5403693A
公开(公告)日：1995-04-04
申请号：US83157
申请日：1993-06-25
申请人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper
发明人： Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Michael A. Hopper
IPC分类号： G03G9/087 , G03G9/08 , G03G9/09 , G03G9/097
CPC分类号： G03G9/0815 , G03G9/0804 , G03G9/0812 , Y10S528/936
摘要： A process for the preparation of toner compositions with controlled particle size comprising:(i) preparing a pigment dispersion in water, which dispersion is comprised of a pigment, an ionic surfactant in amounts of from about 0.5 to about 10 percent by weight of water, and an optional charge control agent;(ii) shearing the pigment dispersion with a latex mixture comprised of a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant, a nonionic surfactant, and resin particles, thereby causing a flocculation or heterocoagulation of the formed particles of pigment, resin, and charge control agent;(iii) stirring the resulting sheared viscous mixture of (ii) at from about 300 to about 1,000 revolutions per minute to form electrostatically bound substantially stable toner size aggregates with a narrow particle size distribution;(iv) reducing the stirring speed in (iii) to from about 100 to about 600 revolutions per minute, and subsequently adding further anionic or nonionic surfactant in the range of from about 0.1 to about 10 percent by weight of water to control, prevent, or minimize further growth or enlargement of the particles in the coalescence step (iii); and(v) heating and coalescing from about 5 to about 50.degree. C. above about the resin glass transition temperature, Tg, which resin Tg is from between about 45.degree. C. to about 90.degree. C. and preferably from between about 50.degree. C. and about 80.degree. C. the statically bound aggregated particles to form said toner composition comprised of resin, pigment and optional charge control agent.
摘要翻译：一种用于制备具有受控粒度的调色剂组合物的方法，包括：（i）在水中制备颜料分散体，该分散体由颜料，约0.5至约10重量％的水的离子表面活性剂，和可选的电荷控制剂; （ii）用包含与所述离子表面活性剂相反电荷极性的反离子表面活性剂，非离子表面活性剂和树脂颗粒的胶体混合物剪切颜料分散体，从而引起所形成的颜料颗粒的絮凝或异凝，树脂和电荷控制剂; （iii）以约300至约1,000转/分钟搅拌得到的（ii）剪切粘稠混合物以形成具有窄粒度分布的静电粘合的基本上稳定的调色剂尺寸聚集体; （iv）将（iii）中的搅拌速度降低至约100至约600转/分钟，随后加入约0.1至约10重量％的水的其它阴离子或非离子表面活性剂以控制，或最小化在聚结步骤（iii）中的颗粒的进一步生长或增大; 和（v）在树脂玻璃化转变温度Tg以上高于约5至约50℃加热和聚结，该树脂Tg为约45℃至约90℃，优选为约50℃ C.和约80℃的静态结合聚集的颗粒以形成由树脂，颜料和任选的电荷控制剂组成的所述调色剂组合物。

22. 发明授权

US5348832A Toner compositions 失效
标题翻译：调色剂组合物
公开(公告)号：US5348832A
公开(公告)日：1994-09-20
申请号：US69792
申请日：1993-06-01
申请人： Guerino G. Sacripante , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz
发明人： Guerino G. Sacripante , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz
IPC分类号： C08G63/688 , G03G9/087
CPC分类号： C08G63/6886 , G03G9/08755
摘要： A toner composition comprised of pigment, and a sulfonated polyester of the formula or as essentially represented by the formula ##STR1## wherein M is an ion independently selected from the group consisting of hydrogen, ammonium, an alkali metal ion, an alkaline earth metal ion and a metal ion; R is independently selected from the group consisting of aryl and alkyl; R' is independently selected from the group consisting of alkyl and oxyalkylene; and wherein n and o represent random segments; and wherein the sum of n and o are equal to 100 mole percent.
摘要翻译：由颜料组成的调色剂组合物和下式的磺化聚酯或基本上由式（I）表示的其中M是独立地选自氢，铵，碱金属离子，碱土金属离子的离子和金属离子; R独立地选自芳基和烷基; R'独立地选自烷基和氧化烯; 并且其中n和o表示随机区段; 并且其中n和o的和等于100摩尔％。

23. 发明授权

US5346797A Toner processes 失效
标题翻译：墨粉处理
公开(公告)号：US5346797A
公开(公告)日：1994-09-13
申请号：US22575
申请日：1993-02-25
申请人： Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , Guerino G. Sacripante
发明人： Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , Guerino G. Sacripante
IPC分类号： G03G9/087 , G03G9/08
CPC分类号： G03G9/0804 , G03G9/0812
摘要： A process for the preparation of toner compositions comprising(i) preparing a pigment dispersion in a solvent, which dispersion is comprised of a pigment, an ionic surfactant and optionally a charge control agent;(ii) shearing the pigment dispersion with a latex mixture comprised of a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant, a nonionic surfactant and resin particles, thereby causing a flocculation or heterocoagulation of the formed particles of pigment, resin and charge control agent to form electrostatically bound toner size aggregates; and(iii) heating the statically bound aggregated particles to form said toner composition comprised of polymeric resin, pigment and optionally a charge control agent.
摘要翻译：一种制备调色剂组合物的方法，包括（i）在溶剂中制备颜料分散体，该分散体由颜料，离子表面活性剂和任选的电荷控制剂组成; （ii）用包含与所述离子表面活性剂相反电荷极性的反离子表面活性剂，非离子表面活性剂和树脂颗粒的胶体混合物剪切所述颜料分散体，从而引起所形成的颜料颗粒的絮凝或杂合，树脂和电荷控制剂以形成静电结合的调色剂尺寸聚集体; 和（iii）加热静态结合的凝集颗粒以形成由聚合树脂，颜料和任选的电荷控制剂组成的所述调色剂组合物。

24. 发明授权

US5283153A Encapsulated toner processes 失效
标题翻译：封装墨粉处理
公开(公告)号：US5283153A
公开(公告)日：1994-02-01
申请号：US868745
申请日：1992-04-15
申请人： Guerino G. Sacripante , Grazyna E. Kmiecik-Lawrynowicz , Hock S. Tan , Raj D. Patel
发明人： Guerino G. Sacripante , Grazyna E. Kmiecik-Lawrynowicz , Hock S. Tan , Raj D. Patel
IPC分类号： B01J13/14 , G03G9/08 , G03G9/093
CPC分类号： G03G9/093 , G03G9/09371 , G03G9/09392
摘要： A process for the preparation of encapsulated toner compositions which comprises dispersing a mixture of addition monomers, an optional preformed polymer resin, a free radical initiator, a colorant comprised of a pigment, dye or mixtures thereof, and shell forming monomer in an aqueous medium containing a cellulose polymer and a first ionic surfactant thereby forming a stable microdroplet suspension; and subsequently adding an aqueous solution of a second stabilizing surfactant followed by the formation of a soluble monomer forming shell wall by interfacial polymerization, and thereafter initiating and completing the core resin-forming free radical polymerization by heating thereby resulting in toner compositions with an average volume particle size of from about 3 to about 7 microns.
摘要翻译：一种制备包封的调色剂组合物的方法，其包括将添加单体的混合物，任选的预成型聚合物树脂，自由基引发剂，由颜料，染料或其混合物组成的着色剂和形成壳的单体混合在含有纤维素聚合物和第一离子表面活性剂，从而形成稳定的微滴悬浮液; 然后加入第二稳定化表面活性剂的水溶液，然后通过界面聚合形成形成壳壁的可溶性单体，然后通过加热引发和完成形成核心树脂的自由基聚合，从而得到平均体积的调色剂组合物粒径为约3至约7微米。

25. 发明授权

US5213938A Oxidation of toner compositions 失效
标题翻译：调色剂组合物的氧化
公开(公告)号：US5213938A
公开(公告)日：1993-05-25
申请号：US868810
申请日：1992-04-15
申请人： Guerino G. Sacripante , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Lurdes M. Martins
发明人： Guerino G. Sacripante , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Lurdes M. Martins
IPC分类号： G03G9/08 , G03G9/087 , G03G9/097
CPC分类号： G03G9/08777 , G03G9/0802 , G03G9/0806 , G03G9/0815 , G03G9/087 , G03G9/0872 , G03G9/09708
摘要： A process for the preparation of toner compositions which comprises the oxidation and metal chelation of the surface thereof; and a process for the preparation of toners which comprises the oxidation and metal chelation of the surface thereof, and subsequently coalescence by the absorption or sticking thereto of a fluoro containing polymer.
摘要翻译：一种制备调色剂组合物的方法，其包括其表面的氧化和金属螯合; 以及制备调色剂的方法，其包括其表面的氧化和金属螯合，随后通过吸收或粘附含氟聚合物而聚结。

26. 发明授权

US5763133A Toner compositions and processes 失效
标题翻译：调色剂组成和工艺
公开(公告)号：US5763133A
公开(公告)日：1998-06-09
申请号：US825451
申请日：1997-03-28
申请人： Beng S. Ong , Walter Mychajlowskij , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
发明人： Beng S. Ong , Walter Mychajlowskij , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
IPC分类号： G03G9/08 , G03G9/087 , G03G9/09 , G03G9/097
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08733
摘要： A process for the preparation of toner comprising (i) blending (a) an aqueous pigment dispersion containing a first ionic surfactant and an optional charge control agent with (b) a latex blend comprised of linear polymer and crosslinked polymer particles, optional nonionic surfactant and a second ionic surfactant with a charge polarity opposite to that of said first ionic surfactant in said pigment dispersion; (ii) heating the resulting mixture at about below the glass transition temperature (Tg) of the linear latex polymer to form toner sized aggregates; and (iii) subsequently heating said aggregate suspension about above the Tg of the linear latex polymer to effect fusion or coalescence of said aggregates.
摘要翻译：一种制备调色剂的方法，包括（i）将（a）含有第一离子型表面活性剂和任选的电荷控制剂的水性颜料分散体与（b）由线性聚合物和交联聚合物颗粒组成的胶乳共混物，任选的非离子表面活性剂和在所述颜料分散体中具有与所述第一离子型表面活性剂相反的电荷极性的第二离子表面活性剂; （ii）将所得混合物加热至低于线性胶乳聚合物的玻璃化转变温度（Tg），以形成调色剂尺寸的聚集体; 和（iii）随后将所述聚集体悬浮液加热至高于线性胶乳聚合物的Tg，以实现所述聚集体的熔融或聚结。

27. 发明授权

US5747215A Toner compositions and processes 失效
标题翻译：调色剂组成和工艺
公开(公告)号：US5747215A
公开(公告)日：1998-05-05
申请号：US841300
申请日：1997-04-29
申请人： Beng S. Ong , Walter Mychajlowskijj , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
发明人： Beng S. Ong , Walter Mychajlowskijj , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
IPC分类号： G03G9/08 , G03G9/087 , G03G9/09 , G03G9/097
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08733
摘要： A process for the preparation of toner comprising (i) blending (a) a colorant dispersion containing a first ionic surfactant and an optional charge control agent with (b) a latex blend comprised of linear polymer and crosslinked polymer particles, optional nonionic surfactant and a second ionic surfactant with a charge polarity opposite to that of said first ionic surfactant in said colorant dispersion; (ii) heating the resulting mixture at about below the glass transition temperature (Tg) of the linear latex polymer to form toner sized aggregates; and (iii) subsequently heating said aggregate suspension about above the Tg of the linear latex polymer to effect fusion or coalescence of said aggregates, and wherein said linear polymer is of an M.sub.w of from about 20,000 to about 40,000.
摘要翻译：一种制备调色剂的方法，包括（i）将（a）含有第一离子型表面活性剂和任选的电荷控制剂的着色剂分散体与（b）由直链聚合物和交联聚合物颗粒组成的胶乳共混物，任选的非离子表面活性剂和第二离子表面活性剂，其电荷极性与所述着色剂分散体中所述第一离子表面活性剂的极性相反; （ii）将所得混合物加热至低于线性胶乳聚合物的玻璃化转变温度（Tg），以形成调色剂尺寸的聚集体; 和（iii）随后将所述聚集体悬浮液加热至高于线性胶乳聚合物的Tg以实现所述聚集体的熔融或聚结，并且其中所述线性聚合物的Mw为约20,000至约40,000。

28. 发明授权

US5698223A Toner process 失效
标题翻译：调色剂过程
公开(公告)号：US5698223A
公开(公告)日：1997-12-16
申请号：US829551
申请日：1997-03-28
申请人： Walter Mychajlowskij , Guerino G. Sacripante , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz
发明人： Walter Mychajlowskij , Guerino G. Sacripante , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/0804 , G03G9/08768
摘要： A process for the preparation of toner comprising (i) solubilizing an imide based resin in water at pH of from about 10 to about 13 and which solubilizing is accomplished in the presence of nonionic surfactants and anionic surfactants; followed by precipitating the resulting dissolved imide resin into colloidal particles with a size diameter of from about 20 nanometers to about 500 nanometers, and which precipitating is accomplished with a high shearing device operating at a speed of from about 500 to about 2,000 revolutions per minute; acidifying the resulting mixture to a pH of from about 2 to about 4; (ii) preparing a pigment dispersion in water, which dispersion is comprised of a pigment, an oppositely charged ionic surfactant and optionally charge control agent; (iii) shearing (i) and (ii), thereby causing a flocculation of the resin, pigment, surfactants, and optional charge control agent; (iv) heating the resulting flocculent mixture of (iii) with stirring at a temperature of from about 25.degree. C. to about 1.degree. C. below the glass transition temperature (Tg) of the imide resin to effect formation of electrostatically bounded toner sized aggregates, and wherein the imide resin has a Tg of from about 45.degree. C. to about 65.degree. C.; (v) heating the resulting aggregate suspension of (iv) in the presence of additional anionic surfactant selected in an amount of from about 0.01 to about 5 weight percent based on the weight percent of the total reaction mixture solids, and which heating is at a temperature of from about 10.degree. C. to about 55.degree. C. above the Tg of the imide resin; and optionally cooling, and optionally (vi) separating said toner by washing, and thereafter drying said toner.
摘要翻译：一种制备调色剂的方法，包括（i）将酰亚胺基树脂溶解在约10至约13的pH下，并且在非离子表面活性剂和阴离子表面活性剂存在下进行增溶; 然后将所得溶解的酰亚胺树脂沉淀成尺寸直径为约20纳米至约500纳米的胶体颗粒，并且以约500至约2000转/分钟的速度运行的高剪切装置完成沉淀; 将所得混合物酸化至约2至约4的pH; （ii）在水中制备颜料分散体，该分散体由颜料，相反电荷的离子表面活性剂和任选的电荷控制剂组成; （iii）剪切（i）和（ii），从而引起树脂，颜料，表面活性剂和任选的电荷控制剂的絮凝; （iv）在低于酰亚胺树脂的玻璃化转变温度（Tg）的约25℃至约1℃的温度下搅拌加热得到的（ⅲ）絮状混合物，以形成静电有界调色剂尺寸聚集体，并且其中所述酰亚胺树脂的Tg为约45℃至约65℃。（v）在所选择的另外的阴离子表面活性剂存在下加热得到的（iv）聚集体悬浮液，其量为总反应混合物固体的重量百分比为约0.01至约5重量％，加热为温度高于酰亚胺树脂的Tg约10℃至约55℃; 并任选地冷却，并且任选地（vi）通过洗涤分离所述调色剂，然后干燥所述调色剂。

29. 发明授权

US5683848A Acrylonitrile-modified toner composition and processes 失效
标题翻译：丙烯腈改性调色剂组合物和方法
公开(公告)号：US5683848A
公开(公告)日：1997-11-04
申请号：US720736
申请日：1996-10-02
申请人： Beng S. Ong , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , Walter Mychajlowskij , David J. Sanders , T. Hwee Ng
发明人： Beng S. Ong , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , Walter Mychajlowskij , David J. Sanders , T. Hwee Ng
IPC分类号： G03G9/08 , G03G9/087 , G03G9/097
CPC分类号： G03G9/08795 , G03G9/0806 , G03G9/08711 , G03G9/08731 , G03G9/09725
摘要： A toner comprised of pigment, and an addition polymer resin generated from about 55 to about 80 weight percent of styrene, from about 1 to about 25 weight percent of acrylate, from about 1 to about 20 weight percent of acrylonitrile, and from about 0.5 to about 5 weight percent of acrylic acid.
摘要翻译：由颜料组成的调色剂和由约55至约80重量％的苯乙烯，约1至约25重量％的丙烯酸酯，约1至约20重量％的丙烯腈和约0.5至约20重量％的丙烯腈产生的加成聚合物树脂约5重量％的丙烯酸。

30. 发明授权

US5679724A Submicron particles for ink jet inks 失效
标题翻译：用于喷墨油墨的亚微米颗粒
公开(公告)号：US5679724A
公开(公告)日：1997-10-21
申请号：US536235
申请日：1995-09-29
申请人： Guerino G. Sacripante , Raj D. Patel , Marcel P. Breton , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Beng S. Ong
发明人： Guerino G. Sacripante , Raj D. Patel , Marcel P. Breton , Michael A. Hopper , Grazyna E. Kmiecik-Lawrynowicz , Beng S. Ong
IPC分类号： B41J2/01 , C08J3/03 , C08J3/215 , C09D11/00 , C08J3/02 , C08J3/05
CPC分类号： C09D11/32 , C08J3/215
摘要： An ink for ink jet printing includes an emulsifiable polymer resin and a pigment, and may be made by: (a) combining (1) an emulsion of an emulsifiable polymer resin in an anionic medium with (2) a pigment and a cationic surfactant; and (b) aggregating particles in the mixture of step (a) to a desired particle size, thereby producing a solution of aggregated particles. The particles can optionally be coalesced to alter the particle size of the particles.
摘要翻译：用于喷墨印刷的油墨包括可乳化聚合物树脂和颜料，并且可以通过以下制备：（a）将（1）阴离子介质中的可乳化聚合物树脂的乳液与（2）颜料和阳离子表面活性剂组合; 和（b）将步骤（a）的混合物中的颗粒聚集成所需的粒径，从而产生凝集颗粒的溶液。颗粒可以任选地聚结以改变颗粒的粒度。

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