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21. 发明申请

US20150106027A1 CHARACTERIZATION OF CRUDE OIL BY NMR SPECTROSCOPY 审中-公开
标题翻译：核磁共振光谱法测定原油的特征
公开(公告)号：US20150106027A1
公开(公告)日：2015-04-16
申请号：US13397273
申请日：2012-02-15
申请人： Omer Refa Koseoglu , Adnan Al-Hajji , Mohammed Abdullah Al-Ghamdi , Alexander Rebrov
发明人： Omer Refa Koseoglu , Adnan Al-Hajji , Mohammed Abdullah Al-Ghamdi , Alexander Rebrov
IPC分类号： G01N24/08 , G06F19/00 , G01N33/28 , G01R33/46
CPC分类号： G01N24/081 , G01N33/2829 , G01R33/46
摘要： A system and a method for applying 13C or 1H NMR spectroscopy to a sample of crude oil in order to calculate the cetane number, pour point, cloud point, aniline point and octane number of a gas oil fraction of the crude oil.
摘要翻译：为了计算原油粗柴油馏分的十六烷值，倾点，浊点，苯胺点和辛烷值，将13C或1 H NMR光谱法应用于原油样品的系统和方法。

22. 发明授权

US08992767B2 Ionic liquid desulfurization process incorporated in a contact vessel 有权
标题翻译：离子液体脱硫工艺结合在接触容器中
公开(公告)号：US08992767B2
公开(公告)日：2015-03-31
申请号：US13071272
申请日：2011-03-24
申请人： Omer Refa Koseoglu , Adnan Al-Hajji
发明人： Omer Refa Koseoglu , Adnan Al-Hajji
IPC分类号： C10G17/00 , C10G21/06 , C10G21/08 , C10G21/28 , C10G45/00 , C10G67/04
CPC分类号： C10G21/06 , C10G21/08 , C10G21/28 , C10G45/00 , C10G67/0463 , C10G2300/1055 , C10G2300/202 , C10G2300/207 , C10G2300/301 , C10G2300/44 , C10G2400/04
摘要： Initial high sulfur levels of a hydrocarbon feedstock are reduced to desired low levels without the need for integration of substantial new equipment or hardware with existing hydroprocessing reactors. Ionic liquids are utilized as organic sulfur extraction agents and are added to and mixed with the hydrocarbon feedstock containing organosulfur compounds downstream of an existing cold separator vessel. The ionic liquid and hydrocarbon mixture is maintained in a contact vessel under conditions which promote the formation of ionic sulfur-containing derivatives that are soluble in the ionic liquid to be formed, thereby enabling extractive removal and separation of the organosulfur compounds from the feedstock.
摘要翻译：烃原料的初始高硫含量降低到所需的低水平，而不需要将大量新设备或硬件与现有的加氢处理反应器集成。离子液体用作有机硫提取剂，并且与现有冷分离器容器下游的含有有机硫化合物的烃原料相加并混合。离子液体和烃混合物在促进形成可溶于要形成的离子液体的离子含硫衍生物的条件下保持在接触容器中，从而能够从原料中萃取除去和分离有机硫化合物。

23. 发明申请

US20100147647A1 Apparatus for upgrading whole crude oil to remove nitrogen and sulfur compounds 审中-公开
标题翻译：用于提升整个原油以除去氮和硫化合物的装置
公开(公告)号：US20100147647A1
公开(公告)日：2010-06-17
申请号：US12658660
申请日：2010-02-09
申请人： Omer Refa Koseoglu , Adnan Al-Haji , Hendrik Muller
发明人： Omer Refa Koseoglu , Adnan Al-Haji , Hendrik Muller
IPC分类号： C10G7/00
CPC分类号： C10G25/11 , C10G7/00 , C10G7/06 , C10G25/003 , C10G25/05 , C10G25/12 , C10G2300/202 , C10G2300/205
摘要： A crude oil feedstream is treated to remove or reduce the content of known undesired heteroatomic and polynuclear aromatic compounds containing nitrogen and sulfur by contacting the feedstream with one or more solid adsorbent materials selected from attapulgus clay, alumina, silica gel and activated carbon in a mixing vessel for a time that is sufficient to optimize the adsorption of the undesired compounds from the crude oil, subjecting the mixture to atmospheric flash distillation and then to vacuum flash distillation to recover presorbed boiling ranges of products having a lowered content of the undesired compounds, and preferably regenerating at least a portion of the solid adsorbent material for reuse in the process.
摘要翻译：处理原油进料流以除去或减少含有氮和硫的已知不需要的杂原子和多核芳族化合物的含量，这是通过将进料流与选自attapulgus粘土，氧化铝，硅胶和活性炭的一种或多种固体吸附剂材料在混合容器足以优化来自原油的不期望的化合物的吸附，使混合物经历大气闪蒸，然后进行真空闪蒸以回收具有降低的不期望的化合物含量的产物的沸点范围，以及优选地在该过程中再生至少一部分固体吸附剂材料以供再利用。

24. 发明授权

US09598647B2 Process for oxidative desulfurization and sulfone disposal using solvent deasphalting 有权
公开(公告)号：US09598647B2
公开(公告)日：2017-03-21
申请号：US12876636
申请日：2010-09-07
申请人： Abdennour Bourane , Omer Refa Koseoglu , Stephane Cyrille Kressmann
发明人： Abdennour Bourane , Omer Refa Koseoglu , Stephane Cyrille Kressmann
IPC分类号： C10G27/04 , C10G21/20 , C10G53/08 , C10G53/14 , C10G21/00 , C10G21/06 , C10G21/12 , C10G21/16 , C10G21/22 , C10G21/28 , C10G25/00 , C10G27/12 , C10G53/04
CPC分类号： C10G27/04 , C10G21/003 , C10G21/06 , C10G21/12 , C10G21/16 , C10G21/22 , C10G21/28 , C10G25/003 , C10G27/12 , C10G53/04 , C10G53/08 , C10G53/14 , C10G2300/202 , C10G2300/206 , C10G2300/44
摘要： A method and apparatus for upgrading a hydrocarbon feedstock is provided. The method includes the steps of (a) supplying a hydrocarbon feedstock to an oxidation reactor, wherein the hydrocarbon feedstock is oxidized in the presence of a catalyst under conditions sufficient to selectively oxidize sulfur compounds present in the hydrocarbon feedstock; (c) separating the hydrocarbons and the oxidized sulfur compounds by solvent extraction; (d) collecting a residue stream that includes the oxidized sulfur compounds; and (e) supplying the residue stream to a deasphalting unit.

25. 发明授权

US08980080B2 System and process for integrated oxidative desulfurization, desalting and deasphalting of hydrocarbon feedstocks 有权
标题翻译：碳氢化合物原料的综合氧化脱硫，脱盐和脱沥青的系统和工艺
公开(公告)号：US08980080B2
公开(公告)日：2015-03-17
申请号：US13049305
申请日：2011-03-16
申请人： Omer Refa Koseoglu , Abdennour Bourane
发明人： Omer Refa Koseoglu , Abdennour Bourane
IPC分类号： C10G53/04 , C10G53/14 , C10G31/08 , C10G27/04 , C10G27/00 , C10G33/02
CPC分类号： C10G31/08 , C10G27/00 , C10G27/04 , C10G33/02 , C10G2300/202
摘要： A system and process for integrated desulfurizing, desalting and deasphalting of hydrocarbon feedstocks is provided. A hydrocarbon feedstock, a water soluble oxidant, and a water soluble catalyst can be introduced in a oxidation zone and retained for a period of time sufficient to achieve the desired degree of desulfurization, or introduced directly into the desalting zone along with wash water. Catalyst and dissolved salt are discharged along with the wastewater effluent from the desalting zone. A hydrocarbon stream including converted hydrocarbons and oxidation by-products is passed to a deasphalting zone. In the deasphalting zone, phase separation occurs, whereby a light phase including desulfurized hydrocarbons are produced, and a heavy phase including asphaltenes and oxidation by-products are discharged, e.g., passed to an asphalt pool.
摘要翻译：提供了一种用于烃原料综合脱硫，脱盐和脱沥青的系统和方法。可将烃原料，水溶性氧化剂和水溶性催化剂引入氧化区并保持足以达到所需程度的脱硫的时间段，或者与洗涤水一起直接引入脱盐区。催化剂和溶解盐与脱盐区的废水一起排放。包含转化烃和氧化副产物的烃流被送到脱沥青区。在脱沥青区，发生相分离，由此产生包括脱硫烃的轻相，并且包括沥青质和氧化副产物的重相排出，例如通过沥青池。

26. 发明授权

US08974701B2 Integrated process for the gasification of whole crude oil in a membrane wall gasifier and power generation 有权
标题翻译：全套原油气化炉膜气化炉和发电的综合工艺
公开(公告)号：US08974701B2
公开(公告)日：2015-03-10
申请号：US13801364
申请日：2013-03-13
申请人： Omer Refa Koseoglu , Jean Pierre Ballaguet
发明人： Omer Refa Koseoglu , Jean Pierre Ballaguet
IPC分类号： C01B3/22 , F01K25/00 , C01B3/36 , C01B3/48 , C10J3/74 , F02C3/28 , C10J3/48 , C10J3/86 , C10K3/04 , C10K1/00
CPC分类号： C01B3/22 , C01B3/36 , C01B3/48 , C10J3/485 , C10J3/74 , C10J3/86 , C10J2300/0903 , C10J2300/093 , C10J2300/0959 , C10J2300/0989 , C10J2300/1653 , C10J2300/1675 , C10J2300/1678 , C10J2300/1846 , C10K1/003 , C10K3/04 , F01K25/00 , F02C3/28 , F05D2220/722 , Y02E20/18 , Y02P20/125
摘要： An integrated process for the partial oxidation of whole crude oil mixed with a low cost finely divided solid ash-producing material in a membrane wall gasification reactor produces a syngas and, optionally, a more hydrogen-rich product stream by subjecting the syngas to a water-gas shift reaction. Process steam and electricity are produced by recovering the sensible heat values from the hot syngas.
摘要翻译：在膜壁气化反应器中与低成本细碎的固体灰分产生材料混合的全部原油的部分氧化的整合方法通过使合成气经受水而产生合成气和任选地更富氢的产物流 - 加速转换反应。通过从热合成气回收显热值来生产蒸汽和电力。

27. 发明授权

US08940155B2 Ebullated-bed process for feedstock containing dissolved hydrogen 有权
标题翻译：用于含有溶解氢的原料的沸腾床方法
公开(公告)号：US08940155B2
公开(公告)日：2015-01-27
申请号：US13556343
申请日：2012-07-24
申请人： Omer Refa Koseoglu
发明人： Omer Refa Koseoglu
IPC分类号： C10G47/02 , C10G49/12 , C10G47/30 , C10G47/26 , C10G45/22 , C10G45/20
CPC分类号： C10G67/14 , B01J8/22 , B01J2208/00283 , B01J2208/00539 , C10G45/04 , C10G45/16 , C10G45/20 , C10G45/22 , C10G47/00 , C10G47/26 , C10G47/30 , C10G49/12 , C10G2300/4081 , C10G2400/02 , C10G2400/04
摘要： An improved system and method for processing feedstocks in an ebullated-bed hydroprocessing reactor is provided in which hydrogen gas is dissolved in the fresh and recycled liquid feedstock by mixing and/or diffusion of an excess of hydrogen, followed by flashing of the undissolved hydrogen upstream of the reactor inlet, introduction of the feed containing dissolved hydrogen into the ebullated-bed hydroprocessing reactor whereby the dissolved hydrogen eliminates or minimizes the prior art problems of gas hold-up and reduced operational efficiency of the recycle pump due to the presence of excess gas in the recycle stream when hydrogen gas was introduced as a separate phase into the reactor.
摘要翻译：提供了一种用于在沸腾床加氢处理反应器中处理原料的改进的系统和方法，其中通过混合和/或扩散过量的氢将氢气溶解在新鲜和再循环的液体原料中，随后闪蒸未溶解的氢气上游的反应器入口，将含有溶解氢的进料引入沸腾床加氢处理反应器中，由此由于存在过量的气体，溶解的氢消除或最小化现有技术的气体滞留问题和降低循环泵的操作效率当氢气作为单独的相引入反应器时，在循环流中。

28. 发明授权

US08821717B2 Process for upgrading hydrocarbon feedstocks using solid adsorbent and membrane separation of treated product stream 有权
标题翻译：使用固体吸附剂升级烃原料和处理产物流的膜分离的方法
公开(公告)号：US08821717B2
公开(公告)日：2014-09-02
申请号：US13331636
申请日：2011-12-20
申请人： Omer Refa Koseoglu
发明人： Omer Refa Koseoglu
IPC分类号： C10C3/08 , C10G25/05 , C10G53/08 , C10G31/09 , C10G25/06 , C10G25/12 , C10G31/11
CPC分类号： C10G25/06 , C10G25/05 , C10G25/12 , C10G31/09 , C10G31/11 , C10G53/08 , C10G2300/1033 , C10G2300/1044 , C10G2300/1055 , C10G2300/1059 , C10G2300/107 , C10G2300/1077 , C10G2300/202 , C10G2300/301 , C10G2300/44 , C10G2400/02 , C10G2400/04 , C10G2400/06
摘要： A process for upgrading hydrocarbon oil feedstreams employs a solid adsorption material to lower sulfur and nitrogen content by contacting the hydrocarbon oil, with a solid adsorbents in a mixing vessel; passing the slurry to a membrane separation zone to separate the solid adsorption material with the adsorbed sulfur and nitrogen compounds from the treated oil; recovering the upgraded hydrocarbon product having a significantly reduced nitrogen and sulfur content as the membrane permeate; mixing the solid adsorbent material with aromatic solvent to remove and stabilize the sulfur and nitrogen compounds; transferring the solvent mixture to a fractionation tower to recover the solvent, which can be recycled for use in the process; and recovering the hydrocarbons that are rich in sulfur and nitrogen for processing in a relatively small high-pressure hydrotreating unit or transferring them to a fuel oil pool for blending.
摘要翻译：一种用于升级烃油进料流的方法采用固体吸附材料以通过使烃油与固体吸附剂在混合容器中接触来降低硫和氮含量; 将浆料通入膜分离区，以将固体吸附材料与经处理的油中吸附的硫和氮化合物分离; 回收具有显着降低的氮和硫含量的升级的烃产品作为膜渗透物; 将固体吸附剂材料与芳族溶剂混合以除去和稳定硫和氮化合物; 将溶剂混合物转移到分馏塔中以回收可以再循环用于该方法的溶剂; 并回收富含硫和氮的烃，以在相对小的高压加氢处理装置中加工或将其转移到燃料油池中进行混合。

29. 发明申请

US20130199968A1 MILD HYDRODESULFURIZATION INTEGRATING GAS PHASE CATALYTIC OXIDATION TO PRODUCE FUELS HAVING AN ULTRA-LOW LEVEL OF ORGANOSULFUR COMPOUNDS 有权
标题翻译：气相加氢合成气相催化氧化生产具有超低浓度有机化合物的燃料
公开(公告)号：US20130199968A1
公开(公告)日：2013-08-08
申请号：US13741819
申请日：2013-01-15
申请人： Abdennour Bourane , Omer Refa Koseoglu , Zinfer Ismagilov , Svetlana Yashnik , Mikhail Kerzhentsev , Valentin Parmon
发明人： Abdennour Bourane , Omer Refa Koseoglu , Zinfer Ismagilov , Svetlana Yashnik , Mikhail Kerzhentsev , Valentin Parmon
IPC分类号： C10G67/12
CPC分类号： C10G67/12 , B01J23/002 , B01J23/005 , B01J23/80 , B01J23/83 , B01J35/0006 , B01J35/006 , B01J35/023 , B01J35/026 , B01J35/08 , B01J35/1014 , B01J35/1038 , B01J35/1061 , B01J37/009 , B01J37/031 , B01J2523/00 , C10G27/04 , C10G45/02 , B01J2523/17 , B01J2523/27 , B01J2523/31
摘要： Desulfurization of hydrocarbon feeds is achieved by first contacting the entire feed with a hydrodesulfurization catalyst in a hydrodesulfurization reaction zone operating under mild conditions; a flashing column downstream of the hydrodesulfurization reaction zone fractionates the effluent to obtain a first fraction which contains refractory organosulfur compounds and a second fraction that is substantially free of organosulfur compounds, since the organosulfur compounds boiling in the range of this fraction were the labile organosulfur compounds which were initially removed by mild hydrodesulfurization. The first fraction is contacted with a gaseous oxidizing agent over an oxidation catalyst having a formula CuxZn1-xAl2O4 in a gas phase catalytic oxidation reaction zone to convert the refractory organosulfur compounds to SOx and low sulfur hydrocarbons. The by-product SOx is subsequently removed, producing a stream containing a reduced level of organosulfur compounds.
摘要翻译：通过在温和条件下操作的加氢脱硫反应区中首先使整个进料与加氢脱硫催化剂接触来实现烃进料的脱硫; 在加氢脱硫反应区下游的闪烁柱对流出物进行分馏，得到含有难熔有机硫化合物的第一馏分和基本上不含有机硫化合物的第二馏分，因为在该馏分范围内沸腾的有机硫化合物是不稳定的有机硫化合物最初由轻度加氢脱硫除去。在气相催化氧化反应区中，将第一级分与具有式CuxZn1-xAl2O4的氧化催化剂上的气态氧化剂接触，以将难熔有机硫化合物转化成SOx和低硫烃。随后除去副产物SOx，产生含有降低水平的有机硫化合物的物流。

30. 发明申请

US20130062257A1 Integrated Isomerization and Hydrotreating Process 审中-公开
标题翻译：综合异构化和加氢处理工艺
公开(公告)号：US20130062257A1
公开(公告)日：2013-03-14
申请号：US13559802
申请日：2012-07-27
申请人： Omer Refa Koseoglu
发明人： Omer Refa Koseoglu
IPC分类号： C10G69/02 , B01J8/00 , B01D3/06 , C10G7/00
CPC分类号： C10G25/00 , C10G45/58 , C10G65/00 , C10G65/043 , C10G65/16 , C10G67/00 , C10G67/06 , C10G67/16 , C10G2300/1059 , C10G2300/202 , C10G2300/301
摘要： Deep desulfurization of hydrocarbon feeds containing undesired organosulfur compounds to produce a hydrocarbon product having low levels of sulfur, i.e., 15 ppmw or less of sulfur, is achieved by flashing the feed at a target cut point temperature to obtain two fractions. A low boiling temperature fraction contains refractory, sterically hindered sulfur-containing compounds, which have a boiling point at or above the target cut point temperature. A high boiling temperature fraction, having a boiling point below the target cut point temperature, is substantially free of refractory sulfur-containing compounds. The high boiling temperature fraction is contacted with isomerization catalyst, and the isomerized effluent and the low boiling temperature fraction are combined and contacted with a hydrotreating catalyst in a hydrodesulfurization reaction zone operating under mild conditions to reduce the quantity of organosulfur compounds to an ultra-low level.
摘要翻译：通过在目标切割点温度下使进料闪烁以获得两个级分来实现含有不需要的有机硫化合物的烃进料的深度脱硫以产生具有低含量硫的烃产物，即15ppmw或更少的硫。低沸点馏分含有难燃的位阻含硫化合物，其沸点等于或高于目标馏分温度。沸点低于目标切割点温度的高沸点温度馏分基本上不含难熔含硫化合物。使高沸点馏分与异构化催化剂接触，并将异构化流出物和低沸点馏分合并，并在温和条件下加氢脱硫反应区中与加氢处理催化剂接触，将有机硫化合物的量减少至超低水平。

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