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21. 发明授权

US08415520B2 Work-up of a 3-methyl-1-butene-containing mixture 失效
标题翻译：后处理含3-甲基-1-丁烯的混合物
公开(公告)号：US08415520B2
公开(公告)日：2013-04-09
申请号：US13375091
申请日：2010-04-29
申请人： Markus Winterberg , Alfred Kaizik , Armin Rix , Michael Grass , Wilfried Bueschken , Marc Becker
发明人： Markus Winterberg , Alfred Kaizik , Armin Rix , Michael Grass , Wilfried Bueschken , Marc Becker
IPC分类号： C07C7/04
CPC分类号： C07C7/04 , C07C1/24 , C07C7/06 , C07C11/10
摘要： The invention is a method for processing a mixture containing water, 3-methyl-1-butane and at least one other methylbutene. The method comprises primary distillation of the mixture, giving a gaseous primary overhead product containing methylbutene and water and a water-free primary bottom product containing 3-methyl-1-butene; condensation of the gaseous primary overhead product so as to give a condensate comprising a liquid aqueous phase and a liquid organic phase; separation of the condensate into a liquid aqueous phase and a liquid organic phase; discharge of the liquid aqueous phase; recirculation of the organic phase to the primary distillation; and finally secondary distillation of the water-free primary bottom product from the primary distillation so as to give a secondary overhead product comprising 3-methyl-1-butene and a secondary bottom product. The secondary overhead product obtained has a purity which enables it to be used directly as monomer or comonomer for preparing polymers or copolymers.
摘要翻译：本发明是一种处理含有水，3-甲基-1-丁烷和至少一种其它甲基丁烯的混合物的方法。该方法包括对该混合物进行一次蒸馏，得到含有甲基丁烯和水的气态初级塔顶馏出物和含有3-甲基-1-丁烯的无水初级底物产物; 气态一级塔顶产物的冷凝，以产生包含液态水相和液体有机相的冷凝物; 将冷凝物分离成液态水相和液体有机相; 液体水相的排出; 将有机相再循环至初级蒸馏; 最后从初级蒸馏二次蒸馏无水初级底部产物，得到包含3-甲基-1-丁烯和二级底部产物的二级塔顶产物。获得的二次塔顶产物具有使其能够直接用作制备聚合物或共聚物的单体或共聚单体的纯度。

22. 发明申请

US20120136190A1 PRODUCTION OF 3-METHYLBUT-1-EN BY MEANS OF DEHYDRATION OF 3-METHYLBUTANE-1-OL 审中-公开
标题翻译：通过3-甲基丁-1-醇脱水制备3-甲基-1-
公开(公告)号：US20120136190A1
公开(公告)日：2012-05-31
申请号：US13322527
申请日：2010-04-28
申请人： Alfred Kaizik , Thomas Quandt , Michael Grass , Markus Winterberg , Wilfried Bueschken
发明人： Alfred Kaizik , Thomas Quandt , Michael Grass , Markus Winterberg , Wilfried Bueschken
IPC分类号： C07C1/20
CPC分类号： C07C1/24 , C07C11/10
摘要： The invention relates to a process for preparing 3-methyl-1-butene by dehydration of 3-methyl-1-butanol over an aluminium-containing oxide in the temperature range from 200 to 450° C. in the gas phase or mixed liquid/gas phase, characterized in that an aluminium-containing oxide having a predominantly mesoporous pore structure whose:a) relative proportion of macropores is less than 15%;b) distribution of the pore diameter has a monomodal maximum in the range of mesopores from 3.6 to 50 nm;c) average pore diameter of all pores is in the range of mesopores and macropores from 5 to 20 nm;d) composition comprises more than 80% of gamma-aluminium oxide, is used.
摘要翻译：本发明涉及通过在气相或混合液体/液体中在200-450℃的含铝氧化物上脱水3-甲基-1-丁醇来制备3-甲基-1-丁烯的方法，气相，其特征在于具有主要介孔孔结构的含铝氧化物：a）大孔相对比例小于15％; b）孔径分布在介孔范围为3.6〜50nm的单峰最大值; c）所有孔的平均孔径在5〜20nm的介孔和大孔的范围内; d）组合物包含大于80％的γ-氧化铝。

23. 发明授权

US07632961B2 Method for the production of alicyclic polycarboxylic acid esters from partial esters of aromatic polycarboxylic acids 失效
标题翻译：从芳族多元羧酸的偏酯生产脂环族多元羧酸酯的方法
公开(公告)号：US07632961B2
公开(公告)日：2009-12-15
申请号：US10474044
申请日：2002-09-14
申请人： Wilfried Bueschken , Michael Grass , Alfred Kaizik , Dietrich Maschmeyer , Franz Nierlich , Axel Tuchlenski
发明人： Wilfried Bueschken , Michael Grass , Alfred Kaizik , Dietrich Maschmeyer , Franz Nierlich , Axel Tuchlenski
IPC分类号： C07C69/74
CPC分类号： C07C67/08 , C07C67/303 , C07C69/75
摘要： The invention relates to a process for preparing full esters of alicyclic polycarboxylic acids from partial esters of aromatic polycarboxylic acids by hydrogenation of the partial ester followed by esterification of this compound.
摘要翻译：本发明涉及通过部分酯的氢化，然后酯化该化合物，由芳族多元羧酸的偏酯制备脂环族多元羧酸的全酯的方法。

24. 发明授权

US07361714B2 Catalyst and method for hydrogenating aromatic compounds 有权
标题翻译：用于氢化芳族化合物的催化剂和方法
公开(公告)号：US07361714B2
公开(公告)日：2008-04-22
申请号：US10511595
申请日：2003-04-26
申请人： Michael Grass , Alfred Kaizik , Wilfried Bueschken , Axel Tuchlenski , Dietrich Maschmeyer , Kurt-Alfred Gaudschun , Frank Brocksien
发明人： Michael Grass , Alfred Kaizik , Wilfried Bueschken , Axel Tuchlenski , Dietrich Maschmeyer , Kurt-Alfred Gaudschun , Frank Brocksien
IPC分类号： C08C19/02
CPC分类号： B01J35/10 , B01J23/40 , B01J23/462 , B01J23/74 , B01J35/1014 , B01J35/1061 , B01J35/108 , C07C67/303 , C07C69/75
摘要： The invention relates to the hydrogenation of aromatic compounds, in particular the preparation of alicyclic polycarboxylic acids or esters of these, via ring hydrogenation of the corresponding aromatic polycarboxylic acids or esters of these, and also to catalysts suitable for this purpose.
摘要翻译：本发明涉及芳族化合物的氢化，特别是通过相应的芳族多元羧酸或它们的酯的环加氢制备脂环族多元羧酸或它们的酯，以及适用于该目的的催化剂。

25. 发明申请

US20120116140A1 WORK-UP OF A 3-METHYL-1-BUTENE-CONTAINING MIXTURE 失效
标题翻译：一种含3-甲基-1-丁烯的混合物的研究
公开(公告)号：US20120116140A1
公开(公告)日：2012-05-10
申请号：US13375091
申请日：2010-04-29
申请人： Markus Winterberg , Alfred Kaizik , Armin Rix , Michael Grass , Wilfried Bueschken , Marc Becker
发明人： Markus Winterberg , Alfred Kaizik , Armin Rix , Michael Grass , Wilfried Bueschken , Marc Becker
IPC分类号： C07C5/00 , B01D3/36 , C07C7/04 , B01D3/14
CPC分类号： C07C7/04 , C07C1/24 , C07C7/06 , C07C11/10
摘要： The invention is a method for processing a mixture containing water, 3-methyl-1-butene and at least one other methylbutene. The method comprises primary distillation of the mixture, giving a gaseous primary overhead product containing methylbutene and water and a water-free primary bottom product containing 3-methyl-1-butene; condensation of the gaseous primary overhead product so as to give a condensate comprising a liquid aqueous phase and a liquid organic phase; separation of the condensate into a liquid aqueous phase and a liquid organic phase; discharge of the liquid aqueous phase; recirculation of the organic phase to the primary distillation; and finally secondary distillation of the water-free primary bottom product from the primary distillation so as to give a secondary overhead product comprising 3-methyl-1-butene and a secondary bottom product. The secondary overhead product obtained has a purity which enables it to be used directly as monomer or comonomer for preparing polymers or copolymers.
摘要翻译：本发明是一种处理含有水，3-甲基-1-丁烯和至少一种其它甲基丁烯的混合物的方法。该方法包括对该混合物进行一次蒸馏，得到含有甲基丁烯和水的气态初级塔顶馏出物和含有3-甲基-1-丁烯的无水初级底物产物; 气态一级塔顶产物的冷凝，以产生包含液态水相和液体有机相的冷凝物; 将冷凝物分离成液态水相和液体有机相; 液体水相的排出; 将有机相再循环至初级蒸馏; 最后从初级蒸馏二次蒸馏无水初级底部产物，得到包含3-甲基-1-丁烯和二级底部产物的二级塔顶产物。获得的二次塔顶产物具有使其能够直接用作制备聚合物或共聚物的单体或共聚单体的纯度。

26. 发明授权

US08207375B2 Microporous catalyst and method for hydrogenating aromatic compounds 有权
标题翻译：微孔催化剂和芳烃化合物的加氢方法
公开(公告)号：US08207375B2
公开(公告)日：2012-06-26
申请号：US12025292
申请日：2008-02-04
申请人： Michael Grass , Alfred Kaizik , Wilfried Bueschken , Axel Tuchlenski , Dietrich Maschmeyer , Kurt-Alfred Gaudschun , Frank Brocksien
发明人： Michael Grass , Alfred Kaizik , Wilfried Bueschken , Axel Tuchlenski , Dietrich Maschmeyer , Kurt-Alfred Gaudschun , Frank Brocksien
IPC分类号： C08C19/02 , C07C51/36 , B01J35/10
CPC分类号： B01J21/063 , B01J23/40 , B01J23/462 , B01J35/10 , B01J35/1061 , B01J35/108 , B01J37/0018 , C07C51/36 , C07C67/303 , C07C2601/14 , Y02P20/582 , C07C61/135 , C07C69/75
摘要： The invention relates to the hydrogenation of aromatic compounds, in particular the preparation of alicyclic polycarboxylic acids or their esters by core hydrogenation of the corresponding aromatic polycarboxylic acids or their esters, and also to catalysts suitable therefore.
摘要翻译：本发明涉及芳族化合物的氢化，特别是通过相应的芳族多元羧酸或其酯的核心氢化制备脂环族多元羧酸或其酯，以及由此合适的催化剂。

27. 发明授权

US09353040B2 Method and device for the hydroformylation of isobutene and for the separation of the product mixture 有权
标题翻译：用于异丁烯加氢甲酰化和分离产物混合物的方法和装置
公开(公告)号：US09353040B2
公开(公告)日：2016-05-31
申请号：US14380647
申请日：2013-02-11
申请人： Goetz Baumgarten , Michael Graβ , Alfred Kaizik , Markus Winterberg , Hans-Gerd Lueken , Bart Hamers , Markus Priske , Dirk Fridag , Robert Franke , Dieter Hess
发明人： Goetz Baumgarten , Michael Graβ , Alfred Kaizik , Markus Winterberg , Hans-Gerd Lueken , Bart Hamers , Markus Priske , Dirk Fridag , Robert Franke , Dieter Hess
IPC分类号： C07C51/43 , C07C45/78 , C07C45/50 , C07C51/235 , B01D61/02 , C07C45/82
CPC分类号： C07C51/43 , B01D61/027 , C07C45/50 , C07C45/505 , C07C45/786 , C07C45/82 , C07C51/235 , C07C47/02
摘要： The invention relates to a method for producing a product mixture (2) by means of the technical hydroformylation of a hydrocarbon stream (1) that contains isobutene, and for separating the product mixture (2) that is obtained, as well as to a device for the claimed method and to the use of a claimed device. The problem addressed thereby is that of providing a method and an associated device that allow the amount of high-boiling substances in the product mixture (2) to be kept as low as possible and thus the yield of the reaction to be increased. The problem is solved by the use of a nano-filtration device (M) for separating the catalyst from the product mixture (2), said device having especially high permeability to 3-methylbutanoic acid.
摘要翻译：本发明涉及一种通过含有异丁烯的烃流（1）的技术加氢甲酰化以及用于分离获得的产物混合物（2）以及制备产物混合物（2）的方法，用于所要求保护的方法和所要求保护的装置的使用。由此提出的问题是提供一种方法和相关联的装置，其允许将产物混合物（2）中的高沸点物质的量保持尽可能低，从而提高反应的产率。通过使用纳米过滤装置（M）从产物混合物（2）中分离催化剂来解决该问题，所述装置对3-甲基丁酸具有特别高的渗透性。

28. 发明申请

US20120253083A1 METHOD FOR PRODUCING DECANOLS BY MEANS OF HYDROGENATING DECENALS 有权
标题翻译：通过氢化方法生产癸醇的方法
公开(公告)号：US20120253083A1
公开(公告)日：2012-10-04
申请号：US13502226
申请日：2010-08-13
申请人： Alfred Kaizik , Hans-Gerd Lueken
发明人： Alfred Kaizik , Hans-Gerd Lueken
IPC分类号： C07C29/141
CPC分类号： C07C29/175 , Y02P20/582 , C07C31/125
摘要： The present invention relates to a method for producing at least one decanol by means of hydrogenating at least one decenal, wherein a first hydrogenation is carried out in the liquid phase on a solid first catalyst, wherein the first catalyst contains copper and nickel. The aim of the invention is to provide a method of the type mentioned above, according to which decenals can be hydrogenated into decanols in high yields even after long operating periods. The content of non-reacted decenals in the hydrogenation discharge in particular should be less than 1500 ppm. Said aim is achieved by carrying out the hydrogenation in two steps, which is to say in a first step in a known manner using a catalyst comprising copper, nickel and optionally chromium and/or barium oxide, and subsequently in a second step using a different catalyst that must be free of copper, chromium and nickel.
摘要翻译：本发明涉及通过氢化至少一种癸醛来制备至少一种癸醇的方法，其中第一次氢化在液相中在固体第一催化剂上进行，其中第一催化剂含有铜和镍。本发明的目的是提供一种上述类型的方法，根据该方法，即使在长的操作期后，癸烯也可以高收率氢化成癸醇。氢化放电中未反应的癸醛的含量特别应小于1500ppm。所述目的通过在两步中进行氢化来实现，即在第一步中以已知方式使用包含铜，镍和任选的铬和/或氧化钡的催化剂，然后在第二步中使用不同的必须不含铜，铬和镍的催化剂。

29. 发明申请

US20120136186A1 METHOD FOR PRODUCING LOW-ODOR N-BUTANE 有权
标题翻译：生产低气味N-丁酸的方法
公开(公告)号：US20120136186A1
公开(公告)日：2012-05-31
申请号：US13381735
申请日：2010-05-21
申请人： Hans-Gerd Lueken , Alfred Kaizik , Markus Winterberg , Wilfried Büschken , Drik Fridag
发明人： Hans-Gerd Lueken , Alfred Kaizik , Markus Winterberg , Wilfried Büschken , Drik Fridag
IPC分类号： C07C5/03
CPC分类号： C07C9/10 , C07C7/10 , C07C7/163
摘要： The invention relates to a method for producing low-odor n-butane by catalytic hydrogenation of a feed mixture. The aim of the invention is to provide such a method, wherein the feed material, in addition to n-butane, n-butene and up to 1 mass % formic acid and/or up to 1 mass % pentanals and/or up to 0.5 mass % pentanols, also comprises carbon monoxide. The aim is achieved by treating the feed mixture in the temperature range of 15 to 120° C. with an aqueous solution of an alkali metal or alkaline earth metal hydroxide in the concentration range of 0.5 to 30 mass % and subsequently subjecting the feed mixture to the catalytic hydrogenation.
摘要翻译：本发明涉及通过进料混合物的催化氢化生产低气味正丁烷的方法。本发明的目的是提供这样的方法，其中除了正丁烷，正丁烯和至多1质量％的甲酸和/或至多1质量％的戊醛和/或至多0.5的进料之外，质量％戊醇还含有一氧化碳。目的是通过在0.5〜30质量％的浓度范围内用碱金属或碱土金属氢氧化物的水溶液处理15〜120℃的温度范围内的进料混合物，然后将进料混合物催化氢化。

30. 发明申请

US20120046503A1 METHOD FOR ENRICHING A HOMOGENEOUS CATALYST FROM A PROCESS FLOW 有权
标题翻译：从工艺流程中增加均质催化剂的方法
公开(公告)号：US20120046503A1
公开(公告)日：2012-02-23
申请号：US13203639
申请日：2010-02-23
申请人： Markus Priske , Goetz Baumgarten , Hans-Gerd Lueken , Alfred Kaizik , Klaus-Diether Wiese , Uwe Ernst , Patrick Muhlack
发明人： Markus Priske , Goetz Baumgarten , Hans-Gerd Lueken , Alfred Kaizik , Klaus-Diether Wiese , Uwe Ernst , Patrick Muhlack
IPC分类号： C07C29/38 , B01D61/14
CPC分类号： B01J31/4046 , B01J31/185 , B01J2231/321 , B01J2531/822
摘要： The invention relates to a method for enriching a homogenous catalyst from a process flow comprising said homogenous catalyst as a component, wherein the process flow is conducted over at least one membrane and wherein the membrane wholly or partially comprises a polymer that has planar polymer units connected to one another via a rigid link and wherein the linker is contorted, such that at least one planar polymer unit is connected to at least one second planar polymer unit via the link, in a non-co-planar arrangement. The invention furthermore relates to a method for producing tridecanal.
摘要翻译：本发明涉及从包含所述均匀催化剂作为组分的工艺流程中富集均匀催化剂的方法，其中工艺流程在至少一个膜上进行，并且其中膜完全或部分地包含连接有平面聚合物单元的聚合物通过刚性连接件彼此连接，并且其中接头被扭曲，使得至少一个平面聚合物单元以非共面布置经由连接件连接到至少一个第二平面聚合物单元。本发明还涉及一种生产十三指肠的方法。

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