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21. 发明授权

US06348529B1 Guanidine compound and heat sensitive recording material 失效
标题翻译：胍化合物和热敏记录材料
公开(公告)号：US06348529B1
公开(公告)日：2002-02-19
申请号：US09477545
申请日：2000-01-04
申请人： Naoto Yanagihara , Hisao Yamada , Mitsuyuki Tsurumi
发明人： Naoto Yanagihara , Hisao Yamada , Mitsuyuki Tsurumi
IPC分类号： C07C27700
CPC分类号： B41M5/3375 , C07C279/18
摘要： An object of the present invention is to provide a heat sensitive recording material which can develop color at high density by the inclusion of a novel guanidine compound which is strongly basic and superior in diffusion resistance. The present invention for attaining the above-described object is a heat sensitive recording material comprising a substrate supporting thereon a heat sensitive recording layer containing a diazonium salt compound, a coupler which reacts with the diazonium salt compound when heated to develop color, and abase, wherein the heat sensitive recording layer includes as the base at least one of the guanidine compounds represented by the general formula (1): wherein, in the general formula (1), R1 and R2 represent an alkyl group or aryl group and may be the same or different, R3 and R4 represent a hydrogen atom, alkyl group or halogen atom and may be the same or different, and X represents a divalent connecting group.
摘要翻译：本发明的目的是提供一种热敏记录材料，其通过包含强碱性和优异的扩散阻力的新型胍化合物，可以以高密度显色。用于实现上述目的的本发明是一种热敏记录材料，其包括在其上支撑含有重氮盐化合物的热敏记录层的基底，加热显色时与重氮盐化合物反应的成色剂，其中，所述热敏记录层包含至少一种由通式（1）表示的胍化合物作为碱的基：其中，在通式（1）中，R 1和R 2表示烷基或芳基，可以是相同或不同，R 3和R 4表示氢原子，烷基或卤素原子，可以相同或不同，X表示二价连接基团。

22. 发明授权

US06346359B1 Pyrrolopyrimidineone compound and heat-sensitive recording material using the same 失效
标题翻译：吡咯并嘧啶酮化合物和使用其的热敏记录材料
公开(公告)号：US06346359B1
公开(公告)日：2002-02-12
申请号：US09557871
申请日：2000-04-24
申请人： Hisao Yamada , Mitsuyuki Tsurumi , Kazunori Nigorikawa
发明人： Hisao Yamada , Mitsuyuki Tsurumi , Kazunori Nigorikawa
IPC分类号： G03C172
CPC分类号： C07D487/04 , B41M5/287 , G03C1/58
摘要： Disclosed are a pyrrolopyrimidineone compound represented by the following general formula (1) and a heat-sensitive recording material using the pyrrolopyrimidineone compound as a coupler: General formula (1) wherein R1 and R2 each independently represents a hydrogen atom, a halogen atom, an aryl group, an alkyl group, a cyano group, an acyl group, a carbamoyl group, an alkoxycarbonyl group, an aryloxycarbonyl group, an alkylsulfonyl group, or an arylsulfonyl group; R3 represents an amino group, a substituted amino group, a hydroxyl group, an acyloxy group, an arylcarboxyl group, an alkoxy group, an aryloxy group, an alkylthio group, or an arylthio group; R4 represents a hydrogen atom, a halogen atom, or an electron attracting group whose Hammett substituent constant &sgr;p is 0.2 or more; and L represents a substituent group which can leave when the compound reacts with a diazonium salt. The pyrrolopyrimidineone compound produces a good purple to cyan color hue and a sufficient color density.
摘要翻译：公开了由以下通式（1）表示的吡咯并嘧啶酮化合物和使用吡咯并嘧啶酮化合物作为偶联剂的热敏记录材料：通式（1）其中R 1和R 2各自独立地表示氢原子，卤素原子，芳基，烷基，氰基，酰基，氨基甲酰基，烷氧基羰基，芳氧基羰基，烷基磺酰基或芳基磺酰基; R3表示氨基，取代氨基，羟基，酰氧基，芳基羧基，烷氧基，芳氧基，烷硫基或芳硫基; R4表示氢原子，卤素原子或哈米特取代基常数sigmap为0.2以上的吸电子基团; L表示当化合物与重氮盐反应时可以离开的取代基。吡咯并嘧啶酮化合物产生良好的紫色至青色色调和足够的色密度。

23. 发明授权

US06316605B1 Hydrazone dye 有权
标题翻译：腙染料
公开(公告)号：US06316605B1
公开(公告)日：2001-11-13
申请号：US09684963
申请日：2000-10-10
申请人： Naoto Yanagihara , Tatsuo Kawabuchi , Tetsunori Matsushita , Kimiatsu Nomura , Yohsuke Takeuchi , Hisao Yamada
发明人： Naoto Yanagihara , Tatsuo Kawabuchi , Tetsunori Matsushita , Kimiatsu Nomura , Yohsuke Takeuchi , Hisao Yamada
IPC分类号： C09B2602
CPC分类号： C09B26/02
摘要： A hydrazone dye is provided which forms cyan color having an excellent hue. The hydrazone dye is expressed by the following general formula (I): wherein Ar represents an aryl group or a heterocyclic group; R1 through R4 each represent a hydrogen atom, a halogen, —CN, —NH2, —NO2, —OH, —CO2H, —SO3H, a quaternary ammonium group, —CO2M1/n, —SO3M1/n, an alkyl group, alkenyl group, alkynyl group, aryl group, acyl group, carbamoyl group, sulfamoyl group, alkoxycarbonyl group, aryloxycarbonyl group, acyloxy group, alkoxy group, aryloxy group, alkylthio group, arylthio group, alkylsulfonyl group, arylsulfonyl group, alkylphosphoryl group, arylphosphoryl group, or a substituted amino group; M represents a metal atom; and n represents an integer from 1 to 4.
摘要翻译：提供了形成具有优异色调的青色的腙染料。腙染料由以下通式（I）表示：其中Ar表示芳基或杂环基; R 1至R 4各自表示氢原子，卤素，-CN，-NH 2，-NO 2，-OH，-CO 2 H，-SO 3 H，季铵基，-CO 2 M 1 / n，-SO 3 M 1 / n，烷基，酰基，氨基甲酰基，氨磺酰基，烷氧基羰基，芳氧基羰基，酰氧基，烷氧基，芳氧基，烷硫基，芳硫基，烷基磺酰基，芳基磺酰基，烷基磷酰基，芳基磷酰基，或取代的氨基; M表示金属原子; n表示1〜4的整数。

24. 发明授权

US06197725B1 Heat-sensitive recording material 有权
标题翻译：热敏记录材料
公开(公告)号：US06197725B1
公开(公告)日：2001-03-06
申请号：US09201807
申请日：1998-12-01
申请人： Atsuhiro Ohkawa , Hisao Yamada
发明人： Atsuhiro Ohkawa , Hisao Yamada
IPC分类号： B41M528
CPC分类号： G03C1/58 , G03C1/002
摘要： There is provided a coupler giving a magenta pigment excellent in hue using a diazonium salt compound which can be fixed at a wavelength around 420 nm. A heat-sensitive recording material comprising a substrate carrying thereon a heat-sensitive recording layer containing a diazonium salt compound and a coupler which develops color by reacting with said diazonium salt compound in heating, wherein said coupler comprises at least one compound represented by the following general formula (1):
摘要翻译：提供了使用可以固定在约420nm波长的重氮盐化合物，得到色调优异的品红色颜料的成色剂。一种热敏记录材料，其特征在于，在加热时，含有含有重氮盐化合物的热敏记录层和通过与所述重氮盐化合物反应而显色的成色剂的基板，其中所述成色剂包含至少一种下述化合物通式（1）：

25. 发明授权

US4925609A Oxygen-sensing element 失效
标题翻译：氧传感元件
公开(公告)号：US4925609A
公开(公告)日：1990-05-15
申请号：US182547
申请日：1988-04-18
申请人： Hisao Yamada , Thomas Yuan
发明人： Hisao Yamada , Thomas Yuan
IPC分类号： C04B33/32 , G01N27/407 , G01N27/416
CPC分类号： G01N27/407
摘要： An oxygen-sensing element particularly for use in the exhaust stream of an internal combustion engine. In one embodiment, the sensing element may be a tubular solid electrolyte body with a transverse web forming a relatively shallow recess at one end of the body and a relatively deep tube at the other. Separate electrodes are formed on the surface of the body proximate the recess and on both opposing sides of the web. A porous plug disposed in the recess covers one of the electrodes. When the electrode on the surface of the body is exposed to the exhaust stream of a fuel-rich air-fuel mixture, the EMF across that electrode and the electrode on the underside of the web, which is exposed to fresh air, is indicative of the oxygen content of the exhaust stream. When an exhaust stream from a fuel-lean air-fuel mixture is present, the magnitude of an oxygen pumping current that flows between the electrodes disposed on opposing sides of the web, in response to a voltage applied across those electrodes, indicates the oxygen content of the exhaust stream.The sensing element body may be conveniently formed from a slip prepared by ball milling yttria-stabilized zirconia powder with water and a binder. The slip may be cast in a mold or dried to form a flowable powder that is molded under pressure to form a green body. After calcining of the green body, electrodes are formed on the body by applying a platinum paste and heating it. A slurry of ball-milled calcined yttria-stabilized zirconia powder is disposed in the recess. The calcined green body and slurry are fired to produce a sensing element in which a tightly fitting porous plug, free of cracks and shrinkage away from the body, is disposed in the recess.
摘要翻译：一种特别用于内燃机排气流的氧气感测元件。在一个实施例中，感测元件可以是管状固体电解质体，其横向腹板在主体的一端形成相对浅的凹部，而在另一端形成相对较深的管。单独的电极形成在靠近凹槽的本体的表面上并且在幅材的两个相对侧上。设置在凹部中的多孔塞覆盖电极中的一个。当身体表面上的电极暴露于富燃料空气 - 燃料混合物的排气流时，穿过该电极的EMF和暴露于新鲜空气的幅材下侧的电极表示排气流的氧含量。当存在来自贫燃料的空气燃料混合物的废气流时，响应于施加在这些电极上的电压而在布置在幅材的相对侧上的电极之间流动的氧气抽吸电流的大小表示氧含量的排气流。感测元件主体可以方便地由球磨氧化钇稳定的氧化锆粉末与水和粘合剂制成的滑块形成。滑块可以在模具中铸造或干燥以形成在压力下成型以形成生坯体的可流动粉末。在生坯体煅烧后，通过施加铂膏并加热电极，在体上形成电极。将球磨的煅烧氧化钇稳定的氧化锆粉末的浆料设置在凹槽中。煅烧的生坯和浆料被烧制以产生感测元件，其中紧密配合的多孔塞没有裂缝和远离体的收缩被布置在凹槽中。

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