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21. 发明申请

US20080281117A1 POLYCYCLIC HYDROCARBON GROUP-CONTAINING ORGANOSILICON COMPOUND HAVING HYDROGEN ATOMS BONDED TO SILICON ATOMS, AND METHOD OF PRODUCING SAME 审中-公开
标题翻译：含有氢原子的多环碳氢化合物有机硅化合物与其生成相同的方法
公开(公告)号：US20080281117A1
公开(公告)日：2008-11-13
申请号：US12115835
申请日：2008-05-06
申请人： Eiichi Tabei
发明人： Eiichi Tabei
IPC分类号： C07F7/08
CPC分类号： C07F7/0896 , C08G77/60
摘要： Provided is a polycyclic hydrocarbon group-containing organosilicon compound, which includes two hydrogen atoms bonded to silicon atoms within each molecule, and is an addition reaction product of (a) an organosilicon compound having two hydrogen atoms bonded to silicon atoms within each molecule, and (b) a polycyclic hydrocarbon compound having two hydrosilylation reactive carbon-carbon double bonds within each molecule. The polycyclic hydrocarbon group-containing organosilicon compound is produced by conducting an addition reaction between the above component (a) and the above component (b) in the presence of a hydrosilylation reaction catalyst. The polycyclic hydrocarbon group-containing organosilicon compound yields a cured product that has a high degree of hardness and excellent transparency, crack resistance and heat resistance, and is useful as a raw material for curable silicone materials, encapsulating materials for optical devices such as optical elements, encapsulating materials for other electronic devices such as semiconductor elements, and electrically insulating coating materials.
摘要翻译：提供含有多环烃基的有机硅化合物，其包含在每个分子内与硅原子键合的两个氢原子，并且是（a）在每个分子内具有与硅原子键合的两个氢原子的有机硅化合物的加成反应产物，以及（b）在每个分子内具有两个氢化硅烷化反应性碳 - 碳双键的多环烃化合物。通过在氢化硅烷化反应催化剂的存在下，通过在上述组分（a）和上述组分（b）之间进行加成反应来制备含有多环烃基的有机硅化合物。含有多环烃基的有机硅化合物产生硬度高，透明度高，耐裂纹性和耐热性优异的固化物，可用作可固化硅酮材料的原料，光学元件等的光学元件的封装材料，用于诸如半导体元件的其它电子器件的封装材料和电绝缘涂层材料。

22. 发明授权

US07291691B2 Curable silicone resin composition 有权
标题翻译：可固化硅树脂组合物
公开(公告)号：US07291691B2
公开(公告)日：2007-11-06
申请号：US10917280
申请日：2004-08-13
申请人： Eiichi Tabei , Akira Yamamoto
发明人： Eiichi Tabei , Akira Yamamoto
IPC分类号： C08G77/12
CPC分类号： C08G77/50 , C08G77/42 , C08L83/10 , C08L83/00
摘要： Provided is a curable silicone resin composition including (A) a siloxane/polycyclic hydrocarbon-based compound containing at least 2 silicon-bonded hydrogen atoms, which is an addition reaction product of (a) a siloxane-based compound with at least 3 silicon-bonded hydrogen atoms, and (b) a polycyclic hydrocarbon with at least 2 addition reactive carbon-carbon double bonds, (B) a siloxane-based compound containing at least 2 silicon-bonded alkenyl groups, and (C) a hydrosilylation reaction catalyst. This composition is useful as a material for optical devices or parts, insulation material for electronic devices or parts, or coating material.
摘要翻译：提供一种可固化的有机硅树脂组合物，其包含（A）含有至少2个与硅键合的氢原子的硅氧烷/多环烃基化合物，其是（a）硅氧烷基化合物与至少3个硅键合氢原子的加成反应产物，和（b）具有至少2个加成反应性碳 - 碳双键的多环烃，（B）含有至少2个与硅键合的烯基的硅氧烷基化合物，和（C）氢化硅烷化反应催化剂。该组合物可用作光学器件或部件的材料，电子器件或部件的绝缘材料或涂层材料。

23. 发明申请

US20050061437A1 Curable silicone resin composition 有权
标题翻译：可固化硅树脂组合物
公开(公告)号：US20050061437A1
公开(公告)日：2005-03-24
申请号：US10942837
申请日：2004-09-17
申请人： Tomoyuki Goto , Eiichi Tabei , Akira Yamamoto
发明人： Tomoyuki Goto , Eiichi Tabei , Akira Yamamoto
IPC分类号： C08L83/07 , C08K5/5419 , C08L83/04 , C08L83/05 , G03F7/075 , C09J1/00
CPC分类号： G03F7/0757 , C08G77/12 , C08G77/16 , C08G77/18 , C08G77/20 , C08G77/70 , C08K5/54 , C08K5/5403 , C08K2201/014 , C08L83/04 , C08L83/00
摘要： A curable silicone resin composition is provided. It includes (A) an aromatic ring-containing hydrocarbon compound containing at least 2 silicon-bonded hydrogen atoms, in which the silicon atoms are bonded to the hydrocarbon skeleton; (B) an organopolysiloxane with a branched or three dimensional network structure, and with a viscosity at 25° C. of at least 1,000 mPa·s, having an average composition formula (1): R1xSiO{(4−x)2} (1) wherein, R1 independently represent a substituted or unsubstituted monovalent hydrocarbon group, a substituted or unsubstituted hydrocarbyloxy group, or a hydroxyl group, provided from 0.1 to 80 mol % of all the R1 groups are alkenyl groups, and x represents a positive number that satisfies 1≦x
摘要翻译：提供可固化的有机硅树脂组合物。它包括（A）含有至少2个与硅键合的氢原子的含芳环的烃化合物，其中硅原子键合到烃骨架上; （B）具有支链或三维网状结构的有机聚硅氧烷，并且在25℃下的粘度为至少1,000mPa.s，具有平均组成式（1）：R 1 x SiO（{ ）2}（1）其中，R 1独立地表示取代或未取代的一价烃基，取代或未取代的烃氧基或羟基，所述R 1基团的全部为0.1〜80摩尔％烯基，x表示满足1 <= x <2的正数; 和（C）氢化硅烷化反应催化剂。该组合物产生透明的固化产物并显示出优异的硬度和弯曲强度。

24. 发明授权

US5403943A Chloro-terminated polysilane 失效
标题翻译：氯封端聚硅烷
公开(公告)号：US5403943A
公开(公告)日：1995-04-04
申请号：US125859
申请日：1993-09-24
申请人： Eiichi Tabei , Shigeru Mori
发明人： Eiichi Tabei , Shigeru Mori
IPC分类号： C07F7/12 , C08G77/60 , C07F7/08
CPC分类号： C07F7/12 , C07F7/123 , C08G77/60
摘要： The invention provides a novel chloro-terminated polysilane of the formula:Cl[(R.sup.1 R.sup.2 Si).sub.n (R.sup.3 R.sup.4 Si).sub.m ].sub.k Cl(1)wherein R.sup.1, R.sup.2 and R.sup.3 are alkyl and aryl groups, R.sup.4 is a monovalent hydrocarbon group having 2 to 12 carbon atoms selected from substituted and unsubstituted alkyl and aryl groups, n, m and k are numbers in the range: 0.ltoreq.n.ltoreq.10, 0
摘要翻译：本发明提供了一种新颖的具有下式的氯端基聚硅烷：Cl [（R1R2Si）n（R3R4Si）m] kCl（1）其中R1，R2和R3是烷基和芳基，R4是具有2-12个碳原子的一价烃基选自取代和未取代的烷基和芳基的碳原子，n，m和k是以下范围内的数字：0≤n≤10,0≤m≤10，n + m> = 10，以及 k> / = 1，特别是k> = 5。通过将高分子量聚硅烷在氯化烃中暴露于惰性气体气氛中的紫外线辐射来制备。

25. 发明授权

US5292415A Chloro-terminated polysilane and process for making 失效
标题翻译：氯端基聚硅烷及其制备方法
公开(公告)号：US5292415A
公开(公告)日：1994-03-08
申请号：US6487
申请日：1993-01-21
申请人： Shigeru Mori , Eiichi Tabei , Hisashi Umehara
发明人： Shigeru Mori , Eiichi Tabei , Hisashi Umehara
IPC分类号： C07F7/12 , C08G77/60 , C07F7/08 , C07B9/00
CPC分类号： C08G77/60 , C07F7/12 , C07F7/123
摘要： The invention provides a novel chloro-terminated polysilane of the formula:Cl[(R.sup.1 R.sup.2 Si)n (R.sup.3 R.sup.4 Si)m]kCl (1)wherein R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are alkyl and aryl groups, n, m and k are numbers in the range: 0.ltoreq.n.ltoreq.10, 0.ltoreq.m.ltoreq.10, n+m.gtoreq.10, and k.gtoreq.1, especially k.gtoreq.5. It is prepared by exposing a high-molecular weight polysilane in chlorinated hydrocarbon to ultraviolet radiation in an inert gas atmosphere.
摘要翻译：本发明提供了下式的新型氯封端聚硅烷：Cl [（R1R2Si）n（R3R4Si）m] kCl（1）其中R1，R2，R3和R4是烷基和芳基，n，m和k是范围：0 / = 10，k> / = 1，特别是k> = 5。通过将高分子量聚硅烷在氯化烃中暴露于惰性气体气氛中的紫外线辐射来制备。

26. 发明授权

US5286891A Hydroxy-terminated polysilane and process for making 失效
标题翻译：羟基封端的聚硅烷和制备方法
公开(公告)号：US5286891A
公开(公告)日：1994-02-15
申请号：US6482
申请日：1993-01-21
申请人： Eiichi Tabei , Shigeru Mori
发明人： Eiichi Tabei , Shigeru Mori
IPC分类号： C07F7/08 , C07F7/12 , C08G77/48 , C08G77/60
CPC分类号： C07F7/12 , C07F7/0821 , C07F7/0836 , C08G77/60
摘要： The invention provides a novel hydroxy terminated polysilane of the formula:OH[(R.sup.1 R.sup.2 Si).sub.n (R.sup.3 R.sup.4 Si).sub.m ].sub.k OHwherein R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are alkyl or aryl groups, n, m and k are numbers in the range: 0.ltoreq.n.ltoreq.10, 0.ltoreq.m.ltoreq.10, n+m.gtoreq.10, and k.gtoreq.1, especially k.gtoreq.5. It is prepared by hydrolyzing a chloro- terminated polysilane.
摘要翻译：本发明提供了下式的羟基封端的聚硅烷：OH [（R 1 R 2 Si）n（R 3 R 4 Si）m] k OH其中R 1，R 2，R 3和R 4是烷基或芳基，n，m和k是在0 / = 10，k> / = 1，特别是k> = 5。通过水解氯代封端的聚硅烷制备。

27. 发明申请

US20070104872A1 METHOD OF SEALING SEMICONDUCTOR ELEMENT MOUNTED ON GOLD-PLATED PRINTED CIRCUIT BOARD 有权
标题翻译：在镀金电镀板上密封半导体元件的方法
公开(公告)号：US20070104872A1
公开(公告)日：2007-05-10
申请号：US11557249
申请日：2006-11-07
申请人： Eiichi Tabei , Hideyoshi Yanagisawa
发明人： Eiichi Tabei , Hideyoshi Yanagisawa
IPC分类号： B05D3/10 , C08L83/04 , B32B27/00
CPC分类号： C08L83/06 , H01L23/296 , H01L23/3142 , H01L33/56 , H01L2924/0002 , H01L2924/00
摘要： Methods of sealing a semiconductor element are provided. The methods includes the steps of coating a semiconductor element mounted on a gold-plated printed circuit board with a curable silicone resin, and then curing the curable silicone resin. In a method, the gold-plated printed circuit board is subjected to preliminary treatment with a treatment agent including an acid anhydride group-containing alkoxysilane and/or a partial hydrolysis-condensation product thereof In another method, the curable silicone resin includes the treatment agent. The methods yield favorable adhesion upon sealing.
摘要翻译：提供密封半导体元件的方法。所述方法包括以下步骤：用可固化的硅树脂涂覆安装在镀金印刷电路板上的半导体元件，然后固化可固化的硅树脂。在一种方法中，使用包含含酸酐基团的烷氧基硅烷和/或部分水解缩合产物的处理剂对镀金印刷电路板进行预处理。另一种方法中，可固化有机硅树脂包括处理剂。该方法在密封时产生良好的附着力。

28. 发明授权

US07176270B2 Curable composition 有权
标题翻译：可固化组合物
公开(公告)号：US07176270B2
公开(公告)日：2007-02-13
申请号：US10960048
申请日：2004-10-08
申请人： Eiichi Tabei
发明人： Eiichi Tabei
IPC分类号： C08G77/50
CPC分类号： C08G77/50 , C08G77/045 , C08G77/12 , C08G77/18 , C08G77/485 , C08L83/04
摘要： Provided is a curable composition including (A) an addition reaction product of (a) a compound with 2 silicon atom-bonded hydrogen atoms within each molecule, having a general formula (1): wherein, A is a bivalent group represented by a formula (2): (wherein, R′ represents an unsubstituted or substituted monovalent hydrocarbon group of 1 to 12 carbon atoms, or an alkoxy group of 1 to 6 carbon atoms, and n represents an integer from 0 to 100), or a group having a structural formula (3): and each R represents an unsubstituted or substituted monovalent hydrocarbon group of 1 to 12 carbon atoms, or an alkoxy group of 1 to 6 carbon atoms, and (b) a polycyclic hydrocarbon with 2 addition reactive carbon-carbon double bonds within each molecule, said addition reaction product containing at least two addition reactive carbon-carbon double bonds in each molecule, (B) a compound with at least 3 silicon atom-bonded hydrogen atoms within each molecule, and (C) a hydrosilylation reaction catalyst. This composition is useful as a material for optical devices or parts, insulation material for electronic devices or parts, or coating material.
摘要翻译：本发明提供一种可固化组合物，其包含（A）具有通式（1）的（a）在每个分子内具有2个硅原子键合的氢原子的化合物的加成反应产物：其中A是由式（2）表示：（其中，R'表示1〜12个碳原子的未取代或取代的1价烃基或1〜6个碳原子的烷氧基，n表示0〜100的整数）或具有结构式（3）表示：R表示1〜12个碳原子的未取代或取代的一价烃基或碳原子数1〜6的烷氧基，（b）具有2个加成反应性碳 - 碳的多环烃每个分子中的双键，所述加成反应产物在每个分子中含有至少两个加成反应性碳 - 碳双键，（B）在每个分子内具有至少3个与硅原子键合的氢原子的化合物，和（C）氢化硅烷化反应催化剂。该组合物可用作光学器件或部件的材料，电子器件或部件的绝缘材料或涂层材料。

29. 发明授权

US5905139A Purification of polysilane 失效
标题翻译：聚硅烷的纯化
公开(公告)号：US5905139A
公开(公告)日：1999-05-18
申请号：US992964
申请日：1997-12-18
申请人： Shigeru Mori , Eiichi Tabei , Kazumi Noda
发明人： Shigeru Mori , Eiichi Tabei , Kazumi Noda
IPC分类号： C08G77/34 , C08G77/60 , C08F6/00
CPC分类号： C08G77/34 , C08G77/60
摘要： A polysilane containing insoluble matter and microgel as impurities is purified by dissolving the polysilane in a good solvent to form a polysilane solution, adding a poor solvent to the polysilane solution for causing a minor amount of high molecular weight component to precipitate, thereby agglomerating the insoluble matter and microgel, and removing the resulting agglomerate by filtration. The purifying method of the invention can readily remove the insolubles from the starting polysilane within a short time. A pure polysilane which can form a transparent smooth film is obtainable with commercial advantages.
摘要翻译：通过将聚硅烷溶解在良溶剂中以形成聚硅烷溶液，将聚硅烷溶解于聚硅烷溶液中，使少量高分子量组分沉淀，从而使不溶性物质和微凝胶作为杂质沉淀物质和微凝胶，并通过过滤除去所得的附聚物。本发明的净化方法可以在短时间内容易地从起始聚硅烷中除去不溶物。可以获得商业上的优点，可以形成透明光滑膜的纯聚硅烷。

30. 发明授权

US5804257A Polysilane compositions 失效
标题翻译：聚硅烷组合物
公开(公告)号：US5804257A
公开(公告)日：1998-09-08
申请号：US466278
申请日：1995-06-06
申请人： Akira Hayashida , Shigeru Mori , Eiichi Tabei
发明人： Akira Hayashida , Shigeru Mori , Eiichi Tabei
IPC分类号： C08K5/10 , C09D183/16 , D06P3/00 , D06P5/20 , G02B5/22 , G03F7/075 , C08K5/101 , B05D3/06
CPC分类号： G03F7/0754 , C08K5/10 , C09D183/16 , D06P3/002 , D06P5/2005 , G02B5/22
摘要： A polysilane composition including a polysilane and a plasticizer can be coated as a thin film having improved mechanical strength and a high photo decomposition rate. A polysilane composition including a polysilane and an ester can be coated as a thin film which is exposed to UV and readily dyed to form a dyed polysilane film.
摘要翻译：可以将包含聚硅烷和增塑剂的聚硅烷组合物涂布为具有改善的机械强度和高分解率的薄膜。可以将包含聚硅烷和酯的聚硅烷组合物作为薄膜进行涂布，所述薄膜暴露于紫外线并易于染色以形成染色的聚硅烷膜。

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