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21. 发明授权

US06613860B1 Compositions comprising fluorinated polyether silanes for rendering substrates oil and water repellent 有权
标题翻译：包含氟化聚醚硅烷的组合物，用于使底物油和憎水性
公开(公告)号：US06613860B1
公开(公告)日：2003-09-02
申请号：US09689013
申请日：2000-10-12
申请人： Rudolf J. Dams , Franceska M. Fieuws , Steven J. Martin , Michael S. Terrazas , Mark J. Pellerite
发明人： Rudolf J. Dams , Franceska M. Fieuws , Steven J. Martin , Michael S. Terrazas , Mark J. Pellerite
IPC分类号： C08G7760
CPC分类号： C04B41/009 , C03C17/30 , C04B41/4933 , C04B41/84 , C08G65/007 , C08G65/336 , C04B41/46 , C04B41/463 , C04B41/502 , C04B33/00
摘要： The present invention provides composition for treating a substrate comprising a homogeneous mixture of: (a) a fluorinated polyether silane of the formula: Rf1—[—Q—SiY3−xR1x]y (I) wherein Rf1 represents a monovalent or divalent polyfluoropolyether group, Q represents an organic divalent linking group, R1 represents a C1-C4 alkyl group, Y represents a hydrolysable group; x is 0 or 1 and y is 1 or 2; (b) an organic or an inorganic acid; (c) water; and (d) an organic solvent. The invention further provides a method of making such a composition and the use thereof to treat substrates to render them oil and water repellent.
摘要翻译：本发明提供了一种用于处理底物的组合物，其包含以下均匀混合物：（a）下式的氟化聚醚硅烷：其中Rf1表示一价或二价多氟聚醚基团，Q表示有机二价连接基团，R1表示C1-C4 烷基，Y表示可水解基团; x为0或1，y为1或2;（b）有机或无机酸;（c）水; 和（d）有机溶剂。本发明还提供了一种制备这种组合物的方法及其用途来处理基材以使其具有防水和防水性。

22. 发明授权

US08633288B2 Fluorinated ether compounds and methods of using the same 失效
标题翻译：氟化醚化合物及其使用方法
公开(公告)号：US08633288B2
公开(公告)日：2014-01-21
申请号：US13054601
申请日：2009-07-15
申请人： Rudolf J. Dams , Michael S. Terrazas , Klaus Hintzer , Zai-Ming Qiu , Miguel A. Guerra , Andreas R. Maurer , Harald Kaspar , Kai H. Lochhaas , Michael Juergens , Tilman C. Zipplies , Werner Schwertfeger
发明人： Rudolf J. Dams , Michael S. Terrazas , Klaus Hintzer , Zai-Ming Qiu , Miguel A. Guerra , Andreas R. Maurer , Harald Kaspar , Kai H. Lochhaas , Michael Juergens , Tilman C. Zipplies , Werner Schwertfeger
IPC分类号： C08F4/44
CPC分类号： C07C235/10 , C07C69/708 , C07C211/11 , C07C211/14 , C07C291/04 , C07C309/14 , C07F9/091 , C07F9/3808 , C08G65/007
摘要： Compounds represented by formula (Rf-Q-X)s—Z. Each Rf is independently a partially fluorinated or fully fluorinated group selected from Rfa-(O)r—CHF—(CF2)n—; [Rfb-(O)tC(L)H—CF2—O]m—W—; CF3CFH—O—(CF2)p—; CF3—(O—CF2)z—; and CF3—O—(CF2)3—O—CF2—. Methods of reducing surface tension of a liquid, making foams, and treating a surface using the compounds are also disclosed.
摘要翻译：由式（Rf-Q-X）s-Z表示的化合物。每个Rf独立地是选自Rfa-（O）r -CHF-（CF 2）n - 的部分氟化或完全氟化基团; [Rfb-（O）tC（L）H-CF2-O] m -W-; CF 3 CFH-O-（CF 2）p-; CF 3 - （O-CF 2）z - ; 和CF 3 -O-（CF 2）3 -O-CF 2 - 。还公开了降低液体的表面张力，制造泡沫以及使用该化合物处理表面的方法。

23. 发明申请

US20100233492A1 COMPOSITIONS FOR AQUEOUS DELIVERY OF FLUORINATED OLIGOMERIC SILANES 失效
标题翻译：氟化低聚硅烷的水分输送组合物
公开(公告)号：US20100233492A1
公开(公告)日：2010-09-16
申请号：US12784892
申请日：2010-05-21
申请人： Rudolf J. Dams , Mark J. Pellerite , Steven J. Martin , Michael S. Terrazas
发明人： Rudolf J. Dams , Mark J. Pellerite , Steven J. Martin , Michael S. Terrazas
IPC分类号： B32B17/10 , C08G18/42 , B05D3/10 , C08K5/05 , C08K5/3415 , C08K5/20 , C08K5/07 , C08K5/06 , C08K5/02 , C08L83/00 , B32B18/00
CPC分类号： C04B41/009 , C03C17/30 , C04B41/495 , C04B41/52 , C04B41/84 , C08F30/08 , C08L27/12 , C09D127/12 , Y10T428/31612 , Y10T428/31663 , C04B41/502 , C04B2103/40 , C04B41/5022 , C04B33/00 , C08L33/00
摘要： The invention relates to a dilutable, non-aqueous concentrate and an aqueous dilution used for aqueous delivery of fluorinated oligomeric silanes to a substrate, a method of treating a substrate with the aqueous dilution composition to render it oil and water repellent, and articles having coatings made from the aqueous dilution.
摘要翻译：本发明涉及一种可稀释的非水性浓缩物和用于将氟化低聚硅烷水性输送到底物的水性稀释液，用水稀释组合物处理底物以使其具有防水和防水性的方法，以及具有涂层的制品由水稀释制成。

24. 发明授权

US08476385B2 Fluorinated ether compositions and methods of using the same 失效
标题翻译：氟化醚组合物及其使用方法
公开(公告)号：US08476385B2
公开(公告)日：2013-07-02
申请号：US12602877
申请日：2008-06-06
申请人： Rudolf J. Dams , Miguel A. Guerra , Klaus Hintzer , Michael Jürgens , Harald Kaspar , Kai H. Lochhaas , Andreas R. Maurer , Zai-Ming Qiu , Werner Schwertfeger , Michael S. Terrazas , Tilman C. Zipplies
发明人： Rudolf J. Dams , Miguel A. Guerra , Klaus Hintzer , Michael Jürgens , Harald Kaspar , Kai H. Lochhaas , Andreas R. Maurer , Zai-Ming Qiu , Werner Schwertfeger , Michael S. Terrazas , Tilman C. Zipplies
IPC分类号： C08F18/20
CPC分类号： C08F220/24 , C08F220/28 , C08F220/36 , C08F230/08 , C08G65/007 , C08L33/08 , C08L35/06 , C09D133/08 , C09D133/14 , C09D135/06 , C08L2666/04
摘要： A composition including at least one first divalent unit represented by formula: Each Rf is independently selected from the group consisting of Rfa—(O)t—CHF—(CF2)n—; [Rfa—(O)t—C(L)H—CF2—O]m—W—; Rfb-O—(CF2)p-; F(CkF2k)—(O—CkF2k)P—O—CF2—; and CF3—O—(CF2)3—(OCF(CF3)—CF2)Z—O-L1-. Each Q is independently selected from the group consisting of a bond, —C(O)—N(R1)—, and —C(O)—O—. Each X is independently selected from the group consisting of alkylene and arylalkylene, wherein alkylene and arylalkylene are each optionally interrupted by at least one ether linkage and optionally terminated by —N(R1)—C(O)— or —O—C(O)—. R and R1 are each independently selected from the group consisting of hydrogen and alkyl having from 1 to 4 carbon atoms. Rfa represents a partially or fully fluorinated alkyl group having from 1 to 10 carbon atoms and optionally interrupted with at least one oxygen atom. Rfb is selected from the group consisting of CF3CFH— and F(CjF2j)-. Methods of reducing surface tension of a liquid, making foams, and treating a surface using the compositions are also disclosed.
摘要翻译：包含至少一个由式表示的第一二价单元的组合物：每个Rf独立地选自Rfa-（O）t-CHF-（CF 2）n - ; [Rfa-（O）t -C（L）H-CF 2 -O] m -W-; Rfb-O-（CF2）p-; F（CkF2k） - （O-CkF2k）P-O-CF2-; 和CF 3 -O-（CF 2）3 - （OCF（CF 3）-CF 2）Z-O-L 1。每个Q独立地选自由键，-C（O）-N（R 1） - 和-C（O）-O-组成的组。每个X独立地选自亚烷基和芳基亚烷基，其中亚烷基和芳基亚烷基各自任选地被至少一个醚键中断，并且任选地被-N（R 1）-C（O） - 或-OC（O） - 。 R和R 1各自独立地选自氢和具有1至4个碳原子的烷基。 Rfa表示具有1至10个碳原子并且任选被至少一个氧原子中断的部分或完全氟化的烷基。 Rfb选自CF 3 CFH-和F（C 1 F 2）） - 。还公开了降低液体的表面张力，制造泡沫和使用组合物处理表面的方法。

25. 发明授权

US07998585B2 Compositions for aqueous delivery of fluorinated oligomeric silanes 失效
标题翻译：含氟低聚硅烷的水分输送组合物
公开(公告)号：US07998585B2
公开(公告)日：2011-08-16
申请号：US12784892
申请日：2010-05-21
申请人： Rudolf J. Dams , Mark J. Pellerite , Steven J. Martin , Michael S. Terrazas
发明人： Rudolf J. Dams , Mark J. Pellerite , Steven J. Martin , Michael S. Terrazas
IPC分类号： B32B17/00
CPC分类号： C04B41/009 , C03C17/30 , C04B41/495 , C04B41/52 , C04B41/84 , C08F30/08 , C08L27/12 , C09D127/12 , Y10T428/31612 , Y10T428/31663 , C04B41/502 , C04B2103/40 , C04B41/5022 , C04B33/00 , C08L33/00
摘要： The invention relates to a dilutable, non-aqueous concentrate and an aqueous dilution used for aqueous delivery of fluorinated oligomeric silanes to a substrate, a method of treating a substrate with the aqueous dilution composition to render it oil and water repellent, and articles having coatings made from the aqueous dilution.
摘要翻译：本发明涉及一种可稀释的非水性浓缩物和用于将氟化低聚硅烷水性输送到底物的水性稀释液，用水稀释组合物处理底物以使其具有防水和防水性的方法，以及具有涂层的制品由水稀释制成。

26. 发明申请

US20100179262A1 FLUORINATED ETHER COMPOSITIONS AND METHODS OF USING THE SAME 失效
标题翻译：氟化醚组合物及其使用方法
公开(公告)号：US20100179262A1
公开(公告)日：2010-07-15
申请号：US12602877
申请日：2008-06-06
申请人： Rudolf J. Dams , Miguel A. Guerra , Klaus Hintzer , Michael Jürgens , Harald Kaspar , Kai H. Lochhaas , Andreas R. Maurer , Zai-Ming Qiu , Worner Schwertfeger , Michael S. Terrazas , Tilman C. Zipplies
发明人： Rudolf J. Dams , Miguel A. Guerra , Klaus Hintzer , Michael Jürgens , Harald Kaspar , Kai H. Lochhaas , Andreas R. Maurer , Zai-Ming Qiu , Worner Schwertfeger , Michael S. Terrazas , Tilman C. Zipplies
IPC分类号： C07C69/52 , C08K5/10 , C09K3/00 , C07F7/08
CPC分类号： C08F220/24 , C08F220/28 , C08F220/36 , C08F230/08 , C08G65/007 , C08L33/08 , C08L35/06 , C09D133/08 , C09D133/14 , C09D135/06 , C08L2666/04
摘要： A composition including at least one first divalent unit represented by formula: Each Rf is independently selected from the group consisting of Rfa—(O)t—CHF—(CF2)n—; [Rfa—(O)t—C(L)H—CF2—O]m—W—; Rfb-O—(CF2)p-; F(CkF2k)—(O—CkF2k)P—O—CF2—; and CF3—O—(CF2)3—(OCF(CF3)—CF2)Z—O-L1-. Each Q is independently selected from the group consisting of a bond, —C(O)—N(R1)—, and —C(O)—O—. Each X is independently selected from the group consisting of alkylene and arylalkylene, wherein alkylene and arylalkylene are each optionally interrupted by at least one ether linkage and optionally terminated by —N(R1)—C(O)— or —O—C(O)—. R and R1 are each independently selected from the group consisting of hydrogen and alkyl having from 1 to 4 carbon atoms. Rfa represents a partially or fully fluorinated alkyl group having from 1 to 10 carbon atoms and optionally interrupted with at least one oxygen atom. Rfb is selected from the group consisting of CF3CFH— and F(CjF2j)-. Methods of reducing surface tension of a liquid, making foams, and treating a surface using the compositions are also disclosed.
摘要翻译：包含至少一个由式表示的第一二价单元的组合物：每个Rf独立地选自Rfa-（O）t-CHF-（CF 2）n - ; [Rfa-（O）t -C（L）H-CF 2 -O] m -W-; Rfb-O-（CF2）p-; F（CkF2k） - （O-CkF2k）P-O-CF2-; 和CF 3 -O-（CF 2）3 - （OCF（CF 3）-CF 2）Z-O-L 1。每个Q独立地选自由键，-C（O）-N（R 1） - 和-C（O）-O-组成的组。每个X独立地选自亚烷基和芳基亚烷基，其中亚烷基和芳基亚烷基各自任选地被至少一个醚键中断，并且任选被-N（R 1）-C（O） - 或-O-C（O ） - 。 R和R 1各自独立地选自氢和具有1至4个碳原子的烷基。 Rfa表示具有1至10个碳原子并且任选被至少一个氧原子中断的部分或完全氟化的烷基。 Rfb选自CF 3 CFH-和F（C 1 F 2）） - 。还公开了降低液体的表面张力，制造泡沫和使用组合物处理表面的方法。

27. 发明申请

US20100168300A1 AQUEOUS COMPOSITIONS OF FLUORINATED SURFACTANTS AND METHODS OF USING THE SAME 失效
标题翻译：氟化表面活性剂的水性组合物及其使用方法
公开(公告)号：US20100168300A1
公开(公告)日：2010-07-01
申请号：US12601143
申请日：2008-05-21
申请人： Rudolf J. Dams , Michael S. Terrazas
发明人： Rudolf J. Dams , Michael S. Terrazas
IPC分类号： C08K5/42 , C08K5/09
CPC分类号： C11D1/004 , C09D5/027 , C09D7/45 , C09D7/47 , C09G1/04 , C11D3/37
摘要： Aqueous compositions comprising surfactant represented by a formula selected from the group consisting of: [Rf—(O)t—CHF—(CF2)n—COO−]iXi+; {[Rf—(O)t—CQH—CF2—O]m—R—COO−}iXi+; {[Rf—(O)t—CQH—CF2—O]m—R—SO3−)i, Xi+; and [CF3CFH—O—(CF2)p—COO−]iXi+; wherein Rf represents a partially or fully fluorinated aliphatic group optionally interrupted with at least one oxygen atom; Q is selected from the group consisting of F and CF3; R is selected from the group consisting of alkylene and arylene; X1+ represents a cation having a valence i, wherein i is 1, 2 or 3; t is O or 1; m is 1, 2, or 3; n is O or 1; and p is an integer from 1 to 6. In some aspects, the aqueous composition comprises a non-fluorinated polymer and is essentially free of fluoropolymers. In another aspect, the aqueous composition has a pH of greater than 11. In another aspect, the aqueous composition has a pH of at least 8 and is essentially free of fluorinated olefins. Methods of coating a surface and an article having a surface in contact with the composition are provided. Methods of cleaning a surface, and methods of lowering the surface tension of a liquid having a pH greater than 11 using aqueous compositions comprising the surfactants are also provided.
摘要翻译：包含由选自以下的式的表面活性剂组成的水性组合物：[Rf-（O）t-CHF-（CF 2）n -CO 2 - ] i X i + {[Rf-（O）t-CQH-CF2-O] m -R-COO-} iXi +; {[Rf-（O）t-CQH-CF2-O] m -R-SO3-）i，Xi + 和[CF 3 CFH-O-（CF 2）p-COO-] i X i +; 其中Rf表示任选被至少一个氧原子间断的部分或完全氟化的脂族基团; Q选自F和CF 3; R选自亚烷基和亚芳基; X1 +表示具有i价的阳离子，其中i为1,2或3; t为O或1; m为1,2或3; n为0或1; 并且p是1至6的整数。在一些方面，水性组合物包含非氟化聚合物，并且基本上不含含氟聚合物。另一方面，水性组合物的pH值大于11.另一方面，水性组合物的pH值至少为8，基本上不含氟化烯烃。提供涂覆表面和具有与组合物接触的表面的制品的方法。还提供了使用包含表面活性剂的水性组合物来清洁表面的方法和降低pH大于11的液体的表面张力的方法。

28. 发明申请

US20110124782A1 FLUORINATED ETHER COMPOUNDS AND METHODS OF USING THE SAME 失效
标题翻译：氟化醚化合物及其使用方法
公开(公告)号：US20110124782A1
公开(公告)日：2011-05-26
申请号：US13054601
申请日：2009-07-15
申请人： Rudolf J. Dams , Michael S. Terrazas , Klaus Hintzer , Zai-Ming Qiu , Miguel A. Guerra , Andreas R. Maurer , Harald Kaspar , Kai H. Lochhaas , Michael Juergens , Tilman C. Zipplies , Werner Schwertfeger
发明人： Rudolf J. Dams , Michael S. Terrazas , Klaus Hintzer , Zai-Ming Qiu , Miguel A. Guerra , Andreas R. Maurer , Harald Kaspar , Kai H. Lochhaas , Michael Juergens , Tilman C. Zipplies , Werner Schwertfeger
IPC分类号： C08K5/53 , C07F9/28 , C08K5/19 , C08K5/095 , C08K5/06 , C08K5/101 , C08K5/20 , C07C229/04 , C08K5/36 , C07C53/21 , C07C211/02 , C07F9/06 , C09K3/00
CPC分类号： C07C235/10 , C07C69/708 , C07C211/11 , C07C211/14 , C07C291/04 , C07C309/14 , C07F9/091 , C07F9/3808 , C08G65/007
摘要： Compounds represented by formula (Rf-Q-X)s—Z. Each Rf is independently a partially fluorinated or fully fluorinated group selected from Rfa-(O)r—CHF—(CF2)n—; [Rfb-(O)tC(L)H—CF2—O]m—W—; CF3CFH—O—(CF2)p—; CF3—(O—CF2)z—; and CF3—O—(CF2)3—O—CF2—. Methods of reducing surface tension of a liquid, making foams, and treating a surface using the compounds are also disclosed.
摘要翻译：由式（Rf-Q-X）s-Z表示的化合物。每个Rf独立地是选自Rfa-（O）r -CHF-（CF 2）n - 的部分氟化或完全氟化基团; [Rfb-（O）tC（L）H-CF2-O] m -W-; CF 3 CFH-O-（CF 2）p-; CF 3 - （O-CF 2）z - ; 和CF 3 -O-（CF 2）3 -O-CF 2 - 。还公开了降低液体的表面张力，制造泡沫以及使用该化合物处理表面的方法。

29. 发明申请

US20110124532A1 FLUORINATED ETHER SILANES AND METHODS OF USING THE SAME 审中-公开
标题翻译：氟化硅烷及其使用方法
公开(公告)号：US20110124532A1
公开(公告)日：2011-05-26
申请号：US13054579
申请日：2009-07-16
申请人： Andreas R. Maurer , Harald Kaspar , Kai H. Lochhaas , Michael Juergens , Michael S. Terrazas , Miguel A. Guerra , Rudolf J. Dams , Tilman C. Zipplies , Zai-Ming Qiu , Klaus Hintzer , Werner Schwertfeger
发明人： Andreas R. Maurer , Harald Kaspar , Kai H. Lochhaas , Michael Juergens , Michael S. Terrazas , Miguel A. Guerra , Rudolf J. Dams , Tilman C. Zipplies , Zai-Ming Qiu , Klaus Hintzer , Werner Schwertfeger
IPC分类号： C09K8/60 , C07F7/18 , C08G77/26
CPC分类号： C07F7/1804
摘要： Fluorinated compounds represented by formula Rf-Q-X—[Si(R)f(R1)3-f]g. Each Rf is independently a partially fluorinated or fully fluorinated group selected from Rfa-(O)r-CHF—(CF2)n-; [Rfb-(O)t-C(L)H—CF2—O]m-W—; CF3CFH—O—(CF2)p-; CF3—(O—CF2)z-; and CF3—O—(CF2)3—O—CF2—. Methods of treating a surface or a hydrocarbon-bearing formation using the fluorinated compounds and treated articles and treated hydrocarbon-bearing formations are also disclosed.
摘要翻译：由式Rf-Q-X- [Si（R）f（R 1）3-f] g表示的氟化合物。每个Rf独立地是选自Rfa-（O）r -CHF-（CF 2）n - 的部分氟化或完全氟化基团; [Rfb-（O）t -C（L）H-CF 2 -O] m -W-; CF 3 CFH-O-（CF 2）p-; CF 3 - （O-CF 2）z - ; 和CF 3 -O-（CF 2）3 -O-CF 2 - 。还公开了使用含氟化合物和经处理的制品和经处理的含烃地层处理表面或含烃地层的方法。

30. 发明授权

US06592659B1 Compositions for aqueous delivery of fluorinated silanes 失效
标题翻译：氟化硅烷水性输送组合物
公开(公告)号：US06592659B1
公开(公告)日：2003-07-15
申请号：US10002543
申请日：2001-11-15
申请人： Michael S. Terrazas , Mark J. Pellerite , Rudolf J. Dams
发明人： Michael S. Terrazas , Mark J. Pellerite , Rudolf J. Dams
IPC分类号： C09D18308
CPC分类号： C08G65/336 , C08G65/007 , C09D4/00 , Y10T428/3154 , Y10T428/31663 , C08G77/00
摘要： The invention relates to a dilutable, non-aqueous concentrate and an aqueous dilution used for aqueous delivery of fluorinated silanes to a substrate, a method of treating a substrate with the aqueous dilution composition to render it oil and water repellent, and articles having coatings made from the aqueous dilution.
摘要翻译：本发明涉及一种可稀释的非水浓缩物和用于将氟化硅烷水性递送至基材的水性稀释液，用水稀释组合物处理底物以使其具有防水和防水性的方法，以及制备具有涂层的制品从水稀释液中。

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