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21. 发明授权

US5117036A Preparation of aromatic carbamates 失效
标题翻译：芳香碳酸钙的制备
公开(公告)号：US5117036A
公开(公告)日：1992-05-26
申请号：US313864
申请日：1989-02-23
申请人： Philippe Leconte , Francois Metz
发明人： Philippe Leconte , Francois Metz
IPC分类号： B01J31/22 , C07B61/00 , C07C269/00 , C07C271/26
CPC分类号： C07C269/00
摘要： Aromatic carbamates are selectively and actively prepared by reacting (a) at least one nitroaromatic compound with (b) carbon monoxide and (c) at least one organic compound bearing at least one hydroxyl group, in the presence of:(d) a palladium-based catalyst,(e) at least one coordinate of the formula: ##STR1## in which each of G and G', which may be identical or different, is a bridging group which contains 3 or 4 atoms, at least 2 of which are carbon atoms, with the proviso that G and G' may be linked to each other, and(f) at least one protonic acid in which no proton is linked to a halogen atom, and wherein the amount of palladium present in the reaction medium is less than or equal to 0.01 mole per liter of such reaction medium and the reaction is carried out such that:(i) either the molar ratio (H.sup.+ /Pd) is higher than 150, and/or(ii) the molar ratio (coordinate/Pd) is higher than 20.
摘要翻译：通过使（a）至少一种硝基芳族化合物与（b）一氧化碳和（c）至少一种含有至少一个羟基的有机化合物在下列存在下反应来选择性和主动地制备芳族氨基甲酸酯：（d）（e）至少一个下式的坐标：其中G和G'各自可以相同或不同，是含有3或4个原子的桥连基团，至少2个其中G和G'可以彼此连接，和（f）至少一种其中没有质子与卤素原子连接的质子酸，其中存在于反应介质小于或等于0.01摩尔/升这种反应介质，并且反应进行使得：（i）摩尔比（H + / Pd）高于150，和/或（ii）摩尔比比（坐标/ Pd）高于20。

22. 发明授权

US09334050B2 Rotary wing blade, rotor comprising at least two of such blades and method to implement such a rotor 有权
标题翻译：旋翼机叶片，包括至少两个这种叶片的转子和实现这种转子的方法
公开(公告)号：US09334050B2
公开(公告)日：2016-05-10
申请号：US13445702
申请日：2012-04-12
申请人： Hugues Mercier Des Rochettes , Léon Buchaniek , Didier Joly , Jacques Dupas , Philippe Leconte
发明人： Hugues Mercier Des Rochettes , Léon Buchaniek , Didier Joly , Jacques Dupas , Philippe Leconte
IPC分类号： B64C27/72 , B64C27/473
CPC分类号： B64C27/72 , B64C27/473 , B64C2027/7216 , Y02T50/34
摘要： The present disclosure is directed to a rotary wing rotor comprising one or more blades. Each blade has a torsion frequency around its span being substantially equal to a rotation frequency (Ω) of the rotor; torsion means twist to the rotation frequency of the rotor, in synchronization with said rotation; and comprising a material configured to dampen the torsion resonance, so as to avoid the resonance divergence.
摘要翻译：本公开涉及包括一个或多个叶片的旋转翼转子。每个叶片具有围绕其跨度的扭转频率，其基本上等于转子的旋转频率（＆amp; OHgr）; 扭转装置与所述旋转同步地转动到转子的旋转频率; 并且包括被配置为抑制扭转共振的材料，以避免共振发散。

23. 发明申请

US20120095212A1 PROCESS FOR PREPARING LACTAMS 失效
标题翻译：制备纱线的方法
公开(公告)号：US20120095212A1
公开(公告)日：2012-04-19
申请号：US13260268
申请日：2010-04-27
申请人： Philippe Leconte
发明人： Philippe Leconte
IPC分类号： C07D223/10
CPC分类号： C07D201/08 , C07D223/10
摘要： A method for preparing lactams by cyclizing hydrolysis of a corresponding aminonitrile is described. A method for manufacturing a lactam by reacting an aminonitrile with water in the presence of a catalyst involving placing the water and the aminonitrile in contact in vapor phase, passing the mixture of vapors through a bed of catalyst arranged in at least one tube forming a reaction chamber and recovering the lactam at the outlet of the tube is also described.
摘要翻译：描述了通过环化相应的氨基腈的水解制备内酰胺的方法。一种在催化剂存在下使氨基腈与水反应的方法，所述催化剂涉及使水和氨基腈气相接触，使蒸汽混合物通过排列在形成反应的至少一个管中的催化剂床还描述了在管的出口处回收内酰胺的腔室。

24. 发明授权

US08119838B2 Conversion of nitrile compounds into carboxylic acids and corresponding esters thereof 有权
标题翻译：腈化合物转化成羧酸及其相应的酯
公开(公告)号：US08119838B2
公开(公告)日：2012-02-21
申请号：US12308176
申请日：2007-05-25
申请人： Philippe Leconte , Cyril Denis
发明人： Philippe Leconte , Cyril Denis
IPC分类号： C07C55/00
CPC分类号： C07C51/08 , C07C67/08 , C07C55/12 , C07C55/02 , C07C55/10 , C07C55/14 , C07C69/44 , C07C69/34
摘要： Hydrocarbon-based compounds containing at least one nitrile function are converted into compounds containing at least one carboxylic function, and into ester compounds from the carboxylic compounds thus obtained; such conversion entails reacting the nitrile compound with a hydroxyl basic compound in solution in a solvent at a temperature of between 80 and 150° C., in eliminating the ammonia formed, in reacting the salt obtained with a mineral acid, and then in recovering the compound containing at least one carboxylic function and, optionally, esterifying the acids obtained by reaction with an alcohol.
摘要翻译：含有至少一个腈官能团的烃基化合物被转化成含有至少一个羧酸官能团的化合物，并由如此获得的羧酸化合物转化为酯化合物; 这种转化需要使腈化合物与溶剂中的羟基碱性化合物在溶剂中在80-150℃的温度下反应，以消除所形成的氨与无机酸反应获得的盐，然后回收含有至少一个羧酸官能团的化合物，和任选地，通过与醇反应获得的酸酯化。

25. 发明申请

US20100145091A1 CONVERSION OF NITRILE COMPOUNDS INTO CORRESPONDING CARBOXYLIC ACIDS AND ESTERS 有权
标题翻译：氮化合物转化成相应的羧酸和酯类
公开(公告)号：US20100145091A1
公开(公告)日：2010-06-10
申请号：US12516042
申请日：2007-11-23
申请人： Olivier Buisine , Philippe Leconte , Malanie Agati
发明人： Olivier Buisine , Philippe Leconte , Malanie Agati
IPC分类号： C07C51/08 , C07C67/00
CPC分类号： C07C51/08 , C07C67/08 , C07C55/14 , C07C53/128 , C07C53/126 , C07C69/24 , C07C69/34
摘要： Hydrocarbon compounds having at least one nitrile function are converted into compounds having at least one carboxylic function by hydrating the nitrile functions into amide functions by reaction with water in the presence of a strong inorganic acid, and then hydrolyzing the amide functions into carboxylic functions by reaction with water and a strong inorganic acid; the carboxylic compounds thus obtained can be esterified into diesters, advantageously diester solvents.
摘要翻译：具有至少一个腈官能团的烃化合物通过在强无机酸存在下与水反应将腈官能团化合成酰胺官能团，然后通过反应将酰胺官能团水解成羧基官能团，将其转化成具有至少一个羧酸官能团的化合物与水和强无机酸; 由此得到的羧酸化合物可酯化成二酯，有利的是二酯溶剂。

26. 发明授权

US07612223B2 Process for the hydrocyanation of unsaturated compounds 有权
标题翻译：不饱和化合物的氢化方法
公开(公告)号：US07612223B2
公开(公告)日：2009-11-03
申请号：US10556628
申请日：2004-05-07
申请人： Cécile Rosier , Philippe Leconte , Damien Bourgeois
发明人： Cécile Rosier , Philippe Leconte , Damien Bourgeois
IPC分类号： C07C253/00
CPC分类号： C07C253/34 , C07C255/04
摘要： The present invention relates to a process for the hydrocyanation of unsaturated compounds to unsaturated mononitrile compounds or to dinitrile compounds; It relates more particularly to a process for the manufacture of dinitriles by double hydrocyanation of diolefins, such as butadiene, comprising a recovery and separation of the catalytic system. The process for the manufacture of dinitriles of the invention by hydrocyanation of unsaturated compounds, comprising at least one stage of hydrocyanation in the presence of a catalytic system comprising an organometallic complex formed by one or more monodentate organophosphite ligands and one or more bidentate organophosphorus ligands and optionally a promoter of Lewis acid type, comprises at least one stage of separation by distillation of a reactant used in the process or of a compound formed by the reaction from a medium comprising the said catalytic system.
摘要翻译：本发明涉及不饱和化合物氢化成不饱和单腈化合物或二腈化合物的方法; 更具体地涉及通过二烯烃如丁二烯的双氢氰化制备二腈的方法，其包括催化体系的回收和分离。通过氢化不饱和化合物的方法制备本发明的二腈的方法，该方法在包含由一个或多个单齿有机亚磷酸酯配体和一个或多个二齿有机磷配体形成的有机金属络合物的催化体系存在下包含至少一个氢化氰化阶段，以及任选的路易斯酸型助催化剂包括通过蒸馏在该方法中使用的反应物或由包含所述催化体系的介质通过反应形成的化合物的至少一个阶段分离。

27. 发明申请

US20080064902A1 Method for the Production of Cyclohexanone 失效
标题翻译：环己酮生产方法
公开(公告)号：US20080064902A1
公开(公告)日：2008-03-13
申请号：US11792373
申请日：2005-11-30
申请人： Philippe Leconte , Serge Veracini , Philippe Morel
发明人： Philippe Leconte , Serge Veracini , Philippe Morel
IPC分类号： C07C45/27
CPC分类号： C07C29/132 , C07C45/33 , C07C407/00 , C07C409/14 , C07C2601/14 , C07C49/403 , C07C35/08
摘要： The invention relates to a method for the preparation of cyclohexanone from cyclohexane. The invention relates more particularly to a method for the production of cyclohexane whose impurity content enables cyclohexanone to be used as a raw material for the production of e-caprolactam. The inventive method consists in treating the mixture of cyclohexanol/cyclohexanone arising from oxidation of cyclohexane by oxygen in a dehydrogenation stage in order to transform cyclohexanol into cyclohexanone and the impurities present such as cyclopentenal. The inventive method makes it possible to obtain highly pure cyclohexanone which is compatible when used as a raw material in the synthesis of e-caprolactam.
摘要翻译：本发明涉及从环己烷制备环己酮的方法。本发明更具体地涉及一种生产环己烷的方法，其中杂质含量使得环己酮可用作生产ε-己内酰胺的原料。本发明的方法是在脱氢阶段用氧处理由环己烷氧化产生的环己醇/环己酮的混合物，以便将环己醇转化成环己酮和存在的杂质如环戊烯醛。本发明的方法使得可以获得在用作合成ε-己内酰胺的原料时相容的高纯度环己酮。

28. 发明申请

US20070260086A1 Process for the Preparation of Dinitriles 有权
标题翻译：制备二腈的方法
公开(公告)号：US20070260086A1
公开(公告)日：2007-11-08
申请号：US10556629
申请日：2004-05-07
申请人： Cecile Rosier , Philippe Leconte , Damien Bourgeois
发明人： Cecile Rosier , Philippe Leconte , Damien Bourgeois
IPC分类号： C07C253/08
CPC分类号： C07C253/10 , C07C253/34 , Y02P20/584 , C07C255/04
摘要： The present invention relates to a process for the preparation of dinitriles by hydrocyanation of unsaturated nitrile compounds in the presence of a catalyst based on a metal element in the zero oxidation state and on organophosphorus ligands;the invention relates more particularly to a process for the recovery from the hydrocyanation medium of a catalyst for the hydrocyanation of unsaturated nitrites to dinitriles. It consists in controlling the concentration of unsaturated nitrites in the reaction medium resulting from the hydrocyanation reaction in order to obtain a concentration by weight of unsaturated nitrites of less than 20% in the said medium, and in then feeding the said medium to a stage of settling into two upper and lower phases. The lower phase comprises most of the catalytic system, while the upper phase is composed essentially of the dinitriles.
摘要翻译：本发明涉及一种通过在基于零氧化态的金属元素和有机磷配体的催化剂存在下，通过不饱和腈化合物的氢氰化来制备二腈的方法;本发明更具体地涉及一种回收方法来自用于将不饱和亚硝酸盐氢化成二腈的催化剂的氢化细胞培养基。它包括控制由氢氰化反应产生的反应介质中的不饱和亚硝酸盐的浓度，以便在所述介质中获得小于20％的不饱和亚硝酸盐的重量浓度，然后将所述介质供给到沉入两个上下相。较低的相包含大部分催化体系，而上部相基本上由二腈组成。

29. 发明申请

US20070155979A1 Process for the hydrocyanation of unsaturated compounds 有权
标题翻译：不饱和化合物的氢化方法
公开(公告)号：US20070155979A1
公开(公告)日：2007-07-05
申请号：US10556628
申请日：2004-05-07
申请人： Cécile Rosier , Philippe Leconte , Damien Bourgeois
发明人： Cécile Rosier , Philippe Leconte , Damien Bourgeois
IPC分类号： C07C255/06 , C07C253/10
CPC分类号： C07C253/34 , C07C255/04
摘要： The present invention relates to a process for the hydrocyanation of unsaturated compounds to unsaturated mononitrile compounds or to dinitrile compounds; It relates more particularly to a process for the manufacture of dinitriles by double hydrocyanation of diolefins, such as butadiene, comprising a recovery and separation of the catalytic system. The process for the manufacture of dinitriles of the invention by hydrocyanation of unsaturated compounds, comprising at least one stage of hydrocyanation in the presence of a catalytic system comprising an organometallic complex formed by one or more monodentate organophosphite ligands and one or more bidentate organophosphorus ligands and optionally a promoter of Lewis acid type, comprises at least one stage of separation by distillation of a reactant used in the process or of a compound formed by the reaction from a medium comprising the said catalytic system.
摘要翻译：本发明涉及不饱和化合物氢化成不饱和单腈化合物或二腈化合物的方法; 更具体地涉及通过二烯烃如丁二烯的双氢氰化制备二腈的方法，其包括催化体系的回收和分离。通过氢化不饱和化合物的方法制备本发明的二腈的方法，该方法在包含由一个或多个单齿有机亚磷酸酯配体和一个或多个二齿有机磷配体形成的有机金属络合物的催化体系存在下包含至少一个氢化氰化阶段，以及任选的路易斯酸型助催化剂包括通过蒸馏在该方法中使用的反应物或由包含所述催化体系的介质通过反应形成的化合物的至少一个阶段进行分离。

30. 发明授权

US06222069B1 Method for purifying adipic acid in water 失效
标题翻译：水中己二酸的纯化方法
公开(公告)号：US06222069B1
公开(公告)日：2001-04-24
申请号：US09194924
申请日：1999-03-17
申请人： Eric B. Henriet , Philippe Leconte , Carl Patois , Robert Perron
发明人： Eric B. Henriet , Philippe Leconte , Carl Patois , Robert Perron
IPC分类号： C07C5500
CPC分类号： C07C51/43 , C07C55/14
摘要： The invention discloses a method for purifying adipic acid in water. More precisely it discloses an improvement in adipic acid crystallization or recrystallization in water, characterised in that the said crystallization or recrystallization is effected in presence of a strong proton acid and/or in the presence of carbon monoxide. This crystallization or recrystallization particularly enables the content of metal catalyst traces in the adipic acid to be reduced.
摘要翻译：本发明公开了一种在水中纯化己二酸的方法。更准确地说，它公开了己二酸结晶或水中的重结晶的改进，其特征在于所述结晶或重结晶在强质子酸存在下和/或在一氧化碳的存在下进行。这种结晶或重结晶特别使得能够降低己二酸中的金属催化剂痕量的含量。

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