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21. 发明授权

US08003817B2 Process for the preparation of diaryl carbonates or arylalkyl carbonates from dialkyl carbonates 失效
标题翻译：从碳酸二烷基酯制备碳酸二芳基酯或碳酸芳基酯的方法
公开(公告)号：US08003817B2
公开(公告)日：2011-08-23
申请号：US12121873
申请日：2008-05-16
申请人： Andre Düx , Pieter Ooms , Johann Rechner , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
发明人： Andre Düx , Pieter Ooms , Johann Rechner , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
IPC分类号： C07C69/96
CPC分类号： C07C68/06 , B01D3/009 , Y02P20/127 , C07C69/96
摘要： The invention provides a process for the preparation of diaryl carbonates and/or alkylaryl carbonates from dialkyl carbonates and aromatic hydroxy compounds using one or more intermediate condensers for improving heat integration.
摘要翻译：本发明提供了一种使用一种或多种中间冷凝器制备碳酸二芳基酯和/或碳酸二烷基酯从碳酸二烷基酯和芳族羟基化合物制备方法，用于改善热量积分。

22. 发明申请

US20100261928A1 PROCESS FOR PREPARING DIARYL CARBONATES OR ALKYL ARYL CARBONATES FROM DIALKYL CARBONATES 有权
标题翻译：从碳酸二甲酯制备二元碳酸盐或碱金属碳酸盐的方法
公开(公告)号：US20100261928A1
公开(公告)日：2010-10-14
申请号：US12755873
申请日：2010-04-07
申请人： Andre DÜX , Helmut Mothes , Kaspar Hallenberger , Georg Ronge , Rafael Warsitz , Pieter Ooms , Johann Rechner
发明人： Andre DÜX , Helmut Mothes , Kaspar Hallenberger , Georg Ronge , Rafael Warsitz , Pieter Ooms , Johann Rechner
IPC分类号： C07C68/06
CPC分类号： C07C68/06 , Y02P20/127 , C07C69/96
摘要： The invention relates to a process for preparing diaryl carbonates and/or alkyl aryl carbonates from dialkyl carbonates and aromatic hydroxy compounds using a reactive dividing wall column.
摘要翻译：本发明涉及使用反应性分隔壁塔从碳酸二烷基酯和芳族羟基化合物制备碳酸二芳基酯和/或烷基芳基碳酸酯的方法。

23. 发明申请

US20090076293A1 PROCESSES FOR PREPARING DIARYL AND/OR ALKYLARYL CARBONATES FROM DIALKYL CARBONATES 有权
标题翻译：从碳酸二甲酯制备二元和/或烷基碳酸的方法
公开(公告)号：US20090076293A1
公开(公告)日：2009-03-19
申请号：US12210279
申请日：2008-09-15
申请人： Andre Dux , Pieter Ooms , Johann Rechner , Matthias Bohm , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
发明人： Andre Dux , Pieter Ooms , Johann Rechner , Matthias Bohm , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
IPC分类号： C07C68/06
CPC分类号： C07C68/06 , C07C69/96
摘要： Processes comprising: reacting a dialkyl carbonate and an aromatic hydroxy compound in the presence of a transesterification catalyst in a first reaction column, the first reaction column comprising a top section, a bottom section, a rectifying section in an upper portion of the column and a reaction zone below the rectifying section; feeding a bottom product from the first reaction column to a further reaction column; the bottom product comprising a diaryl carbonate, an alkylaryl carbonate, or both, and residual unreacted dialkyl carbonate and aromatic hydroxy compound; the further reaction column comprising a top section, a rectifying section in an upper portion of the column and a reaction zone below the rectifying section; and reacting the residual reacted dialkyl carbonate and aromatic hydroxy compound in the further reaction column; feeding a process stream to a distillation column, the process stream comprising a mixture of unreacted dialkyl carbonate and one or more reaction-product alcohols drawn from the first reaction column, the further reaction column, or both, such that the unreacted dialkyl carbonate is separated from the one or more reaction-product alcohols; and recycling the separated, unreacted dialkyl carbonate to the first reaction column; wherein the further reaction column comprises one or more condensers, and heat of condensation from the one or more condensers is fed back into the process.
摘要翻译：方法包括：在第一反应塔中的酯交换催化剂存在下使碳酸二烷基酯和芳族羟基化合物反应，所述第一反应塔包括塔的上部的顶部，底部，精馏段和整流段下方的反应区; 将底部产物从第一反应塔进料至另一反应塔; 底部产物包含碳酸二芳基酯，碳酸二烷基酯或二者，和残留的未反应的碳酸二烷基酯和芳族羟基化合物; 所述另外的反应塔包括顶部，所述塔的上部的精馏部和所述精馏部下方的反应区; 并使残留的反应后的碳酸二烷基酯和芳香族羟基化合物反应进一步反应塔中; 将工艺流输送到蒸馏塔，所述工艺流包含未反应的碳酸二烷基酯和从第一反应塔，进一步的反应塔或两者中抽出的一种或多种反应产物醇的混合物，使得未反应的碳酸二烷基酯被分离由一种或多种反应产物醇; 并将分离的未反应的碳酸二烷基酯再循环到第一反应塔中; 其中所述另外的反应塔包括一个或多个冷凝器，并且将来自所述一个或多个冷凝器的冷凝热反馈到所述方法中。

24. 发明申请

US20080293960A1 Process For The Preparation Of Diaryl Carbonates Or Arylalkyl Carbonates From Dialkyl Carbonates 失效
标题翻译：从碳酸二烷基酯制备碳酸二芳基酯或芳基烷基碳酸酯的方法
公开(公告)号：US20080293960A1
公开(公告)日：2008-11-27
申请号：US12121873
申请日：2008-05-16
申请人： Andre Dux , Pieter Ooms , Johann Rechner , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
发明人： Andre Dux , Pieter Ooms , Johann Rechner , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
IPC分类号： C07C69/96 , B01J19/00
CPC分类号： C07C68/06 , B01D3/009 , Y02P20/127 , C07C69/96
摘要： The invention provides a process for the preparation of diaryl carbonates and/or alkylaryl carbonates from dialkyl carbonates and aromatic hydroxy compounds using one or more intermediate condensers for improving heat integration.
摘要翻译：本发明提供了一种使用一种或多种中间冷凝器制备碳酸二芳基酯和/或碳酸二烷基酯从碳酸二烷基酯和芳族羟基化合物制备方法，用于改善热量积分。

25. 发明申请

US20070289722A1 DEVICES FOR COOLING GASES WHICH FORM A CORROSIVE CONDENSATION PRODUCT UPON COOLING 审中-公开
标题翻译：用于冷却气体的装置，其形成在冷却器上的腐蚀性冷凝产品
公开(公告)号：US20070289722A1
公开(公告)日：2007-12-20
申请号：US11752383
申请日：2007-05-23
申请人： Helmut Diekmann , Lutz Gottschalk , Kaspar Hallenberger , Gerhard Ruffert , Knud Werner
发明人： Helmut Diekmann , Lutz Gottschalk , Kaspar Hallenberger , Gerhard Ruffert , Knud Werner
IPC分类号： F28B9/10
CPC分类号： B01D53/002 , B01D5/0012 , B01D5/0033 , F28B1/00 , F28D7/16 , F28F19/02 , F28F19/04 , F28F19/06
摘要： A device for cooling hot gases (quencher) with the formation of a corrosive condensation product, which device has a pressure-resistant container and at least one corrosion-resistant internal gas guide pipe, and to a method of cooling gases that form corrosive condensation products, which method uses the mentioned device.
摘要翻译：一种用于冷却热气体（淬火剂）的装置，其形成腐蚀性冷凝产品，该装置具有耐压容器和至少一个耐腐蚀内部气体导管，以及冷却形成腐蚀性冷凝产物的气体的方法，哪种方法使用上述设备。

26. 发明申请

US20070274896A1 PROCESSES FOR HYDROGEN CHLORIDE OXIDATION USING OXYGEN 审中-公开
标题翻译：氧化氯化氢氧化工艺
公开(公告)号：US20070274896A1
公开(公告)日：2007-11-29
申请号：US11752598
申请日：2007-05-23
申请人： Andreas Bulan , Helmut Diekmann , Gerhard Ruffert , Kaspar Hallenberger
发明人： Andreas Bulan , Helmut Diekmann , Gerhard Ruffert , Kaspar Hallenberger
IPC分类号： C01B7/00
CPC分类号： C01B7/04 , B01J8/06 , B01J8/18 , B01J19/02 , B01J2219/00247 , B01J2219/0236 , F28F21/08
摘要： Processes which include: (a) providing a gas phase comprising hydrogen chloride; (b) oxidizing the hydrogen chloride in a reactor to form a product gas comprising chlorine, unreacted hydrogen chloride and water, the reactor having structural parts with inner surfaces that are contacted during oxidation by one or both of the gas phase and the product gas; (c) cooling the process gas; (d) separating the unreacted hydrogen chloride and water from the product gas; (e) drying the product gas; and (f) separating the chlorine from the product gas; wherein the inner surfaces of the reactor structural parts that are contacted during oxidation by one or both of the gas phase and the product gas are comprised of a nickel material having a nickel content of at least 60 wt. %, are described
摘要翻译：方法包括：（a）提供包含氯化氢的气相; （b）在反应器中氧化氯化氢以形成包含氯，未反应的氯化氢和水的产物气体，所述反应器具有结构部分，其内表面在气相和产物气体中的一种或两种氧化期间接触; （c）冷却工艺气体; （d）从产物气体中分离未反应的氯化氢和水; （e）干燥产品气体; 和（f）从产物气体中分离氯; 其中通过气相和产物气体中的一种或两种在氧化期间接触的反应器结构部件的内表面由镍含量为至少60重量％的镍材料组成。％

27. 发明授权

US06703473B2 Process for producing polycarbonate 有权
标题翻译：生产聚碳酸酯的方法
公开(公告)号：US06703473B2
公开(公告)日：2004-03-09
申请号：US10038953
申请日：2002-01-02
申请人： Uwe Hucks , Kaspar Hallenberger , Silke Kratschmer , Michael Prein , Steffen Kühling
发明人： Uwe Hucks , Kaspar Hallenberger , Silke Kratschmer , Michael Prein , Steffen Kühling
IPC分类号： C08G6400
CPC分类号： C08G64/406 , C08G64/307
摘要： An improvement to the melt transesterification reaction of diaryl carbonate with dihydroxy aryl compound is disclosed. The improvement entails the following steps (i) introducing the resulting vapor stream at the mid-height of a first distillation column, and (ii) separating the vapor stream into a top product containing high purity monohydroxy aryl compound and a first bottom product, and (iii) recycling the high purity monohydroxy aryl compound of (ii) to the reaction, and (iv) introducing the first bottom product at mid-height of a second distillation column, and (v) separating said first bottom product into high boiling bottom by-product and overhead remaining constituents, and (vi) introducing the overhead remaining constituents at mid-height of a third distillation column, and (vii) separating said overhead remaining constituents into overhead low-boiling fractions and bottom or product side stream that contains diaryl carbonate product, and (viii) recycling the diaryl carbonate product directly to the transesterification reaction.
摘要翻译：公开了碳酸二芳酯与二羟基芳基化合物的熔融酯交换反应的改进。改进需要以下步骤：（i）将所得蒸汽流引入第一蒸馏塔的中间高度，和（ii）将蒸汽流分离成含有高纯度单羟基芳基化合物和第一底部产物的顶部产物，以及（iii）将（ii）的高纯度单羟基芳基化合物再循环到反应中，和（iv）在第二蒸馏塔的中间部分引入第一底部产物，和（v）将所述第一底部产物分离成高沸点底部副产物和塔顶残留组分，和（vi）在第三蒸馏塔的中间高度引入塔顶剩余成分，和（vii）将塔顶剩余组分分离成塔顶低沸点馏分和底部或产物侧流，其含有碳酸二芳基酯产物，和（viii）将碳酸二芳基酯产物直接再循环到酯交换反应中。

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