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21. 发明授权

US08124717B2 Morpholine-substituted poly(arylene ether) and method for the preparation thereof 有权
标题翻译：吗啉取代的聚（亚芳基醚）及其制备方法
公开(公告)号：US08124717B2
公开(公告)日：2012-02-28
申请号：US13083696
申请日：2011-04-11
申请人： Alvaro Carrillo , Stephen M. Farnell , Hua Guo
发明人： Alvaro Carrillo , Stephen M. Farnell , Hua Guo
IPC分类号： C08G65/38 , C08G2/00
CPC分类号： C08G65/46
摘要： A poly(2,6-dimethyl-1,4-phenylene ether) prepared using a morpholine-containing polymerization catalyst has a monomodal molecular weight distribution with a reduced content of very high molecular weight species. It also exhibits increased morpholine incorporation in the high molecular weight fraction. Compared to commercially available poly(2,6-dimethyl-1,4-phenylene ether) prepared using a di-n-butylamine-containing polymerization catalyst, the poly(2,6-dimethyl-1,4-phenylene ether) of the invention exhibits reduced odor. Compared to other poly(2,6-dimethyl-1,4-phenylene ether) prepared using a morpholine-containing polymerization catalyst, the poly(2,6-dimethyl-1,4-phenylene ether) of the invention exhibits improved molecular weight build during compounding and improved compatibilization with polyamides.
摘要翻译：使用含吗啉的聚合催化剂制备的聚（2,6-二甲基-1,4-亚苯基醚）具有单分子分子量分布，具有非常高的分子量物质含量降低。它还表现出高分子量级分中增加的吗啉掺入。与使用含有二正丁胺的聚合催化剂制备的市售聚（2,6-二甲基-1,4-亚苯基醚）相比，聚（2,6-二甲基-1,4-亚苯基醚）发明显示减少的气味。与使用含吗啉的聚合催化剂制备的其它聚（2,6-二甲基-1,4-亚苯基醚）相比，本发明的聚（2,6-二甲基-1,4-亚苯基醚）表现出改善的分子量在复合期间建立并改善与聚酰胺的相容性。

22. 发明授权

US07671167B2 Poly(arylene ether) copolymer 有权
标题翻译：聚（亚芳基醚）共聚物
公开(公告)号：US07671167B2
公开(公告)日：2010-03-02
申请号：US12414856
申请日：2009-03-31
申请人： Alvaro Carrillo , Erik René Delsman , Hua Guo , Alexey Kruglov , Edward N. Peters
发明人： Alvaro Carrillo , Erik René Delsman , Hua Guo , Alexey Kruglov , Edward N. Peters
IPC分类号： C08G65/38
CPC分类号： C08G65/44 , H05K1/0326
摘要： A poly(arylene ether) copolymer is the product of oxidative copolymerization of monomers including a monohydric phenol and a dihydric phenol. It has an intrinsic viscosity of about 0.04 to about 0.15 deciliter per gram and, on average, about 1.8 to about 2 hydroxyl groups per molecule. The poly(arylene ether) copolymer is enriched in low molecular weight copolymer chains and copolymer chains that include a terminal unit derived from the dihydric phenol.
摘要翻译：聚（亚芳基醚）共聚物是包括一元酚和二元酚的单体的氧化共聚的产物。其特性粘度为约0.04至约0.15分升每克，平均每分子约1.8至约2个羟基。聚（亚芳基醚）共聚物富含低分子量共聚物链和共聚物链，其包括源自二元酚的末端单元。

23. 发明申请

US20090062478A1 POLY(ARYLENE ETHER) PREPARATION METHOD 有权
标题翻译： POLY（ARYLENE ETHER）制备方法
公开(公告)号：US20090062478A1
公开(公告)日：2009-03-05
申请号：US11845823
申请日：2007-08-28
申请人： Alvaro Carrillo , Hua Guo , Alexey Kruglov , Edward Norman Peters
发明人： Alvaro Carrillo , Hua Guo , Alexey Kruglov , Edward Norman Peters
IPC分类号： C08G65/48
CPC分类号： C08G65/44 , C08G65/485 , C08L2205/05
摘要： Capped poly(arylene ether)s are prepared by a method that includes reacting a poly(arylene ether) with a capping agent to form a capping reaction mixture, washing the capping reaction mixture with a concentrated basic aqueous solution, and isolating the capped poly(arylene ether) by a total isolation method. The washing method is effective for removal of capping-related impurities, and surprisingly does not result in decomposition of the capped poly(arylene ether).
摘要翻译：通过包括使聚（亚芳基醚）与封端剂反应形成封端反应混合物，用浓缩的碱性水溶液洗涤封端反应混合物并分离封端的聚（亚芳基醚）的聚（亚芳基醚）亚芳基醚）。洗涤方法对于去除封端相关杂质是有效的，并且令人惊奇地不会导致封端的聚（亚芳基醚）的分解。

24. 发明申请

US20070135609A1 Poly(arylene ether) copolymer 有权
标题翻译：聚（亚芳基醚）共聚物
公开(公告)号：US20070135609A1
公开(公告)日：2007-06-14
申请号：US11298182
申请日：2005-12-08
申请人： Alvaro Carrillo , Erik Delsman , Hua Guo , Alexey Kruglov , Edward Peters
发明人： Alvaro Carrillo , Erik Delsman , Hua Guo , Alexey Kruglov , Edward Peters
IPC分类号： C08G61/02
CPC分类号： C08G65/44 , H05K1/0326
摘要： A poly(arylene ether) copolymer is the product of oxidative copolymerization of monomers including a monohydric phenol and a dihydric phenol. It has an intrinsic viscosity of about 0.04 to about 0.15 deciliter per gram and, on average, about 1.8 to about 2 hydroxyl groups per molecule. The poly(arylene ether) copolymer is enriched in low molecular weight copolymer chains and copolymer chains that include a terminal unit derived from the dihydric phenol.
摘要翻译：聚（亚芳基醚）共聚物是包括一元酚和二元酚的单体的氧化共聚的产物。其特性粘度为约0.04至约0.15分升每克，平均每分子约1.8至约2个羟基。聚（亚芳基醚）共聚物富含低分子量共聚物链和共聚物链，其包括源自二元酚的末端单元。

25. 发明申请

US20070106051A1 Polyfunctional poly(arylene ether) method 审中-公开
标题翻译：多官能聚（亚芳基醚）法
公开(公告)号：US20070106051A1
公开(公告)日：2007-05-10
申请号：US11272119
申请日：2005-11-10
申请人： Alvaro Carrillo , Erik Delsman , Hua Guo , Alexey Kruglov , Edward Peters
发明人： Alvaro Carrillo , Erik Delsman , Hua Guo , Alexey Kruglov , Edward Peters
IPC分类号： C08G61/02
CPC分类号： C08G65/44 , C08G65/46 , H05K1/0326
摘要： A polyfunctional poly(arylene ether) resin may be prepared by a method that includes oxidatively copolymerizing a monohydric phenol and a polyhydric phenol in an aromatic hydrocarbon solvent in the presence of a catalyst comprising a metal ion and a nitrogen-containing ligand to form a solution comprising a polyfunctional poly(arylene ether) having an intrinsic viscosity of about 0.04 to about 0.3 deciliter per gram at 25° C. in chloroform; and contacting the polyfunctional poly(arylene ether) solution with an aqueous solution of a chelating agent to extract the metal ion from the solution; wherein the chelating agent and metal ion are present in a molar ratio of about 1.0 to about 1.5. The method reduces the formation of a dispersion during the chelation step.
摘要翻译：多官能聚（亚芳基醚）树脂可以通过包括在包含金属离子和含氮配体的催化剂存在下在芳烃溶剂中将一元酚和多元酚氧化共聚以形成溶液的方法来制备包括在25℃下在氯仿中特性粘度为约0.04至约0.3分升/克的多官能聚（亚芳基醚）并使多官能聚（亚芳基醚）溶液与螯合剂的水溶液接触，从溶液中提取金属离子; 其中所述螯合剂和金属离子以约1.0至约1.5的摩尔比存在。该方法减少了螯合步骤期间分散体的形成。

26. 发明申请

US20060073089A1 Carbon nanotube foam and method of making and using thereof 有权
公开(公告)号：US20060073089A1
公开(公告)日：2006-04-06
申请号：US11005474
申请日：2004-12-07
申请人： Pulickel Ajayan , Alvaro Carrillo , Nirupama Chakrapani , Ravindra Kane , Bingqing Wei
发明人： Pulickel Ajayan , Alvaro Carrillo , Nirupama Chakrapani , Ravindra Kane , Bingqing Wei
IPC分类号： D01F9/12
CPC分类号： D01F9/127 , A61L27/08 , A61L27/422 , A61L27/56 , A61L2400/12 , B01D39/2055 , B01D67/0072 , B01D67/0088 , B01D67/0093 , B01D71/021 , B01D2239/10 , B01D2239/1216 , B01D2239/1291 , B01D2323/24 , B01D2325/08 , B01D2325/24 , B60R13/02 , B60R13/08 , B82Y30/00 , B82Y40/00 , C01B32/168 , H01M4/583 , H01M4/96 , Y10S977/742 , Y10T428/12424
摘要： A method of making a carbon nanotube structure includes providing an array of substantially aligned carbon nanotubes, wetting the array with a liquid, and evaporating the liquid to form the carbon nanotube structure having a pattern in the carbon nanotube array. The structure is preferably a carbon nanotube foam.

27. 发明授权

US08466253B1 Poly(phenylene ether) process 有权
标题翻译：聚（苯醚）工艺
公开(公告)号：US08466253B1
公开(公告)日：2013-06-18
申请号：US13538020
申请日：2012-06-29
申请人： Prashant Kumar , Alvaro Carrillo , Scott Michael Fisher , Nitin Vilas Tople
发明人： Prashant Kumar , Alvaro Carrillo , Scott Michael Fisher , Nitin Vilas Tople
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C08G65/46 , C08G65/485 , C08L71/126
摘要： A method of purifying a capped poly(phenylene ether) includes mixing a poly(phenylene ether) capping reaction mixture comprising a capped poly(phenylene ether), a capping agent, a capping byproduct, a capping catalyst, and a poly(phenylene ether) solvent, and first washing solvents comprising a C1-C4 alkanol and water to form a first liquid phase comprising the capped poly(phenylene ether) and poly(phenylene ether) solvent, and a second liquid phase comprising C1-C4 alkanol and water; and separating the first liquid phase from the second liquid phase. Capped poly(phenylene ether) having reduced levels of residual capping agent, capping byproduct, and capping catalyst is produced from poly(phenylene ether) capping reaction mixtures by this method.
摘要翻译：一种纯化封端聚（亚苯基醚）的方法包括混合包含封端的聚（苯醚），封端剂，封端副产物，封端催化剂和聚苯醚的聚（苯醚）封端反应混合物，溶剂和包含C1-C4链烷醇和水的第一洗涤溶剂以形成包含封端的聚（苯醚）和聚（苯醚）溶剂的第一液相，以及包含C 1 -C 4烷醇和水的第二液相; 以及将第一液相与第二液相分离。通过该方法由聚（苯醚）封端反应混合物产生具有降低的残余封端剂，封端副产物和封端催化剂水平的封端的聚苯醚。

28. 发明申请

US20090121182A1 CARBON NANOTUBE FOAM AND METHOD OF MAKING AND USING THEREOF 审中-公开
标题翻译：碳纳米管泡沫及其制备和使用方法
公开(公告)号：US20090121182A1
公开(公告)日：2009-05-14
申请号：US12251716
申请日：2008-10-15
申请人： Pulickel AJAYAN , Alvaro Carrillo , Nirupama Chakrapani , Ravindra S. Kane , Bingqing Wei
发明人： Pulickel AJAYAN , Alvaro Carrillo , Nirupama Chakrapani , Ravindra S. Kane , Bingqing Wei
IPC分类号： C09K3/00 , D01F9/12 , C08K3/04 , C23C16/00
CPC分类号： D01F9/127 , A61L27/08 , A61L27/422 , A61L27/56 , A61L2400/12 , B01D39/2055 , B01D67/0072 , B01D67/0088 , B01D67/0093 , B01D71/021 , B01D2239/10 , B01D2239/1216 , B01D2239/1291 , B01D2323/24 , B01D2325/08 , B01D2325/24 , B60R13/02 , B60R13/08 , B82Y30/00 , B82Y40/00 , C01B32/168 , H01M4/583 , H01M4/96 , Y10S977/742 , Y10T428/12424
摘要： A method of making a carbon nanotube structure includes providing an array of substantially aligned carbon nanotubes, wetting the array with a liquid, and evaporating the liquid to form the carbon nanotube structure having a pattern in the carbon nanotube array. The structure is preferably a carbon nanotube foam.
摘要翻译：制造碳纳米管结构的方法包括提供基本排列的碳纳米管阵列，用液体润湿阵列，并蒸发液体以形成在碳纳米管阵列中具有图案的碳纳米管结构。该结构优选为碳纳米管泡沫。

29. 发明授权

US07473411B2 Carbon nanotube foam and method of making and using thereof 有权
标题翻译：碳纳米管泡沫及其制造和使用方法
公开(公告)号：US07473411B2
公开(公告)日：2009-01-06
申请号：US11005474
申请日：2004-12-07
申请人： Pulickel Ajayan , Alvaro Carrillo , Nirupama Chakrapani , Ravi S. Kane , Bingqing Wei
发明人： Pulickel Ajayan , Alvaro Carrillo , Nirupama Chakrapani , Ravi S. Kane , Bingqing Wei
IPC分类号： D01F9/12
CPC分类号： D01F9/127 , A61L27/08 , A61L27/422 , A61L27/56 , A61L2400/12 , B01D39/2055 , B01D67/0072 , B01D67/0088 , B01D67/0093 , B01D71/021 , B01D2239/10 , B01D2239/1216 , B01D2239/1291 , B01D2323/24 , B01D2325/08 , B01D2325/24 , B60R13/02 , B60R13/08 , B82Y30/00 , B82Y40/00 , C01B32/168 , H01M4/583 , H01M4/96 , Y10S977/742 , Y10T428/12424
摘要： A method of making a carbon nanotube structure includes providing an array of substantially aligned carbon nanotubes, wetting the array with a liquid, and evaporating the liquid to form the carbon nanotube structure having a pattern in the carbon nanotube array. The structure is preferably a carbon nanotube foam.
摘要翻译：制造碳纳米管结构的方法包括提供基本排列的碳纳米管阵列，用液体润湿阵列，并蒸发液体以形成在碳纳米管阵列中具有图案的碳纳米管结构。该结构优选为碳纳米管泡沫。

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