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21. 发明授权

US06855854B1 Process and apparatus for ethylbenzene production and transalkylation to xylene 失效
标题翻译：用于乙苯生产和烷基转移到二甲苯的方法和装置
公开(公告)号：US06855854B1
公开(公告)日：2005-02-15
申请号：US10461108
申请日：2003-06-13
申请人： Robert B. James, Jr.
发明人： Robert B. James, Jr.
IPC分类号： C07C6/12 , C07C5/27
CPC分类号： C07C6/126 , C07C2529/18 , C07C2529/70 , C07C15/08
摘要： The use of two transalkylation catalysts to react aromatic compounds of carbon number nine (and heavier carbon numbers) with benzene to form carbon number eight aromatics is disclosed. The two catalyst system preserves ethyl-group species on the heavier aromatics that would otherwise de-ethylate over most gas-phase transalkylation catalysts to form undesired ethane gas with benzene or toluene. Thus, by using a transalkylation step to save ethylbenzene, a greater yield of para-xylene or other carbon number eight aromatics may be achieved within an integrated complex. An apparatus and process for the two transalkylation catalyst system is disclosed with a liquid-phase unit and a gas-phase unit.
摘要翻译：公开了使用两个烷基转移催化剂将碳数为9（和较重碳数）的芳族化合物与苯反应以形成碳数为8的芳族化合物。两种催化剂体系在较重的芳族化合物上保留乙基物质，否则在大多数气相烷基转移催化剂上脱乙基化，以形成与苯或甲苯不需要的乙烷气体。因此，通过使用烷基转移步骤来保存乙苯，可以在集成的络合物内实现更高的对二甲苯或其它碳数为8的芳族化合物。公开了一种用于两个烷基转移催化剂体系的装置和方法，其具有液相单元和气相单元。

22. 发明授权

US5013424A Process for the simultaneous hydrogenation of a first feedstock comprising hydrocarbonaceous compounds and having a non-distillable component and a second feedstock comprising halogenated organic compounds 失效
标题翻译：用于同时氢化包含烃类化合物并具有不可蒸馏组分的第一原料和包含卤化有机化合物的第二原料的方法
公开(公告)号：US5013424A
公开(公告)日：1991-05-07
申请号：US559820
申请日：1990-07-30
申请人： Robert B. James, Jr. , Tom N. Kalnes , Steven P. Lankton
发明人： Robert B. James, Jr. , Tom N. Kalnes , Steven P. Lankton
IPC分类号： A62D3/00 , A62D3/37 , A62D101/22 , A62D101/24 , B01J23/44 , B01J23/88 , C10G1/00 , C10G45/02 , C10G65/04 , C10G65/12 , C10M175/00 , C10N40/08 , C10N40/22
CPC分类号： A62D3/37 , C10G45/02 , A62D2101/22 , A62D2101/24 , A62D2203/02
摘要： A process for the production of hydrogenated, distillable hydrocarbonaceous product from a feed comprising hydrocarbonaceous compounds and having a non-distillable component, and a feed comprising halogenated organic compounds by means of contacting the feed comprising hydrocarbonaceous compounds and having a non-distillable component with a hot hydrogen-rich gaseous stream to increase the temperature of this feed stream to vaporize at least a portion of the distillable hydrocarbonaceous compounds thereby producing a distillable hydrocarbonaceous product which is immediately hydrogenated in an integrated hydrogenation zone. The feed comprising halogenated organic compounds is contacted in a second hydrogenated hydrocarbonaceous product and at least one water-soluble inorganic halide compound.
摘要翻译：一种从包含烃类化合物并具有不可蒸馏组分的原料生产氢化，可蒸馏的含烃产物的方法，以及包含卤化有机化合物的进料，其通过使包含烃类化合物的进料与含有不可蒸馏组分的物质接触，热的富氢气流以增加该进料流的温度以蒸发至少一部分可蒸馏烃类化合物，从而产生可在一体化氢化区中立即氢化的可蒸馏烃类产物。包含卤代有机化合物的进料在第二氢化烃产物和至少一种水溶性无机卤化物化合物中接触。

23. 发明授权

US4818368A Process for treating a temperature-sensitive hydrocarbanaceous stream containing a non-distillable component to produce a hydrogenated distillable hydrocarbonaceous product 失效
标题翻译：用于处理含有不可蒸馏组分的温度敏感烃类物流以生产氢化的可蒸馏烃类产物的方法
公开(公告)号：US4818368A
公开(公告)日：1989-04-04
申请号：US113587
申请日：1987-10-28
申请人： Tom N. Kalnes , Robert B. James, Jr. , Darrell W. Staggs
发明人： Tom N. Kalnes , Robert B. James, Jr. , Darrell W. Staggs
IPC分类号： A62D3/00 , A62D3/40 , A62D101/22 , A62D101/24 , A62D101/43 , C10G69/00 , C10G69/06 , C10G69/14
CPC分类号： A62D3/40 , C10G69/00 , C10G69/06 , C10G69/14 , A62D2101/22 , A62D2101/24 , A62D2101/43 , A62D2203/10
摘要： A process for treating a temperature-sensitive hydrocarbonaceous stream containing a non-distillable component to produce a hydrogenated distillable hydrocarbonaceous product while minimizing thermal degradation of the hydrocarbonaceous stream which process comprises the steps of: (a) contacting the hydrocarbonaceous stream with a first hydrogen-rich gaseous stream having a temperature greater than the hydrocarbonaceous stream in a flash zone at flash conditions thereby increasing the temperature of the hydrocarbonaceous stream and vaporizing at least a portion thereof to provide a hydrocarbonaceous vapor stream comprising hydrogen and a heavy stream comprising the non-distillable component; (b) contacting the hydrocarbonaceous vapor stream comprising hydrogen with a hydrogenation catalyst in a hydrogenation reaction zone at hydrogenation conditions to increase the hydrogen content of the hydrocarbonaceous compounds contained in the hydrocarbonaceous vapor stream; (c) condensing at least a portion of the resulting effluent from the hydrogenation reaction zone to provide a second hydrogen-rich gaseous stream and a liquid stream comprising hydrogenated distillable hydrocarbonaceous compounds; (d) recovering a hydrogenated distillable hydrocarbonaceous product from the liquid stream comprising hydrogenated distillable hydrocarbonaceous compounds; and (e) reacting at least a portion of the heavy stream comprising the non-distillable component recovered from step (a) in a thermal coking zone at thermal coking conditions to provide a thermal coking zone effluent.
摘要翻译：一种用于处理含有不可蒸馏组分的温度敏感烃物流以产生氢化的可蒸馏烃类产物同时最小化烃流的热降解的方法，该方法包括以下步骤：（a）使烃流与第一氢 - 富氧气流在闪蒸条件下在闪蒸区中具有大于烃流的温度，从而提高烃流的温度并蒸发其至少一部分，以提供包含氢的烃蒸气流和包含不可蒸馏的重质流零件; （b）在加氢条件下，在加氢反应区中使包含氢气的烃类蒸气物流与氢化催化剂接触，以增加烃类蒸气流中所含烃类化合物的氢含量; （c）将来自氢化反应区的所得流出物的至少一部分冷凝以提供第二富氢气流和包含氢化的可蒸馏烃类化合物的液体流; （d）从包含氢化的可馏分烃类化合物的液体物流中回收氢化的可蒸馏烃类产物; 和（e）使包含从步骤（a）回收的不可蒸馏组分的至少一部分重质流在热焦化条件下在热焦化区中反应，以提供热焦化区流出物。

24. 发明授权

US4806233A Method of separating a hot hydrocarbonaceous stream 失效
标题翻译：分离热含烃物流的方法
公开(公告)号：US4806233A
公开(公告)日：1989-02-21
申请号：US90276
申请日：1987-08-28
申请人： Robert B. James, Jr. , Tom N. Kalnes
发明人： Robert B. James, Jr. , Tom N. Kalnes
IPC分类号： C07C7/00 , C10G49/22 , C10G9/16 , C07C5/28
CPC分类号： C07C7/005 , C10G49/22 , Y10S505/854
摘要： A method of separating a hot hydrocarbonaceous stream having a temperature above the dew point of water and comprising hydrogen, vaporous hydrocarbonaceous compounds and an acidic inorganic compound which method comprises: (a) contacting the hot hydrocarbonaceous stream at a temperature above the dew point of water in a contacting zone with an aqueous alkaline solution in an amount sufficient to simultaneously neutralize the acidic inorganic compound and to cool the hot hydrocarbonaceous stream to a temperature below the dew point of water to produce a flowing stream comprising a hydrogen-rich gas, a liquid hydrocarbonaceous phase and an aqueous solution containing inorganic neutralization products; and (b) introducing the flowing stream produced in step (a) into a separation zone to gravitationally produce an aqueous phase containing inorganic neutralization products, a hydrogen-rich gaseous phase and a hydrocarbonaceous liquid phase.
摘要翻译：一种分离温度高于水露点并包含氢，气态烃化合物和酸性无机化合物的热含烃物流的方法，该方法包括：（a）在高于露点露点的温度下使热含烃物流接触在与碱性水溶液的接触区中，其含量足以同时中和酸性无机化合物，并将热的含烃物流冷却至低于露点的温度，以产生包含富氢气体，液体含烃相和含有无机中和产物的水溶液; 和（b）将步骤（a）中产生的流动流引入分离区以重力产生含有无机中和产物，富氢气相和含烃液相的水相。

25. 发明授权

US08128887B2 Metal-based coatings for inhibiting metal catalyzed coke formation in hydrocarbon conversion processes 有权
标题翻译：用于在烃转化过程中抑制金属催化焦炭形成的金属基涂层
公开(公告)号：US08128887B2
公开(公告)日：2012-03-06
申请号：US12205290
申请日：2008-09-05
申请人： Steven A. Bradley , Robert B. James, Jr. , David W. Alley
发明人： Steven A. Bradley , Robert B. James, Jr. , David W. Alley
IPC分类号： B01J19/00 , B01J8/02 , B01J35/02 , B05D3/02 , B32B15/00 , B32B15/01
CPC分类号： C23C30/00 , B01J19/0026 , B01J19/02 , B01J2219/0236 , B01J2219/024 , C23C4/06 , C23C4/08 , C23C26/00 , Y10T428/12736 , Y10T428/12847 , Y10T428/12944
摘要： A coating applied to at least a portion of the surfaces of reactors, reactor internals, other reactor components, and/or heater tubes is provided in order to minimize the formation of metal catalyzed coke in hydrocarbon conversion processes operating at temperatures at about 350° C. (662° F.) or greater and in reducing environments. These coatings may comprise Nickel coatings or complexes thereof, such as Ni—Al, Ni—Cr/Cr carbide, as well as aluminum painted coatings that are applied in a reduction cure process (e.g., application temperatures of about 600° C. (1112° F.)). Additionally, where H2S is necessary for the process, such as to minimize thermal cracking, the coatings also reduce corrosion of base metal due to sulfidation attack and eliminate the requirement of continuous replacement of reactor internals and other components.
摘要翻译：提供了施加到反应器，反应器内部件，其他反应器部件和/或加热器管的表面的至少一部分的涂层，以便最小化在约350℃的温度下操作的烃转化过程中金属催化焦炭的形成（662°F）或更大，并且在还原环境中。这些涂层可以包括镍涂层或其复合物，例如Ni-Al，Ni-Cr / Cr碳化物，以及以还原固化过程（例如，约600℃的应用温度（1112） F。））。另外，如果H2S对于该方法是必需的，例如最小化热裂解，则涂层还可以减少由于硫化作用引起的贱金属的腐蚀，并消除对反应器内部件和其它部件的连续更换的要求。

26. 发明申请

US20100012552A1 PROCESS AND APPARATUS FOR PRODUCING GASOLINE 审中-公开
标题翻译：生产汽油的工艺和装置
公开(公告)号：US20100012552A1
公开(公告)日：2010-01-21
申请号：US12176290
申请日：2008-07-18
申请人： Robert B. James, JR. , Deng-Yang Jan , Robert J. Schmidt
发明人： Robert B. James, JR. , Deng-Yang Jan , Robert J. Schmidt
IPC分类号： C10G59/00 , B01J19/00
CPC分类号： C10G35/095 , B01J29/70 , C10G59/02
摘要： One exemplary embodiment can be a process for producing a gasoline. The process can include contacting a feed having a naphtha and recycling at least a portion of the reaction zone effluent to the one or more reforming reaction zones. Generally, the reformate includes no more than about 15%, by volume, benzene, with a UZM-8 catalyst in one or more reforming reaction zones to produce a reaction zone effluent.
摘要翻译：一个示例性实施方案可以是用于生产汽油的方法。该方法可以包括使具有石脑油的进料接触并将至少一部分反应区流出物再循环到一个或多个重整反应区。通常，重整产物在一个或多个重整反应区中包含不超过约15体积％的含有UZM-8催化剂的苯，以产生反应区流出物。

27. 发明申请

US20090000985A1 Process for Upgrading Contaminated Hydrocarbons 有权
标题翻译：升级污染烃类的方法
公开(公告)号：US20090000985A1
公开(公告)日：2009-01-01
申请号：US11770826
申请日：2007-06-29
申请人： Mark Van Wees , Robert B. James, JR. , Tom N. Kalnes , Gavin P. Towler
发明人： Mark Van Wees , Robert B. James, JR. , Tom N. Kalnes , Gavin P. Towler
IPC分类号： C10G11/20
CPC分类号： C10M175/0041 , C10G7/003 , C10G7/006 , C10G45/02 , C10G45/44 , C10G2300/1003
摘要： A process for the recovery and purification of a contaminated hydrocarbons, wherein the contamination includes metals, finely divided solids and non-distillable components. The process further includes hydroprocessing the oil to remove deleterious compounds, to produce high quality reusable lubricants, solvents and fuels and to improve the quality of water byproduct.
摘要翻译：用于回收和净化污染的碳氢化合物的方法，其中污染物包括金属，细碎固体和不可蒸馏组分。该方法还包括加氢处理油以除去有害化合物，生产高品质的可重复使用的润滑剂，溶剂和燃料，并提高水副产物的质量。

28. 发明授权

US5969201A Process for the conversion of plastic to produce a synthetic crude oil 失效
标题翻译：塑料转化生产合成原油的工艺
公开(公告)号：US5969201A
公开(公告)日：1999-10-19
申请号：US086112
申请日：1998-05-28
申请人： Tom N. Kalnes , Robert B. James, Jr.
发明人： Tom N. Kalnes , Robert B. James, Jr.
IPC分类号： C10G1/00 , C10G1/10 , C07C1/00
CPC分类号： C10G1/002 , C10G1/10
摘要： A process for the conversion of plastic to produce a synthetic crude oil by means of contacting the plastic with a hydrocarbonaceous recycle stream in a liquefying zone operated at liquefying conditions to produce a liquefied stream of plastic containing non-distillable particulate matter and at least a portion thereof is filtered. The filtered stream having a reduced concentration of finely divided particulate matter and the balance, if any, of the original liquefied stream together with hydrogen is contacted with a hydro-demetallization catalyst in a hydro-demetallization zone at hydro-demetallization conditions to produce gaseous, water-soluble inorganic compounds. The effluent from the hydro-demetallization zone is contacted with a hydrocracking catalyst in a hydrocracking zone to produce lower boiling hydrocarbons suitable for use as a synthetic crude oil. A recovered hydrogen-rich gaseous stream is preferably recycled to the hydro-demetallization zone. The gaseous, water-soluble inorganic compounds are removed by scrubbing the hydrocracking zone effluent with an aqueous stream. A portion of the hydrocarbons recovered from the hydrocracking zone effluent is recycled to the liquefying zone.
摘要翻译：一种通过在液化条件下操作的液化区中使塑料与烃类循环物流接触而产生合成原油的方法，以产生含有不可蒸馏颗粒物质的液化液体流和至少一部分被过滤。在氢化脱金属条件下，将具有降低浓度的细碎颗粒物质和余量（如果有的话）原始液化物流与氢气一起的过滤流与加氢脱金属催化剂接触，以产生气态，水溶性无机化合物。来自加氢脱金属区域的流出物与加氢裂化区中的加氢裂化催化剂接触以产生适合用作合成原油的低沸点烃。回收的富含氢气的气流优选地被再循环到加氢脱金属区。通过用含水流洗涤加氢裂化区流出物来除去气态的水溶性无机化合物。从加氢裂化区流出物回收的一部分烃再循环到液化区。

29. 发明授权

US5904838A Process for the simultaneous conversion of waste lubricating oil and pyrolysis oil derived from organic waste to produce a synthetic crude oil 失效
标题翻译：用于同时转化来自有机废物的废润滑油和热解油的方法，以生产合成原油
公开(公告)号：US5904838A
公开(公告)日：1999-05-18
申请号：US62089
申请日：1998-04-17
申请人： Tom N. Kalnes , Robert B. James, Jr.
发明人： Tom N. Kalnes , Robert B. James, Jr.
IPC分类号： C10G65/04 , C10G45/00 , C10G67/00 , C10M175/00
CPC分类号： C10G65/04
摘要： A process for the simultaneous conversion of waste lubricating oil and pyrolysis oil derived from organic waste to produce a synthetic crude oil by means of contacting the combined feed with a hot hydrogen-rich gaseous stream to increase the temperature of the combined feed to vaporize at least a portion of the distillable organic compounds contained therein which is immediately hydrogenated in a hydrogenation reaction zone. The resulting effluent from the hydrogenation reaction zone is then introduced into a hydroprocessing zone to produce higher hydrogen-content hydrocarbons and to remove heterogeneous components such as sulfur, oxygen, nitrogen and halide, for example. The resulting effluent is cooled and partially condensed to produce a gaseous stream containing hydrogen and gaseous water-soluble inorganic compounds and a liquid stream containing hydrocarbon compounds. The gaseous stream is scrubbed to remove the gaseous water-soluble organic compounds and to thereby produce a hydrogen-rich gaseous recycle stream.
摘要翻译：用于同时转化来自有机废物的废润滑油和热解油的方法，以通过使组合的进料与富含氢气的气态流接触以提高组合进料的温度至少蒸发而产生合成原油其中包含的一部分可馏出的有机化合物在氢化反应区中立即氢化。然后将来自加氢反应区的所得流出物引入加氢处理区以产生较高含氢烃，并除去例如硫，氧，氮和卤化物等不均匀组分。将所得流出物冷却并部分冷凝以产生含有氢气和气态水溶性无机化合物的气流以及含有烃化合物的液体流。洗涤气流以除去气态水溶性有机化合物，从而产生富氢气态循环流。

30. 发明授权

US5552037A Process for the treatment of two halogenated hydrocarbon streams 失效
标题翻译：处理两种卤代烃流的方法
公开(公告)号：US5552037A
公开(公告)日：1996-09-03
申请号：US299873
申请日：1994-09-01
申请人： Tom N. Kalnes , Robert B. James, Jr.
发明人： Tom N. Kalnes , Robert B. James, Jr.
IPC分类号： A62D3/00 , A62D3/34 , A62D3/37 , A62D101/22 , A62D101/28 , C01B7/00 , C01B7/01 , C01B7/07 , B62D3/00 , C01G17/00 , C07C1/00
CPC分类号： A62D3/37 , C01B7/00 , C01B7/01 , C01B7/0737 , A62D2101/22 , A62D2101/28 , Y02P20/125
摘要： An integrated process for simultaneously treating a halogenated organic stream containing less than about 500 ppm by weight of water or water precursors and a halogenated organic stream containing oxygen-containing compounds to produce hydrocarbonaceous compounds having a reduced level of organic halogen and a hydrogen halide stream containing less than about 500 ppm by weight of water.
摘要翻译：一种用于同时处理含有小于约500ppm重量的水或水前体和含有氧化合物的卤代有机物流的卤代有机物流的综合方法，以生产具有降低的有机卤素水平的含烃化合物和含有小于约500ppm重量的水。

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