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21. 发明授权

US09434709B2 Production of adipic acid and derivatives from carbohydrate-containing materials 有权
公开(公告)号：US09434709B2
公开(公告)日：2016-09-06
申请号：US14854780
申请日：2015-09-15
申请人： Rennovia Inc.
发明人： Thomas R. Boussie , Eric L. Dias , Zachary M. Fresco , Vincent J. Murphy , James Shoemaker , Raymond Archer , Hong Jiang
IPC分类号： C07C51/36 , C07C51/31 , C07D309/30 , B01J23/40 , B01J23/44 , B01J23/46 , B01J23/52 , B01J23/652 , B01J23/656 , B01J23/89 , B01J35/00 , B01J37/02 , C07C51/235 , C07C51/377 , C07C51/41 , C07C209/00 , C07C253/00 , C07D201/08 , C07D223/10 , C08G63/16 , C08G69/14 , C08G69/26 , C08G69/36 , C07C201/08 , B01J21/06 , B01J21/08 , B01J21/16 , B01J21/18
CPC分类号： C07C51/377 , B01J21/063 , B01J21/066 , B01J21/08 , B01J21/16 , B01J21/18 , B01J23/40 , B01J23/44 , B01J23/462 , B01J23/464 , B01J23/468 , B01J23/52 , B01J23/6525 , B01J23/6562 , B01J23/6567 , B01J23/8906 , B01J23/8913 , B01J23/8926 , B01J35/006 , B01J37/0205 , C07B2200/07 , C07C51/235 , C07C51/31 , C07C51/412 , C07C201/08 , C07C209/00 , C07C253/00 , C07D201/08 , C07D223/10 , C07D309/30 , C08G63/16 , C08G69/14 , C08G69/26 , C08G69/36 , Y02P20/582 , C07C55/14 , C07C211/12 , C07C255/04
摘要： The present invention generally relates to processes for the chemocatalytic conversion of a glucose source to an adipic acid product. The present invention includes processes for the conversion of glucose to an adipic acid product via glucaric acid or derivatives thereof. The present invention also includes processes comprising catalytic oxidation of glucose to glucaric acid or derivative thereof and processes comprising the catalytic hydrodeoxygenation of glucaric acid or derivatives thereof to an adipic acid product. The present invention also includes products produced from adipic acid product and processes for the production thereof from such adipic acid product.

22. 发明申请

US20160194298A1 PROCESS FOR PRODUCTION OF HEXANETRIOL FROM 5-HYDROXYMETHYLFURFURAL 有权
标题翻译：从5-羟基甲基纤维素生产己内酰胺的方法
公开(公告)号：US20160194298A1
公开(公告)日：2016-07-07
申请号：US14957551
申请日：2015-12-02
申请人： Rennovia Inc.
发明人： Valery SOKOLOVSKII , Mayya LAVRENKO , Alfred HAGEMEYER , Eric L. DIAS , James A. W. SHOEMAKER , Vincent J. MURPHY
IPC分类号： C07D307/28 , B01J8/04 , C07C29/09 , C07D307/12 , C07C29/10
CPC分类号： C07D307/28 , B01J8/04 , B01J2208/027 , C07C29/09 , C07C29/103 , C07C29/132 , C07C29/172 , C07C29/60 , C07D307/12 , C07D307/42 , C07C31/22 , C07C31/20
摘要： Industrial scale conversions of 5-hydroxymethylfurfural to commodity chemicals such as 1,2,6-hexanetriol and 1,6-hexanediol by chemocatalytic conversions using hydrogen and a heterogeneous reduction catalyst are provided. The reactions are suitable for use in continuous flow reactors. Methods of carrying out the conversions are provided, as are product and catalyst compositions.
摘要翻译：提供了通过使用氢和多相还原催化剂的化学转化将5-羟甲基糠醛转化为商品化学品如1,2,6-己三醇和1,6-己二醇的工业规模转化。这些反应适用于连续流动反应器。提供了进行转化的方法，以及产物和催化剂组合物。

23. 发明申请

US20160075676A1 Production of Adipic Acid and Derivatives from Carbohydrate-Containing Materials 有权
标题翻译：由含碳水化合物材料生产己二酸和衍生物
公开(公告)号：US20160075676A1
公开(公告)日：2016-03-17
申请号：US14854780
申请日：2015-09-15
申请人： Rennovia Inc.
发明人： Thomas R. Boussie , Eric L. Dias , Zachary M. Fresco , Vincent J. Murphy , James Shoemaker , Raymond Archer , Hong Jiang
IPC分类号： C07D309/30 , C07C51/377 , C07C51/235
CPC分类号： C07C51/377 , B01J21/063 , B01J21/066 , B01J21/08 , B01J21/16 , B01J21/18 , B01J23/40 , B01J23/44 , B01J23/462 , B01J23/464 , B01J23/468 , B01J23/52 , B01J23/6525 , B01J23/6562 , B01J23/6567 , B01J23/8906 , B01J23/8913 , B01J23/8926 , B01J35/006 , B01J37/0205 , C07B2200/07 , C07C51/235 , C07C51/31 , C07C51/412 , C07C201/08 , C07C209/00 , C07C253/00 , C07D201/08 , C07D223/10 , C07D309/30 , C08G63/16 , C08G69/14 , C08G69/26 , C08G69/36 , Y02P20/582 , C07C55/14 , C07C211/12 , C07C255/04
摘要： The present invention generally relates to processes for the chemocatalytic conversion of a glucose source to an adipic acid product. The present invention includes processes for the conversion of glucose to an adipic acid product via glucaric acid or derivatives thereof. The present invention also includes processes comprising catalytic oxidation of glucose to glucaric acid or derivative thereof and processes comprising the catalytic hydrodeoxygenation of glucaric acid or derivatives thereof to an adipic acid product. The present invention also includes products produced from adipic acid product and processes for the production thereof from such adipic acid product.
摘要翻译：本发明一般涉及将葡萄糖源化学转化为己二酸产物的方法。本发明包括通过葡糖二酸或其衍生物将葡萄糖转化成己二酸产物的方法。本发明还包括将葡萄糖催化氧化成葡糖二酸或其衍生物的方法和包括将葡糖二酸或其衍生物催化加氢脱氧至己二酸产物的方法。本发明还包括由己二酸产物生产的产品和由己二酸产物生产的产品。

24. 发明授权

US09035094B2 Process for production of adipic acid from 1,6-hexanediol 有权
标题翻译：从1,6-己二醇生产己二酸的方法
公开(公告)号：US09035094B2
公开(公告)日：2015-05-19
申请号：US13915120
申请日：2013-06-11
申请人： Rennovia, Inc.
发明人： Eric L. Dias , Vincent J. Murphy , James A. W. Shoemaker
IPC分类号： C07C55/00 , C07C51/235 , B01J23/42 , B01J23/52 , B01J23/44 , B01J21/06 , B01J35/10 , B01J35/00 , B01J23/652 , B01J23/68
CPC分类号： C07C51/235 , B01J21/066 , B01J23/42 , B01J23/44 , B01J23/52 , B01J23/6527 , B01J23/687 , B01J35/0006 , B01J35/1014 , B01J35/1019 , B01J35/1061 , B01J35/1066 , C07C55/14
摘要： Processes are disclosed for the conversion of 1,6-hexanediol to adipic acid employing a chemocatalytic reaction in which 1,6-hexanediol is reacted with oxygen in the presence of particular heterogeneous catalysts including at least one of platinum or gold. The metals are preferably provided on a support selected from the group of titania, stabilized titania, zirconia, stabilized zirconia, silica or mixtures thereof, most preferably zirconia stabilized with tungsten. The reaction with oxygen is carried out at a temperature from about 100° C. to about 300° C. and at a partial pressure of oxygen from about 50 psig to about 2000 psig.
摘要翻译：公开了使用化学催化反应将1,6-己二醇转化为己二酸的方法，其中1,6-己二醇与氧在特定的非均相催化剂（包括至少一种铂或金）存在下反应。金属优选提供在选自二氧化钛，稳定的二氧化钛，氧化锆，稳定的氧化锆，二氧化硅或其混合物，最优选用钨稳定的氧化锆的载体上。与氧的反应在约100℃至约300℃的温度和约50psig至约2000psig的氧分压下进行。

25. 发明授权

US08853458B2 Process for production of hexamethylenediamine from carbohydrate-containing materials and intermediates therefor 有权
标题翻译：由含碳水化合物的材料及其中间体生产六亚甲基二胺的方法
公开(公告)号：US08853458B2
公开(公告)日：2014-10-07
申请号：US13739975
申请日：2013-01-11
申请人： Rennovia, Inc.
发明人： Eric L. Dias , James A. W. Shoemaker , Thomas R. Boussie , Vincent J. Murphy
IPC分类号： C07C209/16 , C07C29/141 , C07D307/50 , C07C29/132 , C07D307/48 , C07C29/17
CPC分类号： C07C29/157 , C07C29/132 , C07C29/141 , C07C29/175 , C07C209/16 , C07D307/46 , C07D307/48 , C07D307/50 , C07C31/20 , C07C31/22 , C07C211/12
摘要： Processes are disclosed for the conversion of a carbohydrate source to hexamethylenediamine (HMDA) and to intermediates useful for the production of hexamethylenediamine and other industrial chemicals. HMDA is produced by direct reduction of a furfural substrate to 1,6-hexanediol in the presence of hydrogen and a heterogeneous reduction catalyst comprising Pt or by indirect reduction of a furfural substrate to 1,6-hexanediol wherein 1,2,6-hexanetriol is produced by reduction of the furfural substrate in the presence of hydrogen and a catalyst comprising Pt and 1,2,6-hexanediol is then converted by hydrogenation in the presence of a catalyst comprising Pt to 1,6 hexanediol, each process then proceeding to the production of HMDA by known routes, such as amination of the 1,6 hexanediol. Catalysts useful for the direct and indirect production of 1,6-hexanediol are also disclosed.
摘要翻译：公开了用于将碳水化合物源转化为六亚甲基二胺（HMDA）的方法和用于生产六亚甲基二胺和其它工业化学品的中间体。 HMDA通过在氢存在下将糠醛底物直接还原为1,6-己二醇和通过Pt的多相还原催化剂或通过将糠醛底物间接还原成1,6-己二醇来制备，其中1,2,6-己三醇通过在氢气存在下还原糠醛底物而制备，然后在包含Pt至1,2,6-己二醇的催化剂存在下，通过氢化将包含Pt和1,2,6-己二醇的催化剂转化，然后进行到通过已知途径生产HMDA，如1,6己糖胺的胺化。还公开了用于直接和间接生产1,6-己二醇的催化剂。

26. 发明申请

US20130310605A1 REDUCTION CATALYSTS 有权
标题翻译：还原催化剂
公开(公告)号：US20130310605A1
公开(公告)日：2013-11-21
申请号：US13894351
申请日：2013-05-14
申请人： Rennovia, Inc.
发明人： George Fredrick Salem , Guang Zhu , Alfred Gerhard Hagmeyer , Eric L. Dias
IPC分类号： B01J23/46
CPC分类号： B01J23/464 , B01J21/063 , B01J21/066 , B01J21/18 , B01J23/40 , B01J23/58 , B01J29/04 , B01J35/1014 , B01J35/1061 , B01J35/1066 , B01J37/0205 , B01J37/024 , C07C51/377 , C07C55/14
摘要： Disclosed are catalysts comprised of platinum and rhodium on a support selected from the group of zirconia, stabilized (doped) zirconia, zirconia-metal oxide composites, and mixtures thereof, wherein the outer surfaces of the support are selected from the group of zirconia, stabilized zirconia, and mixtures thereof. More particularly, the supported catalysts comprise platinum and rhodium, wherein the molar ratio of platinum to rhodium is in the range of about 3:1 to about 1:2. The average pore diameter of the catalyst supports is in the range of about 5 nm to about 70 nm and the surface area is in the range of about 15 m2/g to about 200 m2/g. Also disclosed are methods for the hydrodeoxygenation of carboxylic acids, mono- and/or di-lactones thereof having at least one hydroxyl group on the backbone thereof to corresponding acids where the backbone hydroxyl group has been reduced in the presence of the catalyst.
摘要翻译：公开了由选自氧化锆，稳定（掺杂）氧化锆，氧化锆 - 金属氧化物复合材料及其混合物的载体上的铂和铑组成的催化剂，其中载体的外表面选自氧化锆，稳定的氧化锆及其混合物。更具体地，载体催化剂包括铂和铑，其中铂与铑的摩尔比在约3:1至约1:2的范围内。催化剂载体的平均孔径在约5nm至约70nm的范围内，并且表面积在约15m 2 / g至约200m 2 / g的范围内。还公开了将羧酸，其主链上具有至少一个羟基的单 - 和/或二 - 内酯加氢脱氧至在催化剂存在下骨架羟基已被还原的相应酸的方法。

27. 发明申请

US20170226038A1 PROCESS FOR PRODUCTION OF ADIPIC ACID FROM 1,6-HEXANEDIOL 审中-公开
公开(公告)号：US20170226038A1
公开(公告)日：2017-08-10
申请号：US15295351
申请日：2016-10-17
申请人： Rennovia, Inc.
发明人： Eric L. DIAS , Vincent J. MURPHY , James A.W. SHOEMAKER
IPC分类号： C07C51/235 , B01J35/10 , B01J23/652 , B01J23/42 , B01J21/06
CPC分类号： C07C51/235 , B01J21/066 , B01J23/42 , B01J23/44 , B01J23/52 , B01J23/6527 , B01J23/687 , B01J35/0006 , B01J35/1014 , B01J35/1019 , B01J35/1061 , B01J35/1066 , C07C55/14
摘要： Processes are disclosed for the conversion of 1,6-hexanediol to adipic acid employing a chemocatalytic reaction in which 1,6-hexanediol is reacted with oxygen in the presence of particular heterogeneous catalysts including at least one of platinum or gold. The metals are preferably provided on a support selected from the group of titania, stabilized titania, zirconia, stabilized zirconia, silica or mixtures thereof, most preferably zirconia stabilized with tungsten. The reaction with oxygen is carried out at a temperature from about 100° C. to about 300° C. and at a partial pressure of oxygen from about 50 psig to about 2000 psig.

28. 发明申请

US20170197930A1 PROCESSES FOR THE PREPARATION OF 2,5-FURANDICARBOXYLIC ACID AND INTERMEDIATES AND DERIVATIVES THEREOF 审中-公开
公开(公告)号：US20170197930A1
公开(公告)日：2017-07-13
申请号：US15404996
申请日：2017-01-12
申请人： Rennovia Inc. , Stora Enso Oyj
发明人： Valery Sokolovskii , Vincent J. Murphy , Thomas R. Boussie , Gary M. Diamond , Eric L. Dias , Guang Zhu , James M. Longmire , Stanley Herrmann , Staffan Torssell , Mayya Lavrenko
IPC分类号： C07D307/68 , B01J8/02
CPC分类号： C07D307/68 , B01J8/02 , B01J2208/00893 , Y02P20/582
摘要： The present disclosure provides processes for the production of 2-5-furandicarboxylic acid (FDCA) and intermediates thereof by the chemocatalytic conversion of a furanic oxidation substrate. The present disclosure further provides processes for preparing derivatives of FDCA and FDCA-based polymers. In addition, the present disclosure provides crystalline preparations of FDCA, as well as processes for making the same.

29. 发明申请

US20170158656A1 CONVERSION OF FRUCTOSE-CONTAINING FEEDSTOCKS TO HMF-CONTAINING PRODUCT 有权
公开(公告)号：US20170158656A1
公开(公告)日：2017-06-08
申请号：US15437570
申请日：2017-02-21
申请人： Rennovia Inc.
发明人： Thomas R. Boussie , Eric L. Dias , Vincent J. Murphy , James A. W. Shoemaker
IPC分类号： C07D307/02
CPC分类号： C07D307/46 , B01D61/027 , B01D61/145 , B01D2311/02 , B01D2311/25 , C07D307/50
摘要： The present invention relates generally to processes for converting fructose-containing feedstocks to a product comprising 5-(hydroxymethyl)furfural (HMF) and water in the presence of water, solvent and an acid catalyst. In some embodiments, the conversion of fructose to HMF is controlled at a partial conversion endpoint characterized by a yield of HMF from fructose that does not exceed about 80 mol %. In these and other embodiments, the processes provide separation techniques for separating and recovering the product, unconverted fructose, solvent and acid catalyst to enable the effective recovery and reutilization of reaction components.

30. 发明申请

US20170158593A1 Production of Adipic Acid and Derivatives from Carbohydrate-Containing Materials 审中-公开
公开(公告)号：US20170158593A1
公开(公告)日：2017-06-08
申请号：US15232285
申请日：2016-08-09
申请人： Rennovia Inc.
发明人： Thomas R. Boussie , Eric L. Dias , Zachary M. Fresco , Vincent J. Murphy , James Shoemaker , Raymond Archer , Hong Jiang
IPC分类号： C07C51/377 , C07C51/31
CPC分类号： C07C51/377 , B01J21/063 , B01J21/066 , B01J21/08 , B01J21/16 , B01J21/18 , B01J23/40 , B01J23/44 , B01J23/462 , B01J23/464 , B01J23/468 , B01J23/52 , B01J23/6525 , B01J23/6562 , B01J23/6567 , B01J23/8906 , B01J23/8913 , B01J23/8926 , B01J35/006 , B01J37/0205 , C07B2200/07 , C07C51/235 , C07C51/31 , C07C51/412 , C07C201/08 , C07C209/00 , C07C253/00 , C07D201/08 , C07D223/10 , C07D309/30 , C08G63/16 , C08G69/14 , C08G69/26 , C08G69/36 , Y02P20/582 , C07C55/14 , C07C211/12 , C07C255/04
摘要： The present invention generally relates to processes for the chemocatalytic conversion of a glucose source to an adipic acid product. The present invention includes processes for the conversion of glucose to an adipic acid product via glucaric acid or derivatives thereof. The present invention also includes processes comprising catalytic oxidation of glucose to glucaric acid or derivative thereof and processes comprising the catalytic hydrodeoxygenation of glucaric acid or derivatives thereof to an adipic acid product. The present invention also includes products produced from adipic acid product and processes for the production thereof from such adipic acid product.

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