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21. 发明授权

US4447403A Method for autoclave oxidation of ion species aqueous solutions 失效
标题翻译：高压氧化离子种水溶液的方法
公开(公告)号：US4447403A
公开(公告)日：1984-05-08
申请号：US72304
申请日：1979-09-04
申请人： Laurence W. Bierman , Gary L. Long , David Bortner
发明人： Laurence W. Bierman , Gary L. Long , David Bortner
IPC分类号： C01B25/238 , C01G31/00 , C01G43/00 , C01G49/00 , C21B15/00 , C22B34/22 , C22B60/02
CPC分类号： C22B60/0282 , C01B25/238 , C01G31/00 , C01G43/00 , C01G49/00 , C21B15/00 , C22B34/22
摘要： An improved method and apparatus for effecting a substantial reduction in retention time of oxidation processes by the autoclave oxidation of ion species dissolved in aqueous solutions. In one embodiment, the invention provides for oxidation of dissolved reduced ion species including ferrous iron (Fe.sup.+2), uranium (U.sup.+4) and vanadium (V.sup.+3) from wet process phosphoric acids, or for conditioning of aqueous solutions for other uses, such as corrosion control, by raising the valence state of dissolved ion species. In accordance with the present invention, pure oxygen, present in quantity of at least 94% by volume, is utilized as an oxidizing agent with specified process parameters: temperature, pressure and mixing conditions in an autoclave reaction vessel. In a presently preferred embodiment, the following specified parameters have achieved optimum results with regard to a significant decrease of retention time of the aqueous solution treated in the autoclave vessel: temperature range of from about 120.degree. F. to about 160.degree. F., pressure range of from about 120 psi to about 150 psi and effecting agitation by the use of an impeller located near the interface of the liquid and gas mixture in the vessel to provide a dispersion of the liquid solution in the gaseous phase. In accordance with such embodiment, a reduction of retention time for oxidation of uranium (U.sup.+4 .fwdarw.U.sup.+6) and vandanium (V.sup.+3 .fwdarw.V.sup.+4) metals from wet process phosphoric acid has been found to be less than two minutes, whereas, prior processes for effecting the same oxidation results have taken at least one hour.
摘要翻译：一种改进的方法和装置，用于通过溶解在水溶液中的离子物质的高压釜氧化来显着降低氧化过程的保留时间。在一个实施方案中，本发明提供了从湿法磷酸氧化溶解的还原离子物质，包括二价铁（Fe + 2），铀（U + 4）和钒（V + 3），或用于调节其它水溶液通过提高溶解离子物质的化合价态来应用腐蚀控制。根据本发明，使用存在量为至少94体积％的纯氧作为氧化剂，其具有指定的工艺参数：高压釜反应容器中的温度，压力和混合条件。在目前优选的实施方案中，以下指定参数已经获得了在高压釜容器中处理的水溶液的保留时间的显着降低的最佳结果：温度范围为约120°F至约160°F，压力范围为约120psi至约150psi，并通过使用位于容器中的液体和气体混合物的界面附近的叶轮进行搅拌，以提供液体溶液在气相中的分散体。根据这种实施方案，已经发现，从湿法磷酸中氧化铀（U + 4-> U + 6）和铀（V + 3→V + 4）金属的保留时间的减少已经被发现小于两分钟，而用于实现相同氧化结果的现有方法至少需要1小时。

22. 发明授权

US4277454A Methods for the control of excessive corrosion in phosphoric acid circuits 失效
标题翻译：控制磷酸回路过度腐蚀的方法
公开(公告)号：US4277454A
公开(公告)日：1981-07-07
申请号：US76574
申请日：1979-09-18
申请人： Gary L. Long , Roger B. Humberger
发明人： Gary L. Long , Roger B. Humberger
IPC分类号： C01B25/225 , C01B25/226 , C23F11/04
CPC分类号： C01B25/226 , C01B25/225 , C23F11/04
摘要： Methods for control of excessive corrosion in wet process phosphoric circuits are effected by oxidation of reduced ion species in the acid with maintenance of EMF value of the acid above about 190 millivolts (S.C.E. reference) through the digestion circuit. Supplementary monitoring is by a ceric red-ox titration procedure. In one embodied form, the present invention is utilized to control corrosion in a phosphoric acid plant digestion system (and subsequent processing equipment) operating by a dihydrate (gypsum) process even when such a process employs a calcined western U.S. phosphate ore feed from a relatively highly carbonaceous ore. The invention is also applicable for treating wet process phosphoric acid in phosphoric acid plants having a digester system operating by a hemihydrate process. In a presently preferred embodiment, additions of manganese dioxide to a primary digester in a sufficient amount effective to achieve an EMF value over about 190 millivolts will significantly control the occurrence of excessive corrosion in phosphoric acid circuits. In yet another preferred embodiment, an oxygen autoclave oxidation is used to oxidize the reduced ion species present in the acid to inhibit corrosion.
摘要翻译：用于控制湿法磷酸回路中过度腐蚀的方法是通过在酸中氧化还原的离子物质来实现的，并通过消化回路维持高于约190毫伏（S.C.E.参考）的酸的EMF值。补充监测是通过氧化铈滴定法。在一个实施形式中，本发明用于控制在二水合物（石膏）方法中操作的磷酸设备消化系统（和随后的加工设备）中的腐蚀，即使这种方法使用来自相对的高含碳矿石。本发明也适用于在具有通过半水合法处理的蒸煮器系统的磷酸设备中处理湿法磷酸。在目前优选的实施方案中，以足以实现大约190毫伏的EMF值的足够量的一次蒸煮器添加二氧化锰将显着控制磷酸回路中过度腐蚀的发生。在另一个优选的实施方案中，使用氧气高压釜氧化来氧化存在于酸中的还原离子种类以抑制腐蚀。

23. 发明授权

US09545290B2 Needle probe guide 有权
标题翻译：针探针指南
公开(公告)号：US09545290B2
公开(公告)日：2017-01-17
申请号：US13561945
申请日：2012-07-30
申请人： Karalyn R. Tellio , Mark S. Zeiner , David N. Plescia , Gary L. Long , Peter K. Shires
发明人： Karalyn R. Tellio , Mark S. Zeiner , David N. Plescia , Gary L. Long , Peter K. Shires
IPC分类号： A61B90/11 , A61B18/00 , A61B18/14
CPC分类号： A61B90/11 , A61B18/1206 , A61B18/14 , A61B90/06 , A61B2017/00154 , A61B2018/00577 , A61B2018/00613 , A61B2018/00922 , A61B2018/143 , A61B2018/1475 , A61B2090/064
摘要： A device for guiding electrodes relative to a tissue treatment region. The device can comprise a body have a plurality of passages therethrough. Each passage can axially restrain an electrode positioned therein. When each electrode is axially restrained in a passage, the distal ends of the electrodes can be spaced a predetermined distance apart. Further, the electrodes can be held in a parallel or substantially parallel alignment when axially retained in the passages. The predetermined distance between the electrodes can correspond to a treatment distance in a tissue treatment region and the distal ends of the electrodes can be operably structured to conduct current therebetween when at least one of electrodes is energized by an energy source.
摘要翻译：用于相对于组织处理区域引导电极的装置。该装置可以包括具有穿过其中的多个通道的主体。每个通道可以轴向限制位于其中的电极。当每个电极轴向地限制在通道中时，电极的远端可以间隔开预定距离。此外，当轴向保持在通道中时，电极可以保持平行或基本上平行的对准。电极之间的预定距离可以对应于组织治疗区域中的治疗距离，并且当电极中的至少一个被能量源激励时，电极的远端可以可操作地构造成在其间传导电流。

24. 发明授权

US09011431B2 Electrical ablation devices 有权
标题翻译：电气消融装置
公开(公告)号：US09011431B2
公开(公告)日：2015-04-21
申请号：US13602742
申请日：2012-09-04
申请人： Gary L. Long , Ragae M. Ghabrial , David N. Plescia , Omar J. Vakharia
发明人： Gary L. Long , Ragae M. Ghabrial , David N. Plescia , Omar J. Vakharia
IPC分类号： A61B18/14 , A61B18/00 , A61B18/12
CPC分类号： A61B18/1492 , A61B18/1206 , A61B18/1477 , A61B2018/00214 , A61B2018/00482 , A61B2018/00547 , A61B2018/00577 , A61B2018/00613 , A61B2018/00898 , A61B2018/124 , A61B2018/1425
摘要： An electrical ablation apparatus comprises first and second electrodes. Each electrode comprises a first end configured to couple an energy source and a second end configured to couple to a tissue treatment region. An energy source is coupled to the first and second electrodes. The energy source is configured to deliver a first series of electrical pulses sufficient to induce cell necrosis by irreversible electroporation and a second series of electrical pulses sufficient to induce cell necrosis by thermal heating, through at least one of the first and second electrodes. The first series of electrical pulses is characterized by a first amplitude, a first pulse length, and a first frequency. The second series of electrical pulses is characterized by a second amplitude, a second pulse length, and a second frequency.
摘要翻译：电切除装置包括第一和第二电极。每个电极包括构造成耦合能量源的第一端和被配置为耦合到组织治疗区域的第二端。能量源耦合到第一和第二电极。能量源被配置为递送足以通过不可逆电穿孔诱导细胞坏死的第一系列电脉冲和通过热加热通过第一和第二电极中的至少一个足以诱导细胞坏死的第二系列电脉冲。第一系列电脉冲的特征在于第一幅度，第一脉冲长度和第一频率。第二系列电脉冲的特征在于第二幅度，第二脉冲长度和第二频率。

25. 发明授权

US09005198B2 Surgical instrument comprising an electrode 有权
标题翻译：包括电极的手术器械
公开(公告)号：US09005198B2
公开(公告)日：2015-04-14
申请号：US12696626
申请日：2010-01-29
申请人： Gary L. Long , William D. Dannaher , David N. Plescia , Omar J. Vakharia
发明人： Gary L. Long , William D. Dannaher , David N. Plescia , Omar J. Vakharia
IPC分类号： A61B18/18 , A61B18/14 , A61B17/3205 , A61B17/34 , A61B17/00 , A61B18/00 , A61N1/32 , H02J17/00
CPC分类号： A61B18/1477 , A61B17/3205 , A61B17/3415 , A61B18/1492 , A61B2017/00296 , A61B2018/00577 , A61N1/327 , H02J17/00 , H02J50/10 , H02J50/20
摘要： A surgical instrument configured to deliver electrical energy to tissue of a patient includes a handle, a first conductor, and a second conductor. The surgical instrument further includes a first electrode with a first distal portion, a second electrode with a second distal portion, and a third electrode with a third distal portion, wherein each distal portion is configured to contact the tissue. The second distal portion surrounds the first distal portion and the third distal portion surrounds the second distal portion. A first gap is defined between the first distal portion and the second distal portion. A second gap is defined between the second distal portion and the third distal portion. The first electrode includes a sharp end configured to penetrate the tissue and the second distal portion includes a plurality of projections extending toward third distal portion.
摘要翻译：构造成将电能传送到患者组织的手术器械包括手柄，第一导体和第二导体。手术器械还包括具有第一远端部分的第一电极，具有第二远端部分的第二电极和具有第三远端部分的第三电极，其中每个远端部分构造成接触组织。第二远端部分包围第一远端部分，第三远端部分围绕第二远端部分。在第一远端部分和第二远端部分之间限定第一间隙。第二间隙限定在第二远端部分和第三远端部分之间。第一电极包括构造成穿透组织的尖端，并且第二远端部分包括朝向第三远端部分延伸的多个突起。

26. 发明授权

US08568410B2 Electrical ablation surgical instruments 有权
标题翻译：电消融手术器械
公开(公告)号：US08568410B2
公开(公告)日：2013-10-29
申请号：US12109673
申请日：2008-04-25
申请人： Omar J. Vakharia , Kurt R. Bally , Andrew M. Zwolinski , Gregory J. Bakos , Matthew D. Holcomb , Gary L. Long , Steven P. Woodard , Surag S. Mantri
发明人： Omar J. Vakharia , Kurt R. Bally , Andrew M. Zwolinski , Gregory J. Bakos , Matthew D. Holcomb , Gary L. Long , Steven P. Woodard , Surag S. Mantri
IPC分类号： A61B18/12
CPC分类号： A61B18/1492 , A61B18/1445 , A61B18/1477 , A61B2018/1266 , A61B2018/1412 , A61B2018/1425 , A61B2018/1455
摘要： An electrical ablation device includes an elongated flexible member having a proximal end and a distal end. A clamp jaw portion is located at the distal end of the elongated flexible member. The clamp jaw portion is operatively movable from an open position to a closed position. A cutting blade is located in the clamp jaw portion. The clamp jaw portion is adapted to couple to an electrical waveform generator and to receive an electrical waveform.
摘要翻译：电消融装置包括具有近端和远端的细长柔性构件。钳夹部分位于细长柔性构件的远端。钳夹部分可操作地从打开位置移动到关闭位置。切割刀片位于钳夹部分中。钳夹部分适于耦合到电波形发生器并接收电波形。

27. 发明授权

US08529563B2 Electrical ablation devices 有权
标题翻译：电气消融装置
公开(公告)号：US08529563B2
公开(公告)日：2013-09-10
申请号：US12197749
申请日：2008-08-25
申请人： Gary L. Long , David N. Plescia
发明人： Gary L. Long , David N. Plescia
IPC分类号： A61B18/18
CPC分类号： A61N1/057 , A61B18/14 , A61B18/1477 , A61B18/1492 , A61B2017/22038 , A61B2018/00214 , A61B2018/0022 , A61B2018/00559 , A61B2018/00577 , A61B2018/1425 , A61B2018/1435 , A61B2018/1472 , A61N1/0573
摘要： A connector configured to receive electrical energy from an energy source. A fastener is coupled to the connector. The fastener is configured for attachment through a tissue wall. A first electrode includes at least one electrically conductive portion and is coupled to the connector by a first electrically conductive wire.
摘要翻译：连接器，被配置为从能量源接收电能。紧固件联接到连接器。紧固件构造成通过组织壁附着。第一电极包括至少一个导电部分，并通过第一导电线耦合到连接器。

28. 发明授权

US08361066B2 Electrical ablation devices 有权
公开(公告)号：US08361066B2
公开(公告)日：2013-01-29
申请号：US12352375
申请日：2009-01-12
申请人： Gary L. Long , David N. Plescia , Omar J. Vakharia
发明人： Gary L. Long , David N. Plescia , Omar J. Vakharia
IPC分类号： A61B18/14
CPC分类号： A61B18/1492 , A61B18/1206 , A61B18/1477 , A61B2018/00214 , A61B2018/00482 , A61B2018/00547 , A61B2018/00577 , A61B2018/00613 , A61B2018/00898 , A61B2018/124 , A61B2018/1425
摘要： An electrical ablation apparatus comprises first and second electrodes. Each electrode comprises a first end configured to couple an energy source and a second end configured to couple to a tissue treatment region. An energy source is coupled to the first and second electrodes. The energy source is configured to deliver a first series of electrical pulses sufficient to induce cell necrosis by irreversible electroporation and a second series of electrical pulses sufficient to induce cell necrosis by thermal heating, through at least one of the first and second electrodes. The first series of electrical pulses is characterized by a first amplitude, a first pulse length, and a first frequency. The second series of electrical pulses is characterized by a second amplitude, a second pulse length, and a second frequency.

29. 发明申请

US20120220999A1 ELECTRICAL ABLATION DEVICES AND METHODS 有权
标题翻译：电气设备和方法
公开(公告)号：US20120220999A1
公开(公告)日：2012-08-30
申请号：US13352495
申请日：2012-01-18
申请人： Gary L. Long
发明人： Gary L. Long
IPC分类号： A61B18/16 , A61B18/14
CPC分类号： A61B18/1233 , A61B18/1206 , A61B18/1402 , A61B18/1477 , A61B18/1492 , A61B18/16 , A61B2018/00077 , A61B2018/00577 , A61B2018/00613 , A61B2018/00642 , A61B2018/00732 , A61B2018/00767 , A61B2018/1467 , A61N1/327
摘要： A method for delivering energy to tissue having a necrotic threshold may generally comprise inserting an electrode array comprising a plurality of electrodes into the tissue, inserting a central electrode into the tissue, positioning a ground pad proximal to the tissue, applying a first sequence of electrical pulses to the electrode array less than the necrotic threshold to induce thermal heating in the tissue, applying a second sequence of electrical pulses to the central electrode equal to or greater than the necrotic threshold to induce cell necrosis in the tissue by irreversible electroporation, and applying a ground potential to the ground pad. Electrical ablation devices and systems and methods of using the same are also described herein.
摘要翻译：用于将能量递送到具有坏死阈值的组织的方法通常可以包括将包括多个电极的电极阵列插入组织中，将中心电极插入组织中，将接地垫定位在组织附近，施加第一序列电脉冲到电极阵列小于坏死阈值以诱导组织中的热加热，向中心电极施加等于或大于坏死阈值的第二序列电脉冲以通过不可逆电穿孔诱导组织中的细胞坏死，并施加地面电位到地面垫。本文还描述了电气消融装置及其系统及其使用方法。

30. 发明授权

US08216234B2 Tissue resection device 有权
标题翻译：组织切除装置
公开(公告)号：US08216234B2
公开(公告)日：2012-07-10
申请号：US10986602
申请日：2004-11-10
申请人： Gary L. Long
发明人： Gary L. Long
IPC分类号： A61B18/14
CPC分类号： A61B18/14 , A61B18/1477 , A61B2017/00269 , A61B2018/1407
摘要： A medical device for performing a therapeutic procedure on a patient. The medical device includes an elongate probe extending to an applicator end sized and shaped to be slidably received in an endoscope working channel. The device also includes an injection needle positioned adjacent the applicator end of the probe. The injection needle is communicatible with a fluid source for delivering fluid and an electrical energy source for delivering electrical energy to the needle when performing the therapeutic procedure on the patient. The needle also has a central axis. The device further includes an ablating loop positioned adjacent the applicator end of the probe. The ablating loop is communicatible with the electrical energy source for delivering electrical energy to the ablating loop when performing the therapeutic procedure. The ablating loop also has a central axis that is spaced from the central axis of the injection needle. During operation of the device, the injection needle and ablating loop have opposite charges for ablating tissue of the patient.
摘要翻译：一种用于对患者执行治疗程序的医疗装置。医疗装置包括延伸到施加器端部的细长探针，其尺寸和形状被可滑动地容纳在内窥镜工作通道中。该装置还包括邻近探针的施用器端定位的注射针。注射针与用于输送流体的流体源和用于在对患者执行治疗程序时将电能传递到针的电能源相互连接。针头也有一个中心轴。该装置还包括邻近探针的施用器端定位的消融回路。消融回路与电能源相通，用于在执行治疗过程时将电能传递到消融回路。烧蚀回路还具有与注射针的中心轴线间隔开的中心轴线。在装置的操作期间，注射针和消融环具有相反的用于烧蚀患者组织的电荷。

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