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    • 14. 发明授权
    • Transparent polycrystalline material and production process for the same
    • 透明多晶材料和生产工艺相同
    • US08470724B2
    • 2013-06-25
    • US13142132
    • 2009-12-25
    • Takunori TairaJun AkiyamaShigeo AsaiKunihiko Hara
    • Takunori TairaJun AkiyamaShigeo AsaiKunihiko Hara
    • C04B35/50
    • H01F41/0253B28B1/00B33Y40/00C04B35/447C04B35/50C04B35/6455C04B2235/3224C04B2235/6027C04B2235/605C04B2235/9653C30B28/00C30B29/22C30B29/30C30B30/04H01S3/1603H01S3/1611H01S3/1618H01S3/1671H01S3/1673H01S3/1685
    • Upon producing a transparent polycrystalline material, a suspension liquid (or slurry 1) is prepared, the suspension liquid being made by dispersing a raw-material powder in a solution, the raw-material powder including optically anisotropic single-crystalline particles to which a rare-earth element is added. A formed body is obtained from the suspension liquid by means of carrying out slip casting in a space with a magnetic field applied. On this occasion, while doing a temperature control so that the single-crystalline particles demonstrate predetermined magnetic anisotropy, one of static magnetic fields and rotary magnetic fields is selected in compliance with a direction of an axis of easy magnetization in the single-crystalline particles, and is then applied to them. A transparent polycrystalline material is obtained by sintering the formed body, the transparent polycrystalline material having a polycrystalline structure whose crystal orientation is controlled. In this calcination step, after subjecting the formed body to primary sintering at a temperature of 1,600-1,900 K, the resulting primarily-sintered body undergoes hot-isotropic-press sintering (or HIP processing) at a temperature of 1,600-1,900 K.
    • 在制备透明多晶材料时,制备悬浮液(或浆液1),悬浮液通过将原料粉末分散在溶液中而制成,原料粉末包括光学各向异性单晶颗粒,其中稀有 添加了地面元素。 通过在施加磁场的空间中进行滑移铸造,从悬浮液获得成形体。 在这种情况下,当进行温度控制使得单晶颗粒表现出预定的磁各向异性时,根据单晶颗粒中易磁化轴的方向选择静磁场和旋转磁场之一, 然后应用于它们。 通过烧结成形体获得透明多晶材料,该透明多晶材料具有晶体取向被控制的多晶结构。 在该烧成工序中,在1600〜1900K温度下对成型体进行一次烧结后,在1600〜1900K的温度下进行热均质压制烧结(或HIP加工)。
    • 20. 发明申请
    • Method of Manufacturing Single Crystal
    • 单晶制造方法
    • US20100126409A1
    • 2010-05-27
    • US11988295
    • 2006-04-27
    • Masahiro SakuradaIzumi Fusegawa
    • Masahiro SakuradaIzumi Fusegawa
    • C30B15/20
    • C30B15/305C30B30/04
    • This invention provides a process for producing a single crystal by a Chokralsky method in which a horizontal magnetic field is applied, characterized in that a single crystal is pulled up so that the radial magnetic field strength gradient ΔBr/ΔRc in such a direction that centers of magnetic field generation coils (25) are connected, is more than 5.5 (gauss/mm) and not more than 10 (gauss/mm) wherein ΔBr represents the amount of a variation in magnetic field strength from an original point (O) as the center part on a solid-liquid interface of a single crystal (12) to the inner wall (A) of a crucible on the surface of a melt, gauss; and ΔRc represents a radial distance from the original point (O) to the inner wall (A) of the crucible on the surface of the melt, mm. According to the production process of a single crystal, in growing a single crystal, the variation in temperature gradient near the solid-liquid interface can be minimized, and a high-quality single crystal having a desired defect zone in the direction of crystal growth can easily be produced with high productivity at high yield.
    • 本发明提供了一种通过Chokralsky方法制造单晶的方法,其中施加了水平磁场,其特征在于,将单晶拉起,使得这样的放射状磁场强度梯度Dgr; Br /&Dgr; Rc 连接磁场产生线圈(25)的中心的方向大于5.5(高斯/ mm)且不大于10(高斯/ mm),其中&Dgr; Br表示来自原始磁场强度的磁场强度的变化量 (O)作为单晶(12)与熔体表面上的坩埚的内壁(A)的固 - 液界面的中心部分,高斯; 和R d表示从熔点表面上的坩埚的原始点(O)到内壁(A)的径向距离。 根据单晶的制造工序,在生长单晶时,固液界面附近的温度梯度的变化可以最小化,并且在晶体生长方向上具有期望缺陷区的高质量单晶可以 容易以高产率高产率生产。