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    • 12. 发明申请
    • METHOD FOR PRODUCING LOW ALUMINIUM TITANIUM-ALUMINIUM ALLOYS
    • 生产低铝合金铝合金的方法
    • US20130019717A1
    • 2013-01-24
    • US13514990
    • 2010-12-17
    • Jawad Haidar
    • Jawad Haidar
    • C22C1/00
    • C22C14/00C22B5/04C22B34/1277
    • Disclosed herein is a method for producing a titanium-aluminium alloy containing less than about 15 wt. % aluminium. The method comprises a first step in which an amount of titanium subchlorides at or in excess of the stoichiometric amount required to produce the titanium-aluminium alloy are reduced by aluminium to form a reaction mixture comprising elemental titanium, and then a second step in which the reaction mixture comprising elemental titanium is heated to form the titanium-aluminium alloy. The reaction kinetics are controlled such that reactions resulting in the formation of titanium aluminides are minimised.
    • 本文公开了一种生产含有小于约15重量%的钛 - 铝合金的方法。 %铝。 所述方法包括第一步骤,其中在制造钛 - 铝合金所需的化学计量量或超过化学计量的钛的次氯酸盐由铝还原以形成包含元素钛的反应混合物,然后第二步骤 将包含元素钛的反应混合物加热以形成钛 - 铝合金。 控制反应动力学,使得导致形成钛铝化物的反应最小化。
    • 13. 发明授权
    • Method for the continuous or discontinuous extraction of a metal or several metals from a slag that contains the metal or a compound of the metal
    • 从含有金属或金属化合物的炉渣中连续或不连续地提取金属或几种金属的方法
    • US08157884B2
    • 2012-04-17
    • US12309796
    • 2007-10-25
    • Rolf DegelJürgen Kunze
    • Rolf DegelJürgen Kunze
    • C22B4/00C22B7/02
    • C22B7/04C21D5/04C22B4/04C22B4/08C22B5/04C22B5/18C22B15/0054F27B3/045F27B3/085F27D2099/0023Y02P10/212Y02P10/262
    • The invention concerns a method for the continuous or discontinuous extraction of a metal or several metals from a slag that contains the metal or a compound of the metal, in which the liquefied metal-containing slag is heated in a primary or secondary smelting unit (1). To provide an improved method for extracting metals, especially copper, from slags, the invention provides that the metal-containing slag is heated in a primary or secondary smelting unit (1) designed as an alternating-current electric furnace, and the molten material is then fed from the primary or secondary smelting unit (1) into a furnace (2) designed as a direct-current electric furnace, in which the metal to be extracted is subjected to an electrolytic separation, where a reducing agent in the form of calcium silicide (CaSi), calcium carbide (CaC2), ferrosilicon (FeO), aluminum (Al), and/or reducing gases is added and/or injected into the primary or secondary smelting unit (1).
    • 本发明涉及一种用于从含有金属或金属化合物的炉渣中连续或不连续地提取金属或几种金属的方法,其中含液化金属的炉渣在初级或次级冶炼单元(1 )。 为了提供从炉渣中提取金属,特别是铜的改进方法,本发明提供了在设计为交流电炉的初级或次级冶炼单元(1)中加热金属渣,熔融材料为 然后从主要或次要冶炼单元(1)进料到设计为直流电炉的炉子(2)中,其中待提取的金属进行电解分离,其中以钙的形式存在还原剂 将硅化物(CaSi),碳化钙(CaC 2),硅铁(FeO),铝(Al)和/或还原气体添加和/或注入到初级或次级熔炼单元(1)中。
    • 19. 发明申请
    • Method for electrolyzing molten salt, electrolytic cell, and process for producing ti using said method
    • 使用所述方法电解熔融盐,电解池和制造方法的方法
    • US20090152122A1
    • 2009-06-18
    • US11991072
    • 2006-08-22
    • Tadashi OgasawaraMakoto YamaguchiToru UenishiMasahiko HoriKazuo TakemuraKatsunori Dakeshita
    • Tadashi OgasawaraMakoto YamaguchiToru UenishiMasahiko HoriKazuo TakemuraKatsunori Dakeshita
    • C25B1/26C25B9/00C25C3/28
    • C22B34/129C22B5/04C22B34/1268C25C3/02C25C7/005
    • The present invention provides a method for electrolyzing molten salt that can enhance the concentration of metal-fog forming metal in the molten salt by carrying out the electrolysis under conditions that the molten salt containing the chloride of metal-fog forming metal is supplied from one end of an electrolytic cell to a space between an anode and a cathode in a continuous or intermittent manner to provide a flow rate in one direction to the molten salt in the vicinity of the surface of the cathode and thus to allow the molten salt to flow in one direction in the vicinity of the surface of the cathode. According to the present invention, while high current efficiency is maintained, only the molten salt enriched with metal-fog forming metal such as Ca can be effectively taken out. Further, this method can easily be carried out by using the electrolytic cell according to the present invention. Furthermore, the application of the method for electrolyzing molten salt according to the present invention to the production of Ti by Ca reduction can realize the production of metallic Ti with high efficiency. Thus, the method for electrolyzing molten salt, the electrolytic cell, and the process for producing Ti, each according to the present invention, can be effectively utilized in the production of Ti by Ca reduction.
    • 本发明提供了一种电解熔融盐的方法,该方法可以通过在从一端供给含有金属雾形成金属的氯化物的熔融盐的条件下进行电解,从而提高熔融盐中金属雾形成金属的浓度 的电解池以连续或间歇的方式连接到阳极和阴极之间的空间,以在阴极表面附近向熔融盐提供沿一个方向的流速,从而允许熔融盐流入 在阴极表面附近的一个方向。 根据本发明,在保持高电流效率的同时,仅有效地除去富含金属雾形成金属如Ca的熔盐。 此外,该方法可以通过使用根据本发明的电解槽容易地进行。 另外,通过将本发明的熔盐电解方法应用于通过Ca还原生产Ti,可以实现高效率地生产金属Ti。 因此,根据本发明的电解熔融盐,电解槽和制造Ti的方法的方法可以有效地用于通过Ca还原生产Ti。
    • 20. 发明申请
    • Process for the Production of Ge by Reduction of Gecl4 With Liquid Metal
    • 用液态金属还原Gecl4生产Ge的方法
    • US20080311027A1
    • 2008-12-18
    • US11663795
    • 2005-09-16
    • Eric RobertTjakko Zijlema
    • Eric RobertTjakko Zijlema
    • C01G17/04C22B5/00C25C3/00
    • C22B41/00C22B5/04Y02P10/212
    • The invention relates to the manufacture of high purity germanium for the manufacture of e.g. infra red optics, radiation detectors and electronic devices. GeCl4 is converted to Ge metal by contacting gaseous GeCl4 with a liquid metal M containing one of Zn, Na and Mg, thereby obtaining a Ge-bearing alloy and a metal M chloride, which is removed by evaporation or skimming. The Ge-bearing alloy is then purified at a temperature above the boiling point of metal M. This process does not require complicated technologies and preserves the high purity of the GeCl4 in the final Ge metal, as the only reactant is metal M, which can be obtained in very high purity grades and continuously recycled.
    • 本发明涉及用于制造例如高纯度锗的制造方法。 红外光学,辐射探测器和电子设备。 通过使气体GeCl4与含有Zn,Na和Mg中的一种的液态金属M接触,将GeCl 4转化为Ge金属,由此得到含Ge的合金和金属氯化物,通过蒸发或撇去除去。 然后在高于金属M沸点的温度下纯化含Ge合金。该方法不需要复杂的技术,并且保留了GeCl4在最终的Ge金属中的高纯度,因为唯一的反应物是金属M,它可以 可以获得非常高的纯度等级并持续回收。