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11. 发明授权

US07294729B2 Bis-chelating ligand and use thereof in carbonylation processes 有权
标题翻译：双螯合配体及其在羰基化过程中的应用
公开(公告)号：US07294729B2
公开(公告)日：2007-11-13
申请号：US10527568
申请日：2003-09-26
申请人： Wei-Jun Peng , Johnathan E Holladay
发明人： Wei-Jun Peng , Johnathan E Holladay
IPC分类号： C07F15/00 , C07F9/02 , B01J31/00
CPC分类号： C07F15/008 , B01J31/1608 , B01J31/185 , B01J2231/321 , B01J2531/80 , B01J2531/821 , B01J2531/822 , B01J2531/827 , B01J2531/845 , C07C45/50 , C07F9/65746 , C07C47/42
摘要： A novel bis-chelating composition characterized by formula I: wherein M is a Group VB element; R1 and R2 are each independently selected from hydrogen and monovalent hydrocarbyl radicals; or R1 and R2 are bonded together to form a diradical; or one of R1 or R2 is hydrogen or a monovalent hydrocarbyl radical, while the other of R1 or R2 is a hydrocarbyl radical bonded to an atom in Ar; wherein Ar is selected from 1,2-arylenes; Q is selected from 1,2-arylenes, 2,2′-bisarylenes and alkyl diradicals; and W is selected from II, III, IV, or V: wherein M is as defined hereinbefore; each R is independently selected from hydrogen and monovalent hydrocarbyl radicals; X is selected from alkyl and aryl diradicals; Ar1 and Ar2 are each independently selected from 1,2-arylenes;Ar3 and Ar4 are each independently selected from monovalent aryl radicals; and n in formula IV is 0 or 1. The composition finds utility as a ligand in catalysts for carbonylation processes
摘要翻译：特征在于式I的新型双螯合组合物：其中M是VB族元素; R1和R2各自独立地选自氢和一价烃基; 或者R 1和R 2结合在一起形成双基; 或R 1或R 2中的一个为氢或一价烃基，而R 1或R 2中的另一个为与Ar中的原子键合的烃基; 其中Ar选自1,2-亚芳基; Q选自1,2-亚芳基，2,2'-双芳烯和烷基双基; W选自II，III，IV或V：其中M如上所定义; 每个R独立地选自氢和一价烃基; X选自烷基和芳基双基; Ar 1和Ar 2各自独立地选自1,2-亚芳基; Ar 3和Ar 4是各自独立地选自一价芳基; 式IV中的n为0或1.该组合物用作用于羰基化方法的催化剂中的配体

12. 发明授权

US06177400B1 Unsaturated ketones and their use in perfumery 有权
标题翻译：不饱和酮及其在香料中的用途
公开(公告)号：US06177400B1
公开(公告)日：2001-01-23
申请号：US09306797
申请日：1999-05-07
申请人： Hubert Mimoun , Wolfgang Klaus Giersch
发明人： Hubert Mimoun , Wolfgang Klaus Giersch
IPC分类号： A61K746
CPC分类号： C07C403/16 , C07C31/1355 , C07C33/14 , C07C45/62 , C07C47/32 , C07C47/42 , C07C69/007 , C07C2601/14 , C07C2601/16 , C07D317/12 , C11B9/0034
摘要： The compounds according to the general formula in which formula the dotted lines indicate a single or a double bond, n and m are 0 or 1, R1 is hydrogen or an acyl group —C(O)R3, R3 being a linear or branched alkyl or alkylene group from C1 to C8, the oxygen atom being bound to the adjacent &agr;-carbon atom by a double bond in the case where n is 0 and by a single bond in the case where n is 1, R2 is hydrogen or a linear or branched alkyl, alkenyl or alkoxy group from C1 to C8, or R2 is an alkenoxy group which is linked to the group R1 to form a 1,3-dioxolane cycle having 5 to 7 ring members, are useful perfuming ingredients. The most preferred compounds according to the invention are those which have a damascone- or damascenone-like structure, with the methyl substituent being in 4-position of the ring instead of the 2-position, as is the case in damascones and damascenones.
摘要翻译：根据一般配方的化合物，其虚线表示单键或双键，n和m为0或1，R 1为氢或酰基-C（O）R 3，R 3为直链或支链烷基或在C1至C8的亚烷基中，在n为0的情况下，氧原子通过双键与相邻的α-碳原子结合，在n为1的情况下通过单键结合，R2为氢或直链或支链烷基，烯基或烷氧基，或R2是与基团R1连接形成具有5至7个环成员的1,3-二氧戊环循环的链烯氧基，是有用的加香成分。根据本发明最优选的化合物是具有大马酮酮或大马士革类结构的那些化合物，甲基取代基位于环的4-位而不是2-位，如在damascones和大马士革中的情况。

13. 发明授权

US4283561A Mixture of aldehydes resulting from hydroformylation of .alpha.-terpinene 失效
标题翻译：由α-萜品烯的加氢甲酰化产生的醛的混合物
公开(公告)号：US4283561A
公开(公告)日：1981-08-11
申请号：US94277
申请日：1979-11-14
申请人： Jens Hagen , Klaus Bruns
发明人： Jens Hagen , Klaus Bruns
IPC分类号： A61K8/33 , A61Q13/00 , C07C45/00 , C07C45/50 , C07C47/42 , C07C67/00 , C11B9/00
CPC分类号： C11B9/0034 , C07C45/50 , C07C47/42
摘要： This invention is directed to a mixture of compounds of formulas ##STR1## This invention is also directed to preparation of the mixture and the use of said mixture as a perfuming agent.
摘要翻译：本发明涉及式的化合物的混合物本发明还涉及混合物的制备和所述混合物作为芳香剂的用途。

14. 发明授权

US3515740A Cyano cyclohexenyl compounds 失效
标题翻译：氰基环己酮化合物
公开(公告)号：US3515740A
公开(公告)日：1970-06-02
申请号：US3515740D
申请日：1967-02-20
申请人： ORVILLE D FRAMPTON , JULIAN FELDMAN
发明人： FRAMPTON ORVILLE D , FELDMAN JULIAN
IPC分类号： C07C47/42 , C07C255/45 , C07C121/00
CPC分类号： C07C47/42 , C07C255/45

15. 发明授权

US3179700A Preparation of 1, 3-cyclohexadiene-1-carboxaldehydes 失效
标题翻译：制备1,3-环己二烯-1-甲醛
公开(公告)号：US3179700A
公开(公告)日：1965-04-20
申请号：US17312562
申请日：1962-02-14
申请人： MONSANTO CO
发明人： WILLIAMS JR BYRON L
IPC分类号： C07C47/42
CPC分类号： C07C45/69 , C07C47/42

16. 发明申请

US20160221924A1 METHODS FOR PRODUCING BETA-CYCLOLAVANDULAL AND DERIVATIVE OF SAME 有权
标题翻译：生产β-环糊精和衍生物的方法
公开(公告)号：US20160221924A1
公开(公告)日：2016-08-04
申请号：US15021168
申请日：2014-09-11
申请人： SHIN-ETSU CHEMICAL CO., LTD.
发明人： Takeshi Kinsho , Naoki Ishibashi
IPC分类号： C07C67/40 , C07C41/01 , C07C29/14 , C07C45/42
CPC分类号： C07C67/40 , C07C29/14 , C07C41/01 , C07C45/42 , C07C67/14 , C07C2601/16 , C07C69/24 , C07C33/14 , C07C47/42
摘要： Target compounds are synthesized simply, efficiently and selectively. More specifically, provided are a method for producing (2,4,4-trimethyl-1-cyclohexene)carbaldehyde, comprising the steps of: reacting the carbonyl group of 2,4,4-trimethyl-2-cyclohexenone (1) to obtain a 2,4,4-trimethyl-2-cyclohexenylidenemethyl ether compound (2) and hydrolyzing Compound (2) to obtain the (2,4,4-trimethyl-1-cyclohexene)carbaldehyde (3); a method for producing (2,4,4-trimethyl-1-cyclohexene)methanol, comprising a step of reducing Compound (3) to obtain the (2,4,4-trimethyl-1-cyclohexene)methanol (4); and a method for producing a (2,4,4-trimethyl-1-cyclohexenyl)methyl ester compound, comprising a step of esterifying Compound (4) to obtain the (2,4,4-trimethyl-1-cyclohexenyOmethyl ester compound (5).
摘要翻译：目标化合物被简单，有效和有选择地合成。更具体地说，提供了制备（2,4,4-三甲基-1-环己烯）甲醛的方法，包括以下步骤：使2,4,4-三甲基-2-环己烯酮（1）的羰基反应得到 2,4,4-三甲基-2-环己烯甲醚化合物（2）和水解化合物（2），得到（2,4,4-三甲基-1-环己烯）甲醛（3）; 制备（2,4,4-三甲基-1-环己烯）甲醇的方法，包括还原化合物（3）以获得（2,4,4-三甲基-1-环己烯）甲醇（4）的步骤; 和（2,4,4-三甲基-1-环己烯基）甲酯化合物的制备方法，其包括使化合物（4）酯化以得到（2,4,4-三甲基-1-环己烯基甲基酯化合物（ 5）。

17. 发明申请

US20040054231A1 Ionic liquids and their use 失效
标题翻译：离子液体及其用途
公开(公告)号：US20040054231A1
公开(公告)日：2004-03-18
申请号：US10381059
申请日：2003-08-11
发明人： Andrew Abbott , David L Davies , Glen Capper , Raymond K Rasheed , Vasuki Tambyrajah
IPC分类号： C07C211/63 , C07C211/64
CPC分类号： B01J31/0284 , B01J31/006 , B01J31/0279 , B01J31/26 , B01J2231/125 , B01J2231/326 , C07B37/12 , C07C45/69 , C07C211/63 , C07C215/90 , C07C2601/16 , C07C2602/42 , C07C2602/44 , C25D3/02 , C25D3/665 , C25F3/20 , C25F3/24 , H01M6/164 , H01M6/166 , H01M10/36 , C07C47/42 , C07C49/543 , C07C49/553 , C07C47/445
摘要： Ionic compounds having a freezing point of no more than 50null C., formed by the reaction of at least one amine salt of the formula R1R2R3R4NnullXnull (I) with at least one hydrated salt, which is a chloride, nitrate, sulphate or acetate of Li, Mg, Ca, Cr, Mn, Fe, Co, Ni, Cu, Zn, Cd, Pb, Bi, La or Ce; wherein R1, R2 and R3 are each independently a C1 to C5 alkyl or a C6 to C10 cycloalkyl group, or wherein R2 and R3 taken together represent a C4 to C10 alkylene group, thereby forming with the N atom of formula (I) a 5 to 11 membered heterocyclic ring, and wherein R4 is hydrogen, or phenyl, or C1 to C12 alkyl or cycloalkyl group, optionally substituted with at least one group selected from OH, Cl, Br, F, I, phenyl, NH2, CN, NO2, COOR5, CHO, COR5 and OR5, wherein R5 is a C1 to C10 alkyl or cycloalkyl group, and Xnull is an anion capable of being complexed by the said hydrated salt. The compounds are useful as solvents, electrolytes, and catalysts, and have particular application in solvents/electrolytes for metal plating and electropolishing processes, in particular in chromium plating.
摘要翻译：通过至少一种式R 1 R 2 R 3，R 4，R 3，R 3，R 4，R 4，R 4， - >（I）与至少一种水合盐，其是Li，Mg，Ca，Cr，Mn，Fe，Co，Ni，Cu，Zn，Cd，Pb，Bi，La的氯化物，硝酸盐，硫酸盐或乙酸盐或Ce; 其中R 1，R 2和R 3各自独立地为C 1至C 5烷基或C 6至C 10环烷基，或其中R 2和R 3一起表示C 4至C 10亚烷基由此与式（I）的N原子形成5至11元杂环，并且其中R 4是氢或苯基或C 1至C 12烷基或环烷基，任选被至少一个选自下的基团取代：由OH，Cl，Br，F，I，苯基，NH 2，CN，NO 2，COOR 5，CHO，COR 5和OR 5组成，其中R 5为C 1至C 10烷基或环烷基，X 是能够被所述水合盐络合的阴离子。该化合物可用作溶剂，电解质和催化剂，并且特别适用于用于金属电镀和电解抛光方法的溶剂/电解质，特别是在镀铬中。

18. 发明授权

US06369243B1 Chemical transformation of substrates using nonmetallic, organic catalyst compositions 有权
标题翻译：使用非金属有机催化剂组合物对基材进行化学转化
公开(公告)号：US06369243B1
公开(公告)日：2002-04-09
申请号：US09484082
申请日：2000-01-18
申请人： David W. C. MacMillan , Kateri A. Ahrendt
发明人： David W. C. MacMillan , Kateri A. Ahrendt
IPC分类号： C07D49308
CPC分类号： C07D493/08 , B01J31/0237 , B01J31/0254 , B01J2231/325 , B01J2231/326 , B01J2231/348 , B01J2231/72 , C07B37/12 , C07B53/00 , C07C45/69 , C07C67/293 , C07D233/32 , C07D307/46 , C07C47/445 , C07C47/453 , C07C49/453 , C07C47/42 , C07C69/013 , C07C69/145
摘要： A method is provided for catalytically transforming a functional group within a first reactant by reaction with a second reactant in the presence of a nonmetallic, organic catalyst composition composed of a heteroatom-containing activator and an acid, or a salt of a heteroatom-containing activator and an acid. Exemplary first reactants are &agr;,&bgr;-unsaturated carbonyl compounds such as &agr;,&bgr;-unsaturated ketones and &agr;,&bgr;-unsaturated aldehydes. The heteroatom of the activator is a Group 15 or Group 16 element such as nitrogen, oxygen, sulfur or phosphorus, and exemplary heteroatom-containing activators are amines. Chiral heteroatom-containing activators can be used to catalyze enantioselective reactions, such that a chiral product is obtained from a chiral or achiral starting material in enantiomerically pure form.
摘要翻译：提供了一种通过在由含杂原子的活化剂和酸或含有杂原子的活化剂的盐组成的非金属有机催化剂组合物存在下与第二反应物反应来在第一反应物内催化转化官能团的方法和酸。示例性的第一反应物是α，β-不饱和羰基化合物，例如α，β-不饱和酮和α，β-不饱和醛。活化剂的杂原子是第15族或第16族元素，例如氮，氧，硫或磷，并且示例性的含杂原子的活化剂是胺。手性含杂原子的活化剂可用于催化对映选择性反应，使得手性产物以手性或非手性起始原料以对映体纯的形式获得。

19. 发明授权

US6166263A Processes for the manufacture of acrolein 有权
标题翻译：制备丙烯醛的方法
公开(公告)号：US6166263A
公开(公告)日：2000-12-26
申请号：US169335
申请日：1998-10-09
申请人： William George Etzkorn , Jonathan Lester Brockwell , Mark Anderson Young , John Michael Maher , Barbara Knight Warren
发明人： William George Etzkorn , Jonathan Lester Brockwell , Mark Anderson Young , John Michael Maher , Barbara Knight Warren
IPC分类号： C07C45/33 , C07C45/35 , C07C45/60 , C07C45/64 , C07C45/69 , C07C45/71 , C07C45/32
CPC分类号： C07C45/69 , C07C45/33 , C07C45/35 , C07C45/60 , C07C45/64 , C07C45/71 , Y02P20/142 , C07C47/22 , C07C47/12 , C07C47/19 , C07C47/46 , C07C47/42 , C07C47/198
摘要： Processes are disclosed for the conversion of propylene to acrolein in the presence of propane. The processes utilize oxygen and recycle propane to the acrolein reactor. Process feeds can comprise, propane, propylene or mixtures thereof. The presence of propane in the propylene-to-acrolein reaction can enhance the efficiency of the processes.
摘要翻译：公开了在丙烷存在下将丙烯转化为丙烯醛的方法。该方法利用氧气并将丙烷再循环到丙烯醛反应器中。工艺进料可以包含丙烷，丙烯或其混合物。在丙烯到丙烯醛反应中丙烷的存在可以提高工艺的效率。

20. 发明授权

US5118865A Cyclic ketones and their use as perfuming ingredients 失效
标题翻译：周期性的KETONES及其作为丰富的成分使用
公开(公告)号：US5118865A
公开(公告)日：1992-06-02
申请号：US667702
申请日：1991-03-11
申请人： Christian Chapuis , Karl-Heinrich Schulte-Elte , Herve Pamingle , Christian Margot
发明人： Christian Chapuis , Karl-Heinrich Schulte-Elte , Herve Pamingle , Christian Margot
IPC分类号： A61K8/35 , A61Q13/00 , C07C33/14 , C07C45/30 , C07C45/58 , C07C45/62 , C07C45/75 , C07C47/225 , C07C47/30 , C07C47/32 , C07C47/42 , C07C47/45 , C07C49/11 , C07C49/21 , C07C69/75 , C07C403/16 , C07D303/04 , C11B9/00 , C11D3/50 , C11D9/44
CPC分类号： C07C403/16 , C07C33/14 , C07C45/305 , C07C45/58 , C07C45/62 , C07C47/30 , C07C47/42 , C07C47/45 , C07C49/11 , C07C49/21 , C07C69/75 , C07D303/04 , C07B2200/07 , C07C2101/14 , C07C2101/16
摘要： Novel compounds of formula ##STR1## wherein the dotted lines indicate the location of a single or double bond, symbol R.sup.1 stands for a hydrogen atom or a methyl radical, symbol R.sup.2 represents a linear or branched, saturated or unsaturated, C.sub.1 to C.sub.4 alkyl radical, provided that R.sup.1 is not hydrogen when R.sup.2 represents a methyl or n-propyl radical and the ring is saturated. Compounds (Ia) are useful as perfuming ingredients.A process for their preparation is disclosed.
摘要翻译：式（Ia）的新型化合物，其中虚线表示单键或双键的位置，符号R1表示氢原子或甲基，符号R2表示直链或支链，饱和或不饱和的C1至 C4烷基，条件是当R 2表示甲基或正丙基并且该环饱和时，R 1不是氢。化合物（Ia）可用作加香成分。公开了其制备方法。

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