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11. 发明申请

US20120315483A1 POLYAMIDE-BASED POLYMER POWDER, USE THEREOF IN A MOLDING METHOD, AND MOLDED ARTICLES MADE FROM SAID POLYMER POWDER 审中-公开
标题翻译：基于聚酰胺的聚合物粉末，在模塑方法中使用，以及由固体聚合物粉末制成的模制品
公开(公告)号：US20120315483A1
公开(公告)日：2012-12-13
申请号：US13581085
申请日：2011-04-06
申请人： Franz-Erich Baumann , Wolfgang Diekmann , Beatrice Kueting , Heike Stemmer , Maik Grebe , Kristiane Warnke , Sylvia Monsheimer , Harald Haeger
发明人： Franz-Erich Baumann , Wolfgang Diekmann , Beatrice Kueting , Heike Stemmer , Maik Grebe , Kristiane Warnke , Sylvia Monsheimer , Harald Haeger
IPC分类号： C08L77/06 , B29C35/08
CPC分类号： B29C64/106 , B29C64/153 , B33Y70/00 , C08L77/02 , C08L77/06 , C08L2205/02 , C09D5/03 , Y10T428/2982
摘要： The invention relates to a polymer powder for use in a layer-by-layer method in which areas of each powder layer are selectively fused by introducing electromagnetic energy. Said polymer powder contains: at least one AB-type polyamide produced by polymerizing lactams comprising 10 to 12 carbon atoms in the monomer unit or polycondensing the corresponding ω-amino carboxylic acids comprising 10 to 12 carbon atoms in the monomer unit and at least one AABB-type polyamide produced by polycondensing diamines and dicarboxylic acids, each of which comprises 10 to 14 carbon atoms in the monomer units, the AB-type polyamide containing up to 20 mole % of the AABB comonomer units and the AABB-type polyamide containing up to 20 mole % of the AB monomer units. The invention also relates to a method for producing such a powder, a layer-by-layer method for producing a molded article from such a powder in which areas of each layer are selectively fused by introducing electromagnetic energy, the selectivity being obtained using masks or by applying inhibitors, absorbers or susceptors or focusing the applied energy, and molded articles produced in said manner.
摘要翻译：本发明涉及一种用于逐层方法的聚合物粉末，其中每个粉末层的区域通过引入电磁能被选择性地融合。所述聚合物粉末包含：至少一种AB型聚酰胺，其通过在单体单元中聚合包含10至12个碳原子的内酰胺或将在单体单元中包含10至12个碳原子的相应ω-氨基羧酸或至少一种AABB 通过缩聚二胺和二羧酸制备的聚酰胺，其各自在单体单元中包含10至14个碳原子，AB型聚酰胺含有至多20摩尔％的AABB共聚单体单元和AABB型聚酰胺，其含有至多 20摩尔％的AB单体单元。本发明还涉及一种制备这种粉末的方法，一种从这种粉末制备模制品的逐层方法，其中每层的区域通过引入电磁能选择性地融合，使用掩模获得的选择性或通过应用抑制剂，吸收剂或感受体或聚焦所施加的能量，以及以所述方式制备的模制品。

12. 发明授权

US10040938B2 Moulding compound based on a partially aromatic copolyamide 有权
公开(公告)号：US10040938B2
公开(公告)日：2018-08-07
申请号：US14489612
申请日：2014-09-18
申请人： Jasmin Nitsche , Harald Haeger , Sebastian Geerkens , Franz-Erich Baumann , Reinhard Beuth
发明人： Jasmin Nitsche , Harald Haeger , Sebastian Geerkens , Franz-Erich Baumann , Reinhard Beuth
IPC分类号： C08L77/10 , C08L77/06 , C08K3/16 , C08K5/00 , C08K5/18
CPC分类号： C08L77/06 , C08K3/16 , C08K5/005 , C08K5/18 , C08L2201/08 , C08L2203/18 , Y10T428/1352 , Y10T428/139 , Y10T428/1393 , Y10T428/1397
摘要： A moulding composition contains at least 40 wt % of components a) and b). Based on the sum of components a) and b), there are 60-99 wt % of component a) and 40-1 wt % of component b). Component a) is a partially aromatic copolyamide containing, as polymerized monomer units, 30-90 mol % of a combination of hexamethylenediamine and terephthalic acid and 70-10 mol % of a combination of hexamethylenediamine and a linear aliphatic dicarboxylic acid having 8-19 C atoms. Component b) is an olefinic copolymer containing, as polymerized monomer units, i) 35-94.9 wt % of ethene-based monomer units, ii) 5-65 wt % of monomer units based on a 1-alkene having 4-8 C atoms, iii) 0-10 wt % of monomer units based on an olefin different from i) and ii), and iv) 0.1-2.5 wt % of monomer units based on an aliphatically unsaturated dicarboxylic acid anhydride, where the sum of wt % of i), ii), iii) and iv) is 100%.

13. 发明授权

US08604227B2 Process for preparing linear alpha,omega-dicarboxylic diesters 失效
标题翻译：制备线性α，ω-二羧酸二酯的方法
公开(公告)号：US08604227B2
公开(公告)日：2013-12-10
申请号：US13634111
申请日：2010-11-19
申请人： Frank-Martin Petrat , Franz-Erich Baumann , Harald Haeger , Guido Walther , Andreas Martin , Angela Koeckritz
发明人： Frank-Martin Petrat , Franz-Erich Baumann , Harald Haeger , Guido Walther , Andreas Martin , Angela Koeckritz
IPC分类号： C07C51/10
CPC分类号： C07C67/38 , C07C69/34
摘要： The invention provides a process for preparing linear alpha,omega-dicarboxylic diesters by reacting a triglyceride containing fatty acid residues having monounsaturated or polyunsaturated carbon chains with carbon monoxide, an acid and an OH-group donor in one reaction step in the presence of a catalyst.
摘要翻译：本发明提供了通过在一个反应步骤中在催化剂存在下使含有单不饱和或多不饱和碳链的脂肪酸残基与一氧化碳，酸和OH-给体的甘油三酯反应制备线性α，ω-二羧酸二酯的方法。

14. 发明申请

US20130006005A1 PROCESS FOR PREPARING LINEAR ALPHA,OMEGA-DICARBOXYLIC DIESTERS 失效
标题翻译：制备线性阿尔法，欧米茄二氧化硅胶的方法
公开(公告)号：US20130006005A1
公开(公告)日：2013-01-03
申请号：US13634111
申请日：2010-11-19
申请人： Frank-Martin Petrat , Franz-Erich Baumann , Harald Haeger , Guido Walther , Andreas Martin , Angela Koeckritz
发明人： Frank-Martin Petrat , Franz-Erich Baumann , Harald Haeger , Guido Walther , Andreas Martin , Angela Koeckritz
IPC分类号： C07C67/36
CPC分类号： C07C67/38 , C07C69/34
摘要： The invention provides a process for preparing linear alpha,omega-dicarboxylic diesters by reacting a triglyceride containing fatty acid residues having monounsaturated or polyunsaturated carbon chains with carbon monoxide, an acid and an OH-group donor in one reaction step in the presence of a catalyst.
摘要翻译：本发明提供了通过在一个反应步骤中在催化剂存在下使含有单不饱和或多不饱和碳链的脂肪酸残基与一氧化碳，酸和OH-给体的甘油三酯反应制备线性α，ω-二羧酸二酯的方法。

15. 发明授权

US08470433B2 Transparent decoratable multilayer film 有权
标题翻译：透明可装饰多层膜
公开(公告)号：US08470433B2
公开(公告)日：2013-06-25
申请号：US11816588
申请日：2006-01-04
申请人： Harald Haeger , Michael Beyer , Franz-Erich Baumann
发明人： Harald Haeger , Michael Beyer , Franz-Erich Baumann
IPC分类号： B32B27/34 , B32B7/02
CPC分类号： B32B27/34 , B32B27/08 , B32B2250/24 , B32B2307/412 , B32B2307/75 , B32B2519/00 , C08L23/0846 , C08L23/0869 , C08L23/0884 , C08L23/0892 , C08L77/00 , C08L77/10 , Y10T428/24942 , Y10T428/2495 , Y10T428/24975 , Y10T428/31725 , Y10T428/31728 , C08L2666/06 , C08L2666/04
摘要： A multi layer film which comprises the following layers: I. an upper layer composed of a polyamide molding composition which is transparent at the selected layer thickness, and II. a lower layer composed of a polyamide molding composition which comprises the following components: a) from 70 to 99% by weight of a polyamide selected from a group of polyamides and copolyamides, as described, b) from 1 to 30% by weight of a copolymer which contains units of the following monomers: α) from 20 to 94.5% by weight of one or more α-olefins having from 2 to 12 carbon atoms, β) from 5 to 79.5% by weight of one or more acrylic compounds, γ) from 0 to 50% by weight of an olefinically unsaturated epoxide, carboxylic anhydride, carboximide, oxazoline, or oxazinone, and has good printability and adhesive-bondability and transparency, and can be used, for example, as an overcoating for skis.
摘要翻译：一种多层膜，包括以下层：I.由选择层厚度为透明的聚酰胺模塑组合物构成的上层，II。由聚酰胺模塑组合物组成的下层，其包含以下组分：a）70至99重量％的选自聚酰胺和共聚酰胺的聚酰胺，如所述，b）1至30重量％的共聚物，其包含以下单体的单元：α）20至94.5重量％的一种或多种具有2至12个碳原子的α-烯烃，β）5至79.5重量％的一种或多种丙烯酸化合物，γ ）0〜50重量％的烯属不饱和环氧化物，羧酸酐，甲脒，恶唑啉或恶嗪酮，并且具有良好的印刷性和粘合性和透明性，并且可以用作例如滑雪板的外涂层。

16. 发明申请

US20120203033A1 PREPARATION OF PRIMARY DIAMINES HAVING A LINEAR MAIN CHAIN FOR POLYAMIDE SYNTHESES 失效
标题翻译：具有聚酰胺合成线性主链的主要原料的制备
公开(公告)号：US20120203033A1
公开(公告)日：2012-08-09
申请号：US13364493
申请日：2012-02-02
申请人： Franz-Erich Baumann , Matthias Ullrich , Martin Roos , Peter Hannen , Frank-Martin Petrat , Harald Haeger , Angela Koeckritz , Guido Walther , Jens Deutsch , Andreas Martin
发明人： Franz-Erich Baumann , Matthias Ullrich , Martin Roos , Peter Hannen , Frank-Martin Petrat , Harald Haeger , Angela Koeckritz , Guido Walther , Jens Deutsch , Andreas Martin
IPC分类号： C07C209/16 , C07C209/84
CPC分类号： C07C209/16 , Y02P20/544 , C07C211/09
摘要： The invention provides a method to produce primary diamines by catalytic conversion of diols having a linear main chain of from 4 to 31 carbon atoms into the corresponding diamines. The reaction is conducted in a liquid or supercritical phase and is catalyzed by a homogeneous ruthenium-containing complex. The primary diamines obtained may be suitable for polyamide syntheses.
摘要翻译：本发明提供了通过将具有4至31个碳原子的直链主链的二醇催化转化成相应的二胺来生产伯胺的方法。该反应在液相或超临界相中进行，并由均匀的含钌络合物催化。所得到的伯胺可适用于聚酰胺合成。

17. 发明授权

US08871862B2 Molding compound on the basis of a copolyamide containing terephthalic acid and trimethylhexamethylene diamine units 有权
标题翻译：基于含有对苯二甲酸和三甲基六亚甲基二胺单元的共聚酰胺的成型化合物
公开(公告)号：US08871862B2
公开(公告)日：2014-10-28
申请号：US13377949
申请日：2010-07-08
申请人： Andreas Pawlik , Martin Roos , Franz-Erich Baumann , Harald Haeger
发明人： Andreas Pawlik , Martin Roos , Franz-Erich Baumann , Harald Haeger
IPC分类号： C08L77/00 , C08G69/26 , C08L77/06
CPC分类号： C08G69/265 , C08L77/06
摘要： A molding compound, containing at least 30% by weight of a copolyamide, which is derived from the following monomers: a) 50 to 95 mole percent of the combination of a diamine, selected from the group consisting of 1,9-nonane diamine, 1,10-decane diamine, 1,11-undecane diamine and 1,12-dodecane diamine, and terephthalic acid, and b) 5 to 50 mole percent of the combination of a diamine, selected from the group consisting of 2,2,4-trimethylhexamethylene diamine, 2,4,4-trimethylhexamethylene diamine, and mixtures thereof, and terephthalic acid. The copolyamide is crystalline and has low water absorption.
摘要翻译：含有至少30重量％的共聚酰胺的模制化合物，其衍生自以下单体：a）50-95摩尔％的二胺的组合，其选自1,9-壬二胺， 1,10-癸烷二胺，1,11-十一烷二胺和1,12-十二烷二胺和对苯二甲酸，以及b）5至50摩尔％的二胺的组合，其选自2,2， 4-三甲基六亚甲基二胺，2,4,4-三甲基六亚甲基二胺及其混合物和对苯二甲酸。共聚酰胺是结晶的，吸水率低。

18. 发明授权

US08232333B2 Process for producing ultrafine powders based on polyamides, ultrafine polyamide powders and their use 有权
标题翻译：用于生产基于聚酰胺，超细聚酰胺粉末的超细粉末及其用途的方法
公开(公告)号：US08232333B2
公开(公告)日：2012-07-31
申请号：US12089998
申请日：2006-10-12
申请人： Harald Haeger , Franz-Erich Baumann , Wolfgang Lortz , Christoph Batz-Sohn
发明人： Harald Haeger , Franz-Erich Baumann , Wolfgang Lortz , Christoph Batz-Sohn
IPC分类号： C08J3/215 , C08J3/12 , C08K3/22 , C08K5/49
CPC分类号： C08J3/12 , C08J3/128 , C08J3/14 , C08J2377/00 , C09D177/00 , Y10S524/904
摘要： Process for preparing ultrafine powders based on polyamides by contacting polyamides having a relative solution viscosity ηrel in the range from 1.5 to 2.0, measured in 0.5% m-cresol solution at 25° C., with an alcoholic medium in the presence of inorganic particles under the action of pressure and/or temperature to generate an at least partial solution, and then precipitating the polyamide from the at least partial solution, characterized in that a suspension of the inorganic particles suspended in the alcoholic medium is used. The resulting ultrafine polyamide powders have a specific BET surface area in the range of 5-100 m2/g; a fineness d50 of less than 70 μm; an apparent density AD in the range from 250 to 1000 g/l; and a particle content of 0.1 to 80% by weight of inorganic particles based on the total weight of the polyamide powder. They are equally suitable for coatings and for moldings and components with improved mechanical properties.
摘要翻译：通过使具有相对溶液粘度和相对浓度的相对比例在1.5至2.0的范围内的聚酰胺制备基于聚酰胺制备的超细粉末的方法，其在25℃的0.5％间甲酚溶液中，在无机物存在下用醇介质颗粒在压力和/或温度的作用下产生至少部分溶液，然后从至少部分溶液沉淀聚酰胺，其特征在于使用悬浮在醇介质中的无机颗粒的悬浮液。所得的超细聚酰胺粉末的比BET比表面积在5-100m 2 / g的范围内; 细度d50小于70μm; 在250〜1000g / l范围内的表观密度AD; 和基于聚酰胺粉末的总重量的无机颗粒的0.1〜80重量％的颗粒含量。它们同样适用于具有改善的机械性能的涂料和模制品和组分。

19. 发明申请

US20120095161A1 MOLDING COMPOUND ON THE BASIS OF A COPOLYAMIDE CONTAINING TEREPHTHALIC ACID AND TRIMETHYLHEXAMETHYLENE DIAMINE UNITS 有权
标题翻译：含有十五烷酸和三甲基乙酰胺二胺单体的共聚酰胺的成型化合物
公开(公告)号：US20120095161A1
公开(公告)日：2012-04-19
申请号：US13377949
申请日：2010-07-08
申请人： Andreas Pawlik , Martin Roos , Franz-Erich Baumann , Harald Haeger
发明人： Andreas Pawlik , Martin Roos , Franz-Erich Baumann , Harald Haeger
IPC分类号： C08L77/06 , C08G69/26
CPC分类号： C08G69/265 , C08L77/06
摘要： A molding compound, containing at least 30% by weight of a copolyamide, which is derived from the following monomers: a) 50 to 95 mole percent of the combination of a diamine, selected from the group consisting of 1,9-nonane diamine, 1,10-decane diamine, 1,11-undecane diamine and 1,12-dodecane diamine, and terephthalic acid, and b) 5 to 50 mole percent of the combination of a diamine, selected from the group consisting of 2,2,4-trimethylhexamethylene diamine, 2,4,4-trimethylhexamethylene diamine, and mixtures thereof, and terephthalic acid. The copolyamide is crystalline and has low water absorption.
摘要翻译：含有至少30重量％的共聚酰胺的模制化合物，其衍生自以下单体：a）50-95摩尔％的二胺的组合，其选自1,9-壬二胺， 1,10-癸烷二胺，1,11-十一烷二胺和1,12-十二烷二胺和对苯二甲酸，以及b）5至50摩尔％的二胺的组合，其选自2,2， 4-三甲基六亚甲基二胺，2,4,4-三甲基六亚甲基二胺及其混合物和对苯二甲酸。共聚酰胺是结晶的，吸水率低。

20. 发明授权

US06391982B1 Highly branched polyamide graft copolymers 有权
标题翻译：高分支聚酰胺接枝共聚物
公开(公告)号：US06391982B1
公开(公告)日：2002-05-21
申请号：US09605874
申请日：2000-06-29
申请人： Harald Haeger , Ralf Richter , Georg Oenbrink
发明人： Harald Haeger , Ralf Richter , Georg Oenbrink
IPC分类号： C08G7304
CPC分类号： C08G69/26 , C08G69/02 , C08G69/48 , Y10S424/16
摘要： A graft copolymer is prepared by a process comprising: graft polymerizing a polyamide-forming monomer selected from the group consisting of lactams and &ohgr;-aminocarboxylic acids and an oligocarboxylic acid selected from the group consisting of from 0.015 to about 3 mol. % of dicarboxylic acid and from 0.01 to about 1.2 mol. % of tricarboxylic acid, in each case the stated amounts of oligocarboxylic acid based on a molar amount of lactam, &ohgr;-aminocarboxylic acid or combination thereof, onto from 0.5 to 25% by weight, based on the graft copolymer, of a polyamine having at least 11 nitrogen atoms and a number-average molecular weight Mn of at least 500 g/mol., wherein the amino group concentration in the graft copolymer ranges from 100 to 2500 mmol./kg.
摘要翻译：接枝共聚物通过以下方法制备，该方法包括：将选自内酰胺和ω-氨基羧酸的聚酰胺形成单体和选自0.015至约3mol的寡羧酸接枝聚合。％的二羧酸和0.01至约1.2mol。％的三羧酸，在每种情况下，所述量的基于内酰胺，ω-氨基羧酸或其组合的摩尔量的寡羧酸的量为基于接枝共聚物的0.5至25重量％的多胺，其具有至少11个氮原子和数均分子量Mn为至少500g / mol，其中接枝共聚物中的氨基浓度范围为100-2500mmol / kg。

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