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    • 13. 发明申请
    • SILICA GLASS CRUCIBLE, METHOD OF MANUFACTURING THE SAME AND PULLING METHOD
    • 二氧化硅玻璃巧克力,制造方法和拉伸方法
    • US20100319608A1
    • 2010-12-23
    • US12303139
    • 2008-09-29
    • Minoru Kanda
    • Minoru Kanda
    • C30B15/10C03C10/14C30B15/00
    • C03B19/095C30B15/10C30B35/002Y10T117/1024
    • A silica glass crucible including an outer surface layer formed of a bubble-containing silica glass layer and an inner surface layer formed of a silica glass layer whose bubbles are invisible to the naked eye, so as to sufficiently disperse heat from the external radiation thereby preventing temperature irregularity in the silicon melt, and at the same time, exhibit excellent heat conductivity thereby giving a uniformly heated state over a wide range in the entire crucible without taking a long time for increasing the temperature to form a silicon melt, wherein an intermediate layer is interposed between the outer surface layer and the inner surface layer while in the intermediate layer, a bubble-containing silica glass layer (bubble-containing layer) including bubbles with a diameter of 100 μm or smaller by 0.1% or more in the volumetric bubble content and a silica glass layer (transparent glass layer) including the bubbles by 0.05% or less in the volumetric bubble content are laminated.
    • 一种二氧化硅玻璃坩埚,其包括由含气泡的石英玻璃层形成的外表面层和由石墨玻璃层形成的内表面层,所述内表面层的气泡对肉眼不可见,从而充分地分散来自外部辐射的热量,从而防止 硅熔体中的温度不均匀性,并且同时显示出优异的导热性,从而在整个坩埚中在宽范围内均匀地加热状态,而不需要较长时间来提高温度以形成硅熔体,其中中间层 介于外表面层和内表面层之间,而在中间层中,在体积气泡中包含直径为100μm或更小直径为0.1%或更大的气泡的含气泡石英玻璃层(含气泡层) 含量和包含气泡的二氧化硅玻璃层(透明玻璃层)的体积气泡含量为0.05%以下 ted。
    • 14. 发明申请
    • METHOD AND APPARATUS FOR MANUFACTURING VITREOUS SILICA CRUCIBLE
    • 用于制造维生素二氧化硅可溶性的方法和装置
    • US20100229599A1
    • 2010-09-16
    • US12303134
    • 2008-07-25
    • Takeshi FujitaMinoru Kanda
    • Takeshi FujitaMinoru Kanda
    • C03C1/00
    • C03B19/095C30B15/10
    • In order to provide method and apparatus for manufacturing a vitreous silica crucible with little mixing of foreign matter and stable arc during arc melting, the method and apparatus for manufacturing a vitreous silica crucible have a device which blows off air from the side of arc electrodes toward a melting space of a mold, and air discharge ports which discharge the air within the heating furnace, and perform forced supply of air into the melting space during melting to make the atmospheric pressure of the melting space higher than the surroundings, and preferably, form an air pressure difference of 100 Pa or more between the melting space and the surroundings, thereby performing melting.
    • 为了提供在电弧熔化期间少量异物混合和稳定电弧的制造石英玻璃坩埚的方法和装置,用于制造石英玻璃坩埚的方法和装置具有从电弧电极的侧面吹出空气的装置 模具的熔化空间和排出加热炉内的空气的排气口,并且在熔融期间强制地将空气送入熔融空间,使熔融空间的大气压力高于周围环境,优选形成 熔融空间与周围环境之间的空气压差为100Pa以上,进行熔融。
    • 18. 发明授权
    • Method for purification of silica particles, purifier, and purified silica particles
    • 纯化二氧化硅颗粒,净化剂和纯化二氧化硅颗粒的方法
    • US08506890B2
    • 2013-08-13
    • US13047433
    • 2011-03-14
    • Minoru KandaYoshiyuki Tsuji
    • Minoru KandaYoshiyuki Tsuji
    • B01J8/24B01J19/08
    • C01B33/18B01J8/1836B01J8/42B01J2208/00407B01J2208/00415B03C1/288B03C1/30B03C1/32B03C2201/16B03C2201/18C03C1/02
    • To provide a treatment method having excellent purification effect, in which impurities having high ionicity in a silica powder can be removed in a short time, an apparatus thereof, and a purified silica powder. A purification method of a silica powder comprises making a silica powder into a fluid state; contacting a purified gas to the silica powder in the fluid state at high temperature; and thereby removing impurity components of the silica powder. In the method, the silica powder in the fluid state is positioned in a magnetic field region. Further, the silica powder is contacted with the purified gas, while applying voltage to the silica powder by an electric field generated by moving of the silica powder. Preferably, the silica powder in a fluid state is positioned in the magnetic region of 10 gausses or more, and contacted with the purification gas at a temperature of I000° C. or more.
    • 为了提供具有优异的纯化效果的处理方法,其中可以在短时间内除去二氧化硅粉末中的高离子性的杂质,其装置和纯化的二氧化硅粉末。 二氧化硅粉末的纯化方法包括将二氧化硅粉末制成流体状态; 在高温下将纯化气体以流体状态与二氧化硅粉末接触; 从而除去二氧化硅粉末的杂质成分。 在该方法中,处于流体状态的二氧化硅粉末位于磁场区域中。 此外,二氧化硅粉末与纯化气体接触,同时通过二氧化硅粉末移动产生的电场向二氧化硅粉末施加电压。 优选地,处于流体状态的二氧化硅粉末位于10高斯或更高的磁性区域中,并且在1000℃以上的温度下与净化气体接触。
    • 19. 发明授权
    • Method and apparatus for manufacturing vitreous silica crucible
    • 石英玻璃坩埚的制造方法和装置
    • US08196429B2
    • 2012-06-12
    • US12303134
    • 2008-07-25
    • Takeshi FujitaMinoru Kanda
    • Takeshi FujitaMinoru Kanda
    • C03B19/01
    • C03B19/095C30B15/10
    • In order to provide method and apparatus for manufacturing a vitreous silica crucible with little mixing of foreign matter and stable arc during arc melting, the method and apparatus for manufacturing a vitreous silica crucible have a device which blows off air from the side of arc electrodes toward a melting space of a mold, and air discharge ports which discharge the air within the heating furnace, and perform forced supply of air into the melting space during melting to make the atmospheric pressure of the melting space higher than the surroundings, and preferably, form an air pressure difference of 100 Pa or more between the melting space and the surroundings, thereby performing melting.
    • 为了提供在电弧熔化期间少量异物混合和稳定电弧的制造石英玻璃坩埚的方法和装置,用于制造石英玻璃坩埚的方法和装置具有从电弧电极的侧面吹出空气的装置 模具的熔化空间和排出加热炉内的空气的排气口,并且在熔融期间强制地将空气送入熔融空间,使熔融空间的大气压力高于周围环境,优选形成 熔融空间与周围环境之间的空气压差为100Pa以上,进行熔融。
    • 20. 发明授权
    • Method for purification of silica particles, purifier, and purified silica particles
    • 纯化二氧化硅颗粒,净化剂和纯化二氧化硅颗粒的方法
    • US07935326B2
    • 2011-05-03
    • US11995694
    • 2006-10-25
    • Minoru KandaYoshiyuki Tsuji
    • Minoru KandaYoshiyuki Tsuji
    • C01B33/12
    • C01B33/18B01J8/1836B01J8/42B01J2208/00407B01J2208/00415B03C1/288B03C1/30B03C1/32B03C2201/16B03C2201/18C03C1/02
    • To provide a treatment method having excellent purification effect, in which impurities having high ionicity in a silica powder can be removed in a short time, a apparatus thereof, and a purified silica powder.A purification method of a silica powder comprises: making a silica powder into a fluid state; contacting a purified gas to the silica powder in the fluid state at high temperature; and thereby removing impurity components of the silica powder. In the method, the silica powder in the fluid state is positioned in a magnetic field region. Further, the silica powder is contacted with the purified gas, while applying voltage to the silica powder by an electric field generated by moving of the silica powder. Preferably, the silica powder in a fluid state is positioned in the magnetic region of 10 gausses or more, and contacted with the purification gas at a temperature of 1000° C. or more.
    • 为了提供具有优异的净化效果的处理方法,其中可以在短时间内除去二氧化硅粉末中的高离子性的杂质,其装置和纯化的二氧化硅粉末。 二氧化硅粉末的净化方法包括:将二氧化硅粉末制成流体状态; 在高温下将纯化气体以流体状态与二氧化硅粉末接触; 从而除去二氧化硅粉末的杂质成分。 在该方法中,处于流体状态的二氧化硅粉末位于磁场区域中。 此外,二氧化硅粉末与纯化气体接触,同时通过二氧化硅粉末移动产生的电场向二氧化硅粉末施加电压。 优选地,处于流体状态的二氧化硅粉末位于10高斯或更高的磁性区域中,并且在1000℃以上的温度下与净化气体接触。