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11. 发明授权

US4619667A Method for increasing color density and improving color fastness of dyed fabrics 失效
标题翻译：提高染色密度和提高染色织物色牢度的方法
公开(公告)号：US4619667A
公开(公告)日：1986-10-28
申请号：US743506
申请日：1985-06-11
申请人： Susumu Ueno , Hirokazu Nomura , Shinobu Hashizume , Toshiaki Nishide
发明人： Susumu Ueno , Hirokazu Nomura , Shinobu Hashizume , Toshiaki Nishide
IPC分类号： D06M10/02 , D06P5/02 , D06P5/20
CPC分类号： D06P5/02 , D06M10/025 , D06P5/2016 , D06M2101/32
摘要： The invention provides a method for increasing the color density of a dyed fabric material of, especially, a synthetic fiber as well as the fastness of the color to rubbing and washing. The inventive method comprising (a) pretreating the dyed fabric material with an organopolysiloxane which is an amino-modified organopolysiloxane or a dimethylpolysiloxane, and then (b) exposing the thus pretreated dyed fabric material to low temperature plasma of an inorganic gas under a reduced pressure. The inorganic gas is preferably oxygen or a gaseous mixture containing at least 10% by volume of oxygen. The color-deepening effect is particularly remarkable when the color of the dyed fabric material is black to impart increased graveness and vividness of the color.
摘要翻译：本发明提供了提高特别是合成纤维的染色织物材料的色密度以及颜色摩擦和洗涤牢度的方法。本发明的方法包括（a）用有机聚硅氧烷（其是氨基改性的有机聚硅氧烷或二甲基聚硅氧烷）预处理染色的织物材料，然后（b）将如此预处理的染色织物材料暴露于减压下的无机气体的低温等离子体。无机气体优选为氧气或含有至少10体积％氧气的气体混合物。当染色织物的颜色为黑色以增加颜色的鲜艳度和鲜艳度时，颜色加深效果特别显着。

12. 发明授权

US4317788A Method for modifying surface properties of a shaped article of an acrylic resin 失效
标题翻译：改进丙烯酸树脂成型制品表面性能的方法
公开(公告)号：US4317788A
公开(公告)日：1982-03-02
申请号：US230542
申请日：1981-02-02
申请人： Kiyoshi Imada , Susumu Ueno , Yasuhide Nishina , Hirokazu Nomura
发明人： Kiyoshi Imada , Susumu Ueno , Yasuhide Nishina , Hirokazu Nomura
IPC分类号： C08J7/00 , B29C59/14 , B29C71/00 , B29C71/04 , C08F6/26 , C08J7/06 , C08L25/04 , C08L33/08 , B29C25/00
CPC分类号： C08J7/123 , B29C59/14 , B29K2033/04 , C08J2333/00 , C08J2333/06
摘要： A novel method is proposed for improving the surface properties or, in particular, for increasing the affinity to water of and for reducing accumulation of static electricity on the surface of a shaped article made of an acrylic resin. The inventive method comprises first exposing the surface of the shaped article to low temperature plasma of a gas having no polymerizability in plasma and then bringing the plasma-treated surface into contact with an aqueous solution containing a surface active agent. The effect of the inventive method is so strong and durable that the treated surface remains antistatic even 6 months after the treatment.
摘要翻译：提出了一种改进表面性质，特别是提高由丙烯酸树脂制成的成型制品的表面上的水的亲和力并减少静电累积的新方法。本发明的方法包括首先将成形制品的表面暴露于等离子体中不具有聚合性的气体的低温等离子体，然后使等离子体处理的表面与含有表面活性剂的水溶液接触。本发明方法的效果如此强烈和耐用，使得经处理的表面在治疗后6个月仍然保持抗静电。

13. 发明授权

US4272464A Method for preventing plasticizer bleeding on polyvinyl chloride shaped articles 失效
标题翻译：防止聚氯乙烯制品上增塑剂渗色的方法
公开(公告)号：US4272464A
公开(公告)日：1981-06-09
申请号：US051151
申请日：1979-06-22
申请人： Michihiko Asai , Yoshio Suda , Kiyoshi Imada , Susumu Ueno , Hirokazu Nomura
发明人： Michihiko Asai , Yoshio Suda , Kiyoshi Imada , Susumu Ueno , Hirokazu Nomura
IPC分类号： C08L27/00 , B29D7/01 , B29D23/00 , C08G18/00 , C08J3/28 , C08J7/00 , C08L1/00 , C08L27/06 , C08L33/00 , C08L33/02 , C08L75/00 , C08L75/04 , H05B7/00
CPC分类号： C08J7/123 , C08J2327/06
摘要： A method for preventing bleeding of plasticizers on the surface of shaped articles of plasticized polyvinyl chloride resins. The method comprises the steps of (a) blending a urethane elastomer with the polyvinyl chloride resin together with the plasticizer and other optional additives prior to fabrication of the polyvinyl chloride resin composition into shaped articles, (b) fabricating the resin composition into desired shaped articles, and (c) subjecting the thus shaped article to a treatment with low temperature plasma of a gas. Carbon monoxide is preferred as the gas for the plasma atmosphere.
摘要翻译：防止增塑剂在塑化聚氯乙烯树脂的成型制品表面渗出的方法。该方法包括以下步骤：（a）在将聚氯乙烯树脂组合物制成成型制品之前，将聚氨酯弹性体与聚氯乙烯树脂与增塑剂和其它任选的添加剂一起混合，（b）将树脂组合物制成所需成型制品，和（c）使这样成型的制品经气体的低温等离子体处理。作为等离子体气氛的气体，优选一氧化碳。

14. 发明授权

US4247440A Method for preventing plasticizer bleeding on polyvinyl chloride shaped articles 失效
标题翻译：防止聚氯乙烯制品上增塑剂渗色的方法
公开(公告)号：US4247440A
公开(公告)日：1981-01-27
申请号：US59756
申请日：1979-07-23
申请人： Michihiko Asai , Yoshio Suda , Kiyoshi Imada , Susumu Ueno , Hirokazu Nomura
发明人： Michihiko Asai , Yoshio Suda , Kiyoshi Imada , Susumu Ueno , Hirokazu Nomura
IPC分类号： C08J7/00 , B29C59/14 , B29C71/04 , C08J3/18 , C08J3/28 , C08J7/12 , C08J7/18 , C08K5/09 , C08K5/10 , C08K5/12 , C08L27/06
CPC分类号： C08J7/123 , C08J2327/06
摘要： In the inventive method, shaped articles of a plasticized polyvinyl chloride resin are subjected to the surface treatment by with low temperature plasma so that the undesirable phenomenon of bleeding of the plasticizer on the surface can be effectively prevented when the plasticizer for plasticizing the resin is a compound having at least one aromatic nucleus in a molecule or a combination of two or more of plasticizers including 10% by weight or more of a plasticizer which is a compound having at least one aromatic nucleus in a molecule.
摘要翻译：在本发明的方法中，通过低温等离子体对塑化聚氯乙烯树脂的成型制品进行表面处理，从而当用于增塑树脂的增塑剂为化合物在分子中具有至少一个芳香核，或两种或多种增塑剂的组合，包括10重量％以上的增塑剂，其是在分子中具有至少一个芳香核的化合物。

15. 发明授权

US4639379A Method for the improvement of antistatic performance of synthetic resin shaped articles 失效
标题翻译：提高合成树脂成型制品抗静电性能的方法
公开(公告)号：US4639379A
公开(公告)日：1987-01-27
申请号：US743874
申请日：1985-06-11
申请人： Michihiko Asai , Yukio Shimura , Keishiro Tsuda , Susumu Ueno , Hirokazu Nomura , Kiyoshi Imada
发明人： Michihiko Asai , Yukio Shimura , Keishiro Tsuda , Susumu Ueno , Hirokazu Nomura , Kiyoshi Imada
IPC分类号： C08J7/00 , B05D3/06 , B05D7/26 , B29C71/04 , C08J7/04 , C08J7/12 , C08J7/18 , C08K5/54 , C08L25/04 , C08L77/00
CPC分类号： C08J7/123
摘要： The invention provides a very efficient method for the improvement of the antistatic performance, e.g. decrease in the accumulation of static electricity on the surface and decrease in the surface resistivity, of a synthetic resin shaped article with outstanding durability of the effect. The method comprises two steps in principle, first of which is the formation of a crosslinked layer in the surface portion of the shaped article by a variety of known methods effective for the formation of crosslinks in polymeric materials and the second of which is the exposure of the thus crosslinked surface of the article to low temperature plasma produced in an atmosphere containing a gaseous silicon-containing compound which may be a silane compound or a low-molecular weight vaporizable siloxane compound to form a plasma-polymerized surface film of the silicon compound on the crosslinked layer.
摘要翻译：本发明提供了用于提高抗静电性能的非常有效的方法，例如，具有突出的耐久性的合成树脂成型制品的表面静电积聚减少，表面电阻率降低。该方法原则上包括两个步骤，其中首先是在成型制品的表面部分中通过各种已知的方法形成交联层，所述方法有效地在聚合物材料中形成交联，其中第二步是暴露于将这样交联的制品的表面在含有气态含硅化合物的气氛中产生的低温等离子体，所述气体含硅化合物可以是硅烷化合物或低分子量可汽化硅氧烷化合物，以形成硅化合物的等离子体聚合表面膜交联层。

16. 发明授权

US4637851A Method for the preparation of a laminate 失效
标题翻译：层压制品的制备方法
公开(公告)号：US4637851A
公开(公告)日：1987-01-20
申请号：US819694
申请日：1986-01-17
申请人： Susumu Ueno , Kouiti Kuroda , Hirokazu Nomura , Shigeru Tateno
发明人： Susumu Ueno , Kouiti Kuroda , Hirokazu Nomura , Shigeru Tateno
IPC分类号： B29C59/14 , B32B5/28 , C08J5/06 , D06M10/02 , H05K1/03 , B32B31/00 , B29C17/08
CPC分类号： D06M10/025 , B29C59/14 , B32B5/28 , C08J5/06 , H05K1/0366 , B29C2059/147 , B29C70/34 , B29K2063/00 , B29K2079/00 , B29K2105/0809 , B29K2277/00 , B29K2277/10 , B29K2313/00 , D06M2101/36 , D06M2200/00 , D06M2200/50 , H05K2201/0154 , H05K2201/0278 , H05K2203/095
摘要： A method is proposed for the preparation of a laminate with improved mechanical strength such as the cloth-to-cloth adhesive bonding strength using a prepreg based on a fabric sheet of aromatic polyamide fibers and an adhesive preferably selected from polyimide-based and epoxy resin-based adhesives, in which the fabric sheet is pretreated by exposure to low-temperature plasma of preferably a gas mixture composed of oxygen and nitrogen under a reduced pressure of 0.5 to 20 Torr. The improvement is derived presumably from the increase in the wettability and affinity of the fibers to the adhesive as is suggested by the remarkable increase of adhesive pick-up.
摘要翻译：提出了使用基于芳香族聚酰胺纤维的织物片的预浸料坯和优选选自聚酰亚胺类和环氧树脂粘合剂的粘合剂来制备具有改善的机械强度的层压体的方法，例如布 - 布粘合剂粘合强度，其中织物片通过在0.5至20托的减压下暴露于优选由氧和氮组成的气体混合物的低温等离子体进行预处理。推测可以从纤维对粘合剂的润湿性和亲和性的增加推导出改进，这是由于粘合剂拾取显着增加所提出的。

17. 发明授权

US4601911A Method for increasing hydrophilicity of a fabric material of synthetic fibers 失效
标题翻译：提高合成纤维织物材料亲水性的方法
公开(公告)号：US4601911A
公开(公告)日：1986-07-22
申请号：US743505
申请日：1985-06-11
申请人： Susumu Ueno , Hirokazu Nomura , Shinobu Hashizume , Toshiaki Nishide
发明人： Susumu Ueno , Hirokazu Nomura , Shinobu Hashizume , Toshiaki Nishide
IPC分类号： D06M10/08 , B05D1/00
CPC分类号： D06M10/08
摘要： Hydrophilicity of a poorly hydrophilic fabric material of synthetic fibers can be remarkably and durably increased by the synergistic effect of the treatments first with a specific hydrophilic agent, e.g. water-absorbent agent and antistatic agent, and then by exposure to low temperature plasma generated in an atmosphere of oxygen or oxygen-containing gaseous mixture so that the capacity of the fabric material for water absorption is greatly increased and the antistatic performance thereof is greatly improved with decreased surface resistivity and charge voltage induced by rubbing.
摘要翻译：合成纤维的亲水性低的织物材料的亲水性可以通过首先用特定的亲水剂的处理的协同效应来显着地和持久地增加，例如，吸水剂和抗静电剂，然后通过暴露于在氧气或含氧气体混合物的气氛中产生的低温等离子体，使得织物材料吸水的能力大大增加，并且其抗静电性能大大提高具有降低的表面电阻率和由摩擦引起的充电电压。

18. 发明授权

US4395434A Method for improving surface properties of shaped articles of synthetic resins 失效
标题翻译：改善合成树脂成型制品表面性能的方法
公开(公告)号：US4395434A
公开(公告)日：1983-07-26
申请号：US301536
申请日：1981-09-14
申请人： Kiyoshi Imada , Susumu Ueno , Hirokazu Nomura
发明人： Kiyoshi Imada , Susumu Ueno , Hirokazu Nomura
IPC分类号： B29C59/14 , C08J7/12 , B05D3/04 , B08B17/02
CPC分类号： C08J7/123 , B29C59/14 , C08J7/126 , B29K2027/06
摘要： The invention provides a novel and efficient method for modifying the surface properties of a shaped article of a synthetic resin such as a polyvinyl chloride resin in which a remarkable anti-static effect is obtained on the surface so that accumulation of static electricity on the surface is greatly reduced. The inventive method comprises exposing the surface of the shaped article to a low temperature plasma generated in a gaseous atmosphere containing a nitrogen-containing organic compound such as an amine, acid amide, diamine and heterocyclic organic compound having at least one nitrogen atom in a molecule as the ring member at a pressure from 0.001 to 10 Torr. The gas or vapor of the above mentioned nitrogen-containing organic compound is preferably diluted with an inorganic gas. The effectiveness of the above described plasma treatment is further enhanced when the plasma-treated surface of the shaped article is subsequently brought into contact with a halogen, a hydrogen halide or an organic halogen compound, e.g. chlorine, hydrogen chloride, hydrogen bromide and allyl chloride, preferably, in a gaseous phase at a pressure of at least 10 Torr.
摘要翻译：本发明提供了一种用于改变诸如聚氯乙烯树脂的合成树脂的成形制品的表面性能的新型和有效的方法，其中在表面上获得显着的抗静电效果，使得表面上的静电积累是大大减少。本发明的方法包括将成形制品的表面暴露于在含有分子中具有至少一个氮原子的胺，酰胺，二胺和杂环有机化合物的含氮有机化合物的气体气氛中产生的低温等离子体作为在0.001至10托的压力下的环构件。上述含氮有机化合物的气体或蒸气优选用无机气体稀释。当成型制品的等离子体处理表面随后与卤素，卤化氢或有机卤素化合物接触时，上述等离子体处理的效果进一步提高。氯，氯化氢，溴化氢和烯丙基氯，优选在至少10托压力的气相中。

19. 发明授权

US4293585A Method for the preparation of polarizing films or sheets 失效
标题翻译：偏光膜或片材的制备方法
公开(公告)号：US4293585A
公开(公告)日：1981-10-06
申请号：US168082
申请日：1980-07-10
申请人： Kiyoshi Imada , Susumu Ueno , Yasuhide Nishina , Hirokazu Nomura
发明人： Kiyoshi Imada , Susumu Ueno , Yasuhide Nishina , Hirokazu Nomura
IPC分类号： C08J7/00 , B05D5/06 , B29C49/00 , B29C55/00 , B29C55/02 , B29C59/14 , C08J7/04 , C08J7/12 , G02B5/30 , B05D3/06
CPC分类号： C08J7/047 , B05D5/06 , B29C59/14 , C08J7/123 , G02B5/3033 , B29K2027/06 , C08J2327/06 , C08J2429/04 , Y10T428/265 , Y10T428/31928
摘要： The invention provides a novel method for the preparation of a polarizing film or sheet based on a polyvinyl alcohol which is easily prepared and easy to handle. The inventive method comprises first subjecting a substrate film or sheet of a vinyl chloride resin to exposure to low temperature plasma, the surface of the substrate is coated with an aqueous solution of a polyvinyl alcohol and dried so as that a coating layer of the polyvinyl alcohol is formed as firmly bonded to the substrate surface owing to the increased affinity of the surface by the plasma treatment, the thus polyvinyl alcohol-clad substrate is stretched as such unidirectionally and the stretched polyvinyl alcohol layer is treated with iodine to be imparted with a polarizing power. The adhesion between the substrate and the polyvinyl alcohol layer is so strong without an adhesive agent that the difficulty in the prior art in handling fragile stretched polyvinyl alcohol film is completely overcome.
摘要翻译：本发明提供了一种制备基于容易制备并易于处理的聚乙烯醇的偏光膜或片的新方法。本发明的方法包括首先使氯乙烯树脂的基材膜或片材暴露于低温等离子体中，将基材的表面用聚乙烯醇的水溶液涂布并干燥，使得聚乙烯醇的涂层由于通过等离子体处理增加了表面的亲和性，因此形成为牢固地结合到基板表面，因此聚乙烯醇包覆基板单向拉伸，拉伸的聚乙烯醇层用碘处理以赋予极化功率。衬底和聚乙烯醇层之间的粘合力如此强烈，而没有粘合剂，现有技术难以处理脆弱的拉伸聚乙烯醇膜被完全克服。

20. 发明授权

US4261806A Method for the treatment of inner surfaces of a tubular body of a plastic with low temperature plasma 失效
标题翻译：用低温等离子体处理塑料管状体的内表面的方法
公开(公告)号：US4261806A
公开(公告)日：1981-04-14
申请号：US112194
申请日：1980-01-15
申请人： Michihiko Asai , Yoshio Suda , Kiyoshi Imada , Susumu Ueno , Hirokazu Nomura
发明人： Michihiko Asai , Yoshio Suda , Kiyoshi Imada , Susumu Ueno , Hirokazu Nomura
IPC分类号： C08J7/00 , A61L33/00 , B05D7/22 , B29C59/14 , B01K1/00 , B05D3/06
CPC分类号： B05D7/22 , A61L33/0094 , B05D1/62 , B05D3/141 , B05D7/222 , B29C59/142 , B05D2201/00 , B29K2023/00 , B29K2027/06 , B29L2023/22
摘要： The invention provides an effective method for subjecting the inner surface of a tubular body made of a plastic resin to a treatment with low temperature plasma according to which the tubular body is dipped in an insulating oil bath while the inside of the tubular body is filled with a plasma gas under a reduced pressure and electric power for the generation of a low temperature plasma is supplied to electrodes surrounding the tubular body in the insulating oil. Several of the problems in the prior art methods can be solved by the present invention such as undesirable thermal degradation of the tube surface by the evolved by the electric discharge, and power loss due to the generation of plasma outside the tubular body. When the method of the invention is applied to the treatment of a continuous length tubular body, the tubular body is continuously moved in the insulating oil through the electrodes surrounding it, with the optional provision of a sleeve made of an insulating material placed between the electrodes and the tubular body, so as that the tubular body is free from adverse effects caused by direct contact with the electrodes.
摘要翻译：本发明提供了一种有效的方法，用于使由塑料树脂制成的管状体的内表面经受低温等离子体处理，根据该等离子体，管状体浸入绝缘油浴中，同时管状体的内部被填充将用于产生低温等离子体的减压下的等离子体气体和电力供给到绝缘油中的管状体周围的电极。通过本发明可以解决现有技术方法中的几个问题，例如通过放电产生的管表面的不期望的热降解，以及由于在管体外部产生等离子体造成的功率损耗。当将本发明的方法应用于连续长度管状体的处理时，管状体通过围绕它的电极在绝缘油中连续移动，可选地提供由置于电极之间的绝缘材料制成的套筒以及管状体，使得管状体没有与电极直接接触引起的不利影响。

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