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11. 发明授权

US5478803A 3,5-dimethyl-pentenyl-dihydro-2(3H)-furanone isomer mixtures, organoleptic uses thereof, process for preparing same and process intermediates therefor 失效
标题翻译： 3,5-二甲基 - 戊烯基 - 二氢-2（3H） - 呋喃酮异构体混合物，其感官用途，制备方法及其中间体
公开(公告)号：US5478803A
公开(公告)日：1995-12-26
申请号：US330847
申请日：1994-10-27
申请人： Richard M. Boden , William J. Fylak , Marie R. Hanna , Futoshi Fujioka
发明人： Richard M. Boden , William J. Fylak , Marie R. Hanna , Futoshi Fujioka
IPC分类号： C07C69/587 , C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C11D3/50 , C11B9/0076
摘要： Described are 3,5-dimethyl-pentenyl-dihydro-2(3H)-furanone isomer mixtures defined according to the structure: ##STR1## wherein structure represents mixtures wherein in the mixture in each of the compounds, one of the dashed lines represents a carbon-carbon double bond and the other of the dashed lines represents a carbon-carbon single bond, processes for preparing same and uses thereof in augmenting or enhancing the aroma of consumable materials including perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, hair preparations, fabric softeners, fabric softener articles, cosmetic powders and perfumed polymers). Also described is a process for preparing such 3,5-dimethyl-pentenyl-dihydro-2(3H)-furanone isomer mixtures using as a starting material 2,7-octadienol having the structure: ##STR2## as well as the process intermediates having the structures: ##STR3## wherein R represents C.sub.1 -C.sub.4 alkyl; R.sub.1 and R.sub.2 are the same or different and each represents 2,7-octadienyl or R.
摘要翻译：描述的是根据以下结构定义的3,5-二甲基 - 戊烯基 - 二氢-2（3H） - 呋喃酮异构体混合物：其中结构表示混合物，其中在每个化合物的混合物中，虚线之一表示碳 - 碳双键，虚线中的另一个代表碳 - 碳单键，其制备方法及其用于增强或增强消耗材料的香气，包括香料组合物，古龙水和香料制品（例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，毛发制剂，织物柔软剂，织物柔软剂制品，化妆粉和加香聚合物）。还描述了使用具有以下结构的起始原料2,7-辛二烯醇制备这种3,5-二甲基 - 戊烯基 - 二氢-2（3H） - 呋喃酮异构体混合物的方法，以及具有结构：和其中R表示C1-C4烷基; R1和R2相同或不同，各自表示2,7-辛二烯基或R.

12. 发明授权

US5077275A Acylated bicycloalkadiene-compound-containing compositions of matter process for preparing same and perfumery uses thereof 失效
标题翻译：含酰化双环链二烯化合物的物质组合物及其制备方法及其香料用途
公开(公告)号：US5077275A
公开(公告)日：1991-12-31
申请号：US701849
申请日：1991-05-17
申请人： Richard M. Boden , Joseph A. McGhie
发明人： Richard M. Boden , Joseph A. McGhie
IPC分类号： C07C45/45 , C07C49/553 , C07C49/557 , C11B9/00 , C11D3/50
CPC分类号： C07C49/553 , C07C45/455 , C07C49/557 , C11B9/0038 , C11B9/0049 , C11D3/50
摘要： Described are acylated bicycloalkadiene-compound-containing compositions of matter, mixtures of compounds containing predominantly compounds having the structures: ##STR1## with the compositions of matter containing from 50 up to 100% of the compound having the structure: prepared by reacting the compound having the structure: ##STR2## or a mixture containing, predominently, the compound having the structure: with acetic anhydride in the presence of a Lewis acid catalyst such as boron trifluoride etherate.Also described are perfumery uses of such compositions of matter for augmenting or enhancing the aroma of perfume compositions, colognes or perfumed articles such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, cosmetic powders, hair preparations and the like.

13. 发明授权

US5059434A Microwave browning composition and process for producing the same 失效
标题翻译：微波褐变组合物及其制备方法
公开(公告)号：US5059434A
公开(公告)日：1991-10-22
申请号：US596498
申请日：1990-10-12
申请人： Young C. Kang , Chee-Teck Tan , Brian Byrne , Lawrence L. Buckholz, Jr. , Marion A. Sudol , Richard M. Boden
发明人： Young C. Kang , Chee-Teck Tan , Brian Byrne , Lawrence L. Buckholz, Jr. , Marion A. Sudol , Richard M. Boden
IPC分类号： A21D2/24
CPC分类号： A21D2/245
摘要： Described is a process for producing a cooked edibly browned storage-stable fibrous proteinaceous muscle tissue foodstuff including the steps of:(a) providing a particulate flowable flavoring powder which contains individually discretly encapsulated Maillard reaction reagents with the reaction reagents being at least one enxapsulated amino acid and at least one encapsulated sugar;(b) providing an uncooked fibrous proteinaceous muscle tissue foodstuff containing more than 50% water;(c) placing in intimate the contact with at least part of the surface of the foodstuff, a flavor augmenting, imparting or enhancing quantity of the particulate flowable flavoring powder of (a); and(d) exposing the flavoring powder coated foodstuff surface to microwave powder-radiation for a period of time to cause the foodstuff to be ediblewhereby the resulting product is caused to be edible as a foodstuff and the cooked fibrous proteinaceous muscle tissue is edibly browned. Optionally, the particulate flowable flavoring powder may be in the form of a slurry with a solvent composition which is capable of raising the dielectric constant of the foodstuff to be cooked whereby the foodstuff to be cooked is completely cooked and edibly browned in the period of time under 600 seconds.
摘要翻译：描述了一种生产煮熟的可熟化的贮存稳定的纤维蛋白质肌肉组织食品的方法，包括以下步骤：（a）提供颗粒状可流动的调味粉末，其包含单独的离心包裹的美拉德反应试剂，其中反应试剂是至少一个被包封的氨基酸和至少一种包封的糖; （b）提供含有超过50％水的未煮过的纤维蛋白质肌肉组织食物; （c）与食品的表面的至少一部分紧密接触，增加，赋予或增加数量的（a）的颗粒状可流动调味粉末; 和（d）将调味粉末涂覆的食品表面暴露于微波粉末辐射一段时间以使食物可食用，从而使得所得产品作为食品可食用，并且煮熟的纤维蛋白质肌肉组织易于变褐。任选地，颗粒状可流动的调味粉末可以是具有溶剂组成的浆料形式，其可以提高要烹饪的食品的介电常数，从而待烹饪的食物在一段时间内被完全烹饪和柔软地变褐 600秒以下。

14. 发明授权

US4950495A Tetrahydro-5-isopropyl-2-methyl-2-thiophene acetonitrile, organoleptic uses thereof and process for preparing same 失效
公开(公告)号：US4950495A
公开(公告)日：1990-08-21
申请号：US379944
申请日：1989-07-14
申请人： Richard M. Boden , Joseph A. McGhie
发明人： Richard M. Boden , Joseph A. McGhie
IPC分类号： C07C323/54 , C07C327/28 , C07C327/32 , C07D333/24 , C11B9/00
CPC分类号： C11B9/0076 , C07C323/54 , C07C327/28 , C07C327/32 , C07D333/24 , C11B9/0011
摘要： Described is the tetrahydro-5-isopropyl-2-methyl-2-thiophene acetonitrile of our invention having the structure: ##STR1## and organoleptic uses thereof in augmenting or enhancing the aroma or taste of perfume compositions, colognes, perfumed articles, foodstuffs and chewing gums.

15. 发明授权

US4681976A Process for preparing alkyl substituted and unsubstituted para-carboalkoxy cyclohexanones 失效
标题翻译：制备烷基取代和未取代的对 - 烷氧羰基环己酮的方法
公开(公告)号：US4681976A
公开(公告)日：1987-07-21
申请号：US842783
申请日：1986-03-21
申请人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
发明人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
IPC分类号： C08K5/101 , C11B9/00 , C11D3/50 , C07C69/74
CPC分类号： C11D3/50 , C08K5/101 , C11B9/0034
摘要： Described are para-carboalkoxy cyclohexanones defined according to the structure: ##STR1## wherein R.sub.1 represents hydrogen or C.sub.1 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl and uses thereof in augmenting or enhancing the aroma of consumable materials including foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, cosmetic compositions, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers. The compounds defined according to the structure: ##STR2## wherein R.sub.1 ' represents C.sub.4 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl are novel compounds.
摘要翻译：描述了根据以下结构定义的对 - 烷氧基环己酮：其中R 1表示氢或C 1 -C 7烷基，R 2表示甲基或乙基，并且其用于增强或增强消耗材料的香气，包括食品，口香糖，牙膏，药用产品，咀嚼烟草，香水组合物，古龙水和香料制品（例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，化妆品组合物，织物柔软剂组合物，织物柔软剂制品，毛发制剂和加香聚合物。结构：其中R 1'表示C 4 -C 7烷基，R 2表示甲基或乙基是新化合物。

16. 发明授权

US4636333A Alkoxy-substituted polyhydroindan carboxaldehydes 失效
标题翻译：烷氧基取代的多羟基茚满羧醛
公开(公告)号：US4636333A
公开(公告)日：1987-01-13
申请号：US837386
申请日：1986-03-07
申请人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
发明人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
IPC分类号： C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0042 , C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523
摘要： Described is a mixture of polyhydroindan carboxaldehydes defined according to the structure: ##STR1## wherein R.sub.7 represents a moiety selected from the group consisting of methyl and isopropyl prepared by means of reacting bicyclopentadiene with a lower alkanol in the presence of a Lewis acid in order to form a mixture of compounds defined according to the structure: ##STR2## and then reacting the resulting ether with carbon monoxide and hydrogen in the presence of an "oxo" reaction catalyst.
摘要翻译：描述了根据以下结构定义的多羟基茚基甲醛的混合物：其中R 7表示选自甲基和异丙基的部分，其通过在路易斯酸存在下通过双环戊二烯与低级链烷醇反应制备，以便形成根据以下结构定义的化合物的混合物：，然后在“氧代”反应催化剂存在下，使所得的醚与一氧化碳和氢气反应。

17. 发明授权

US4634547A Organoleptic uses of bicyclononenyl alcohols 失效
标题翻译：感官用途的双环壬烯醇
公开(公告)号：US4634547A
公开(公告)日：1987-01-06
申请号：US796430
申请日：1985-11-08
申请人： Richard M. Boden , John R. Helm
发明人： Richard M. Boden , John R. Helm
IPC分类号： C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C11D3/50 , C11B9/0049
摘要： Described are oxobicyclononane derivatives and mixtures of same having the generic structure: ##STR1## wherein X, Y, X' and Y' each represents the moiety having one of the structures: ##STR2## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond with the proviso that when X' and Y' are each the moiety: ##STR3## then the dashed line at the "2-3" position is a carbon-carbon double bond and the dashed line at the "6-7" position is a carbon-carbon single bond and one of X or Y has the structure: ##STR4## and the other of X or Y has the structure: ##STR5## and with the further proviso that when X and Y are the moieties: ##STR6## then the dashed line at the "6-7" position is a carbon-carbon double bond and the dashed line at the "2-3" position is a carbon-carbon single bond and one of X' or Y' has the structure: ##STR7## and the other of X' or Y' has the structure: ##STR8## and wherein R represents hydrogen, C.sub.1 -C.sub.3 acyl or C.sub.1 -C.sub.2 alkoxy carbonyl with the major portion of the mixtures defined according to the generic structure: ##STR9## wherein one of X or Y is the moiety: ##STR10## and the other of X or Y is the moiety: ##STR11## with R being one of hydrogen, C.sub.1 -C.sub.3 acyl or C.sub.1 -C.sub.2 alkoxy carbonyl and uses thereof in augmenting or enhancing the aroma of perfume compositions, perfumed articles, perfumed polymers and colognes.
摘要翻译：描述了具有以下通用结构的氧代二环壬烷衍生物及其混合物：其中X，Y，X'和Y'各自表示具有以下结构之一的部分：其中虚线之一代表碳 - 碳单键，另一个虚线表示碳 - 碳双键，条件是当X'和Y'各自为部分时：“IMAGE”，则“2-3”位的虚线是碳 - 碳双键，“6-7”位置的虚线是碳 - 碳单键，X或Y之一具有以下结构：X或Y具有以下结构：和进一步的条件是当X和Y是部分时：“IMAGE”，则“6-7”位置处的虚线是碳 - 碳双键，“2-3”位的虚线是碳碳单键和X'或Y'之一具有以下结构：X'或Y'具有以下结构：其中R表示氢，C 1-C3酰基或C1-C2烷氧基羰基，其主要部分是根据通用结构定义的混合物：其中X或Y之一为部分：X，Y中的另一个为部分：其中R为氢，C 1 -C 3酰基或C 1 -C 2烷氧基羰基之一，其用于增强或增强香料组合物，香料制品，加香聚合物和古龙水的香气。

18. 发明授权

US4605793A Methyl substituted pinyl oxopentenes, organoleptic uses thereof and process for preparing same 失效
标题翻译：甲基取代的戊基氧代戊烯，其感官用途及其制备方法
公开(公告)号：US4605793A
公开(公告)日：1986-08-12
申请号：US630727
申请日：1984-07-13
申请人： Braja D. Mookherjee , Robert W. Trenkle , Robin K. Wolff , Richard M. Boden , Takao Yoshida
发明人： Braja D. Mookherjee , Robert W. Trenkle , Robin K. Wolff , Richard M. Boden , Takao Yoshida
IPC分类号： C07C33/12 , C07C45/50 , C07C45/74 , C11B9/00 , C07C35/22
CPC分类号： C11B9/0046 , C07C33/12 , C07C45/50 , C07C45/74
摘要： Described is a process for preparing at least one secondary alcohol of the class of methyl substituted pinyl hydroxy pentenes comprising the step of:(i) reacting alpha pinene or beta pinene with a mixture of carbon monoxide and hydrogen in the presence of a hydroformalation catalyst in order to produce at least one methyl substituted pinyl carboxyaldehyde;(ii) reacting the resulting methyl substituted pinyl carboxyaldehyde with methyl ethyl ketone in the presence of a basic catalyst; and(iii) reacting the resulting product with a reducing agent selected from the group consisting of alkali metal borohydrides and lithium aluminum hydride.
摘要翻译：描述了一种制备甲基取代的戊基羟基戊烯类的至少一种仲醇的方法，其包括以下步骤：（i）在一种氢化异构化催化剂存在下，使α-蒎烯或β-蒎烯与一氧化碳和氢气的混合物反应以产生至少一种甲基取代的哌啶基羧基甲醛; （ii）在碱性催化剂存在下使所得甲基取代的吡啶甲酰甲醛与甲基乙基酮反应; 和（iii）使所得产物与选自碱金属硼氢化物和氢化铝锂的还原剂反应。

19. 发明授权

US4591451A Methyl substituted pinyl oxopentenes and organoleptic uses thereof 失效
标题翻译：甲基取代的戊基氧代戊烯及其感官用途
公开(公告)号：US4591451A
公开(公告)日：1986-05-27
申请号：US613569
申请日：1984-05-24
申请人： Braja D. Mookherjee , Robert W. Trenkle , Robin K. Wolff , Richard M. Boden , Takao Yoshida
发明人： Braja D. Mookherjee , Robert W. Trenkle , Robin K. Wolff , Richard M. Boden , Takao Yoshida
IPC分类号： A24B15/34 , C07C45/50 , C07C45/74 , C07C49/21 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0046 , A24B15/34 , A24B15/345 , C07C45/50 , C07C45/74 , C07C49/21 , C11B9/0034
摘要： Described are methyl substituted pinyl oxopentenes and mixtures of same defined according to the structure: ##STR1## wherein Z represents methylidene pinyl oxopentenes and mixtures of same defined according to the structure: ##STR2## ethylidene defined according to the structure: ##STR3## or ethylenyl defined according to the structure: ##STR4## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents no bond; wherein n is 0 or 1 and m is 0 or 1 with the sum of n+m being equal to 1; wherein X represents carbinol having the structure: ##STR5## or ketone having the structure: ##STR6## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 represent hydrogen or methyl.
摘要翻译：描述的是甲基取代的戊基氧代戊烯和根据以下结构定义的相同的混合物：其中Z代表亚甲基哌啶基氧代戊烯，以及根据以下结构定义的相同的混合物：根据以下结构定义的亚乙基：根据以下结构定义：其中虚线中的一条代表碳 - 碳单键，虚线中的另一条不表示键; 其中n为0或1，m为0或1，n + m的和为1; 其中X表示具有以下结构的甲醇：具有以下结构的结构：其中R 1，R 2，R 3和R 4表示氢或甲基。

20. 发明授权

US4587981A Use of norbornyl pyridine derivatives in augmenting or enhancing the aroma of tobacco and in flavored tobacco composition 失效
标题翻译：降冰片基吡啶衍生物在增加或增强烟草香味和调味烟草组合物中的应用
公开(公告)号：US4587981A
公开(公告)日：1986-05-13
申请号：US742326
申请日：1985-06-07
申请人： Richard M. Boden , Claude Grim
发明人： Richard M. Boden , Claude Grim
IPC分类号： C07D213/16 , C11B9/00 , A24B15/38
CPC分类号： C07D213/16 , C11B9/0092
摘要： Described is the use in (a) a process for augmenting or enhancing the aroma of tobacco; and (b) a flavored tobacco composition of norbornyl pyridine derivatives defined according to the generic structure: ##STR1## wherein R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "' and R.sub.5 "" each represents hydrogen or methyl with the proviso that at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "' and R.sub.5 "" represent hydrogen; wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond and wherein the pyridinyl moiety is bonded to the norbornyl moiety at the 2' position of the norbornyl moiety and at either the 2 or the 4 position of the pyridinyl moiety.
摘要翻译：描述了（a）增加或增强烟草香气的过程中的用途; 和（b）根据通用结构定义的降冰片基吡啶衍生物的风味烟草组合物：其中R5，R5'，R5“，R5”和R5“”各自表示氢或甲基，条件是 R5，R5'，R5“，R5”和R5“中的至少四个表示氢; 其中虚线表示碳 - 碳单键或碳 - 碳双键，其中吡啶基部分与降冰片基部分的2'位的降冰片基部分结合，并且在吡啶基的2位或4位上部分。

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