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11. 发明授权

US4405368A Iron-aluminum alloys containing boron which have been processed by rapid solidification process and method 失效
标题翻译：含有硼的铁铝合金已经通过快速凝固过程和方法加工
公开(公告)号：US4405368A
公开(公告)日：1983-09-20
申请号：US261626
申请日：1981-05-07
申请人： Ranjan Ray , Viswanathan Panchanathan , Bill C. Giessen
发明人： Ranjan Ray , Viswanathan Panchanathan , Bill C. Giessen
IPC分类号： C22C45/02 , F16H29/10
CPC分类号： C22C45/02 , Y10T428/12431
摘要： New iron base alloys containing aluminum and boron are disclosed. The alloys are subjected to a rapid solidification processing (RSP) technique which produces cooling rates between .about.10.sup.5 to 10.sup.7 .degree. C./sec. The as-quenched ribbon or powder, etc consists primarily of a metastable crystalline solid solution phase. The metastable crystalline phases are subjected to suitable heat treatments so as to produce a transformation to a stable multiphase microstructure which includes borides. The heat treated alloy exhibits superior mechanical properties with good corrosion and oxidation resistance.
摘要翻译：公开了含有铝和硼的新铁基合金。对合金进行快速凝固处理（RSP）技术，其产生105至107℃/秒之间的冷却速率。淬火的带或粉末等主要由亚稳态的结晶固溶体相组成。对亚稳态结晶相进行适当的热处理，以产生包含硼化物的稳定的多相微结构的转变。热处理合金具有优异的机械性能，具有良好的耐腐蚀和抗氧化性。

12. 发明授权

US5677265A Process for oxygenation of ceramic high T.sub.c superconductors 失效
标题翻译：陶瓷高Tc超导体氧化工艺
公开(公告)号：US5677265A
公开(公告)日：1997-10-14
申请号：US398289
申请日：1995-03-03
申请人： Bill C. Giessen , Robert S. Markiewicz , Bala Maheswaran , Thomas R. Gilbert
发明人： Bill C. Giessen , Robert S. Markiewicz , Bala Maheswaran , Thomas R. Gilbert
IPC分类号： C04B35/64 , H01L39/24 , C04B35/638 , C04B35/76
CPC分类号： C04B35/64 , H01L39/2464 , Y10S505/728 , Y10S505/785
摘要： A process for the oxygenation of ceramic high T.sub.c superconductors is disclosed. The superconductor is formed from a sintered powdered ceramic. Microchannels are formed in the ceramic material by embedding in the powder a plurality of wires or fibers formed of a material which is thermally removable during the sintering process to leave thin, continuous, tubular channels. After sintering, the ceramic is exposed to oxygen in a high temperature, high pressure environment. The microchannels aid in the transport of oxygen into the interior of the material by providing passages along which the oxygen travels prior to diffusing into the material. The lengths of the diffusion paths in the material are thereby greatly shortened. In another embodiment, the channels are formed after sintering and prior to oxygenation by drilling, punching, or etching.
摘要翻译：公开了一种用于陶瓷高Tc超导体氧合的方法。超导体由烧结陶瓷粉末形成。在陶瓷材料中形成微通道，通过在粉末中埋入由在烧结过程中可热去除的材料形成的多根线或纤维，以留下薄而连续的管状通道。烧结后，陶瓷在高温，高压环境下暴露于氧气。微通道有助于通过在扩散到材料中之前提供氧气在其中行进的通道将氧气输送到材料的内部。因此，材料中的扩散路径的长度大大缩短。在另一个实施方案中，通道在烧结之后并且在通过钻孔，冲压或蚀刻进行氧合之前形成。

13. 发明授权

US5593514A Amorphous metal alloys rich in noble metals prepared by rapid solidification processing 失效
标题翻译：通过快速固化处理制备富含贵金属的无定形金属合金
公开(公告)号：US5593514A
公开(公告)日：1997-01-14
申请号：US348017
申请日：1994-12-01
申请人： Bill C. Giessen , Sunil V. Gokhale , Krassimir G. Marchev
发明人： Bill C. Giessen , Sunil V. Gokhale , Krassimir G. Marchev
IPC分类号： C22C45/00 , C22C5/02 , C22C5/04 , C22C5/06
CPC分类号： C22C45/003
摘要： Amorphous metal alloys rich in noble metals prepared by rapid solidification processing are disclosed. The alloys have at least a ternary composition having the formula M.sub.a G1.sub.b G2.sub.c, wherein M is at least one element selected from the group consisting of Ag, Au, Ru, Os, Rh, Ir, Pd, and Pt, and G1 is at least one element selected from the group consisting of B, C, Cu, Ni, Si, and Be, and G2 is at least one element selected from the group consisting of Y, the lanthanides, Zr, Hf, Ca, Mg, Ti, Nb, and Ta. The subscripts a, b, and c are atomic percentages; a ranges from 70 to 90 percent, and b and c range from 5 to 15 percent each. Preferably, a is at least 80 percent and b and c are generally equal. The amorphous metal alloys are readily glass forming and thermally stable at room temperatures.
摘要翻译：公开了通过快速凝固处理制备的富含贵金属的无定形金属合金。该合金具有至少一种具有式MaG1bG2c的三元组合物，其中M是选自Ag，Au，Ru，Os，Rh，Ir，Pd和Pt中的至少一种元素，G1是至少一种元素选自由B，C，Cu，Ni，Si和Be组成的组中的至少一种元素，G 2是选自Y，镧系元素，Zr，Hf，Ca，Mg，Ti，Nb和 Ta 下标a，b和c是原子百分比; a范围从70％到90％，b和c范围从5％到15％。优选地，a为至少80％，b和c通常相等。非晶态金属合金在室温下易于形成玻璃并具有热稳定性。

14. 发明授权

US4540546A Method for rapid solidification processing of multiphase alloys having large liquidus-solidus temperature intervals 失效
标题翻译：用于液相线 - 固相线温度较高的多相合金的快速凝固加工方法
公开(公告)号：US4540546A
公开(公告)日：1985-09-10
申请号：US558612
申请日：1983-12-06
申请人： Bill C. Giessen
发明人： Bill C. Giessen
IPC分类号： B22D11/06 , B22F9/00 , B22F9/10 , C22C1/10 , C22C45/00 , C22C1/02 , C21C5/56
CPC分类号： B22D11/0611 , B22F9/008 , B22F9/10 , C22C1/1042 , C22C45/00 , Y10S75/956
摘要： Rapid solidification processing by liquid quenching is made practical for multiphase alloys having relatively large liquidus-solidus temperature intervals by a new processing technique termed "melt mix reaction" involving chemically reacting two starting alloys in a mixing nozzle in which a melt mix reaction takes place between the chemically reactable components of the starting alloys to form submicron particles of the resultant compound in the final alloy. The mixing and chemical reaction is performed at a temperature which is at or above the highest liquidus temperature of the starting alloys but which is also substantially below the liquidus temperature of the final alloy, and as close to the solidus temperature of the final alloy as possible. Rapid solidification may be accomplished through the utilization of a melt spinning wheel or may be accomplished through the utilization of an atomizing nozzle configuration, with the rapidly solidified alloy containing a matrix with a microdispersion or a precipitate of the resulting compound contained therein. Heat treatment of the rapidly solidified final alloy may be additionally employed to produce precipitate hardening of the final alloy should such microdispersed precipitates not be formed or be formed incompletely during the rapid solidification process.
摘要翻译：通过液体淬火的快速凝固处理对于具有相对较大的液相线 - 固相线温度间隔的多相合金是实用的，通过称为“熔融混合反应”的新的加工技术，包括在混合喷嘴中使两种起始合金化学反应，其中发生熔融混合反应起始合金的化学反应成分，以在最终合金中形成所得化合物的亚微米颗粒。混合和化学反应在等于或高于原始合金的最高液相线温度的温度下进行，但也大大低于最终合金的液相线温度，并且尽可能接近最终合金的固相线温度。可以通过利用熔融纺丝轮来实现快速凝固，或者可以通过利用雾化喷嘴构型来实现快速凝固的合金，其中含有微分散体的基质或其中所含的所得化合物的沉淀物。如果这种微分散的沉淀物在快速凝固过程中不形成或不完全形成，则可以另外使用快速固化的最终合金的热处理来产生最终合金的沉淀硬化。

15. 发明授权

US08349093B2 Method of plasma nitriding of alloys via nitrogen charging 有权
标题翻译：通过氮气充填等离子体氮化合金的方法
公开(公告)号：US08349093B2
公开(公告)日：2013-01-08
申请号：US12479904
申请日：2009-06-08
申请人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen
发明人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen
IPC分类号： C23C8/24
CPC分类号： C23C8/26 , C23C8/02 , C23C8/80 , Y10T428/12 , Y10T428/12458
摘要： A nitrided metal includes a metal core with a first microstructure and a nitrogen-containing solid solution region on the metal core. The nitrogen-containing solid solution region is free of nitride compounds and includes a second microstructure which is equivalent to the first microstructure. The first microstructure and the second microstructure are a tetragonal crystal structure.
摘要翻译：氮化金属包括在金属芯上具有第一微结构和含氮固溶体区域的金属芯。含氮固溶体区域不含氮化物，并且包括与第一微结构相当的第二微结构。第一微结构和第二微结构是四方晶体结构。

16. 发明申请

US20090246551A1 METHOD OF PLASMA NITRIDING OF ALLOYS VIA NITROGEN CHARGING 有权
标题翻译：通过氮素充填法合成氮等离子体的方法
公开(公告)号：US20090246551A1
公开(公告)日：2009-10-01
申请号：US12479904
申请日：2009-06-08
申请人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen
发明人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen
IPC分类号： B32B5/14 , B32B15/04
CPC分类号： C23C8/26 , C23C8/02 , C23C8/80 , Y10T428/12 , Y10T428/12458
摘要： A method of nitriding a metal includes transforming a surface region of a generally nitrogen-free metal into a nitrogen-containing solid solution surface region. A first heating process heats the surface region at a first temperature in the presence of a nitrogen gas partial pressure to form a nitrogen-charged surface portion on the surface region. A second heating process heats the surface region and nitrogen-charged surface portion at a second temperature for a predetermined time to interstitially diffuse nitrogen from the nitrogen-charged surface portion a depth into the surface region. Coincident with the second heating process, an ionized inert or reducing gas removes the nitrogen-charged surface portion. The resulting nitrogen-containing solid solution surface region has a gradual transition in nitrogen concentration.
摘要翻译：金属氮化的方法包括将一般无氮金属的表面区域转化为含氮固溶体表面区域。在氮气分压的存在下，第一加热工艺在第一温度下加热表面区域，以在表面区域上形成带氮表面部分。第二加热过程在第二温度下将表面区域和带氮表面部分加热预定时间，从而将含氮表面部分的氮气间隙地扩散到表面区域。与第二加热方法一致，电离的惰性或还原气体除去带氮的表面部分。所得到的含氮固溶体表面区域的氮浓度逐渐变化。

17. 发明授权

US07695573B2 Method for processing alloys via plasma (ion) nitriding 失效
标题翻译：通过等离子体（离子）氮化处理合金的方法
公开(公告)号：US07695573B2
公开(公告)日：2010-04-13
申请号：US10937100
申请日：2004-09-09
申请人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen , Raymond C. Benn , Edward H. Bittner , Harsh Vinayak
发明人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen , Raymond C. Benn , Edward H. Bittner , Harsh Vinayak
IPC分类号： C23C8/24 , C23C8/48 , C23C22/00
CPC分类号： C23C8/36
摘要： A surface processing method and power transmission component includes transforming a surface region of a metal alloy into a hardened surface region at a temperature that is less than a heat treating temperature of the metal alloy. The metal alloy includes about 11.1 wt % Ni, about 13.4 wt % Co, about 3.0 wt % Cr, about 0.2 wt % C, and about 1.2 wt % Mo which reacts with the C to form a metal carbide precipitate of the form M2C. The surface processing temperature, vacuum pressure, precursor gas flow and ratio, and time of processing are controlled to provide a desirable hardened surface region having a gradual transition in nitrogen concentration.
摘要翻译：表面处理方法和动力传递部件包括在小于金属合金的热处理温度的温度下将金属合金的表面区域变形为硬化的表面区域。金属合金包括约11.1重量％的Ni，约13.4重量％的Co，约3.0重量％的Cr，约0.2重量％的C和约1.2重量％的Mo，其与C反应形成M2C形式的金属碳化物沉淀。控制表面处理温度，真空压力，前体气体流量和比例以及加工时间，以提供在氮浓度中具有逐渐转变的期望的硬化表面区域。

18. 发明授权

US07556699B2 Method of plasma nitriding of metals via nitrogen charging 失效
标题翻译：通过氮气充电等离子体氮化氮化的方法
公开(公告)号：US07556699B2
公开(公告)日：2009-07-07
申请号：US10870489
申请日：2004-06-17
申请人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen
发明人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen
IPC分类号： C23C8/36 , C23C8/24
CPC分类号： C23C8/26 , C23C8/02 , C23C8/80 , Y10T428/12 , Y10T428/12458
摘要： A method of nitriding a metal includes transforming a surface region of a generally nitrogen-free metal into a nitrogen-containing solid solution surface region. A first heating process heats the surface region at a first temperature in the presence of a nitrogen gas partial pressure to form a nitrogen-charged surface portion on the surface region. A second heating process heats the surface region and nitrogen-charged surface portion at a second temperature for a predetermined time to interstitially diffuse nitrogen from the nitrogen-charged surface portion a depth into the surface region. Coincident with the second heating process, an ionized inert or reducing gas removes the nitrogen-charged surface portion. The resulting nitrogen-containing solid solution surface region has a gradual transition in nitrogen concentration.
摘要翻译：金属氮化的方法包括将一般无氮金属的表面区域转化为含氮固溶体表面区域。在氮气分压的存在下，第一加热工艺在第一温度下加热表面区域，以在表面区域上形成带氮表面部分。第二加热过程在第二温度下将表面区域和带氮表面部分加热预定时间，从而将含氮表面部分的氮气间隙地扩散到表面区域。与第二加热方法一致，电离的惰性或还原气体除去带氮的表面部分。所得到的含氮固溶体表面区域的氮浓度逐渐变化。

19. 发明授权

US5114905A Crystal alignment technique for superconductors 失效
标题翻译：超声波晶体对准技术
公开(公告)号：US5114905A
公开(公告)日：1992-05-19
申请号：US490752
申请日：1990-03-08
申请人： Bill C. Giessen , Robert S. Markiewicz , Feng Chen
发明人： Bill C. Giessen , Robert S. Markiewicz , Feng Chen
IPC分类号： C04B35/45 , H01L39/24
CPC分类号： H01L39/2419 , C04B35/45 , C04B35/4504 , Y10S505/727
摘要： A method of processing polycrystalline material by performing multi-axis crystal alignment utilizing anisotropies in the crystalline structure including the step of providing a polycrystalline material in a fluid suspension or malleable form having a magnetic moment. An external force to which the material is reactive is applied to align the individual crystals along a first axis. A magnetic field is applied to orient the magnetic moment of the crystals along a second axis, transverse to the first axis. The crystalline material may have a magnetic moment associated with a rare earth element of the material.
摘要翻译：通过利用晶体结构中的各向异性进行多轴晶体取向来处理多晶材料的方法，包括提供具有磁矩的流体悬浮液或可延展形式的多晶材料的步骤。施加材料反应的外力以沿着第一轴对准各个晶体。施加磁场以沿着与第一轴横切的第二轴定向晶体的磁矩。结晶材料可以具有与材料的稀土元素相关联的磁矩。

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