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11. 发明授权

US5925488A Toner processes using in-situ tricalcium phospate 失效
标题翻译：使用原位磷酸三钙的调色剂过程
公开(公告)号：US5925488A
公开(公告)日：1999-07-20
申请号：US972380
申请日：1997-11-18
申请人： Raj D. Patel , Grazyna E. Kmieckik-Lawrynowicz , Anthony J. Paine , T. Hwee Ng
发明人： Raj D. Patel , Grazyna E. Kmieckik-Lawrynowicz , Anthony J. Paine , T. Hwee Ng
IPC分类号： G03G9/087 , G03G9/08
CPC分类号： G03G9/0804 , Y10S977/788
摘要： A process for the preparation of toner which comprises(i) preparing a pigment dispersion comprised of a pigment dispersed in an ionic surfactant;(ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin particles and a counterionic surfactant;(iii) heating the above sheared blend below the glass transition temperature (Tg) of said resin particles to form electrostatically bound toner size aggregates;(iv) adding a stabilizer of in situ tricalcium phosphate solid particulants generated from a solution of calcium chloride and trisodium phosphate;(v) heating the mixture of (iii) and (iv) above about the Tg of the resin particles to obtain toner size particles comprised of resin and pigment;(vi) washing with an acid to dissolve the trisodium phosphate; and(vii) optionally washing with water, and optionally drying the toner obtained.
摘要翻译：一种制备调色剂的方法，其包括（i）制备由分散在离子表面活性剂中的颜料组成的颜料分散体; （ii）用由树脂颗粒和抗衡离子表面活性剂组成的胶乳或乳液共混物剪切所述颜料分散体; （iii）将上述剪切混合物加热到所述树脂颗粒的玻璃化转变温度（Tg）以下以形成静电结合的调色剂尺寸聚集体; （iv）加入由氯化钙和磷酸三钠生成的原位磷酸三钙固体颗粒的稳定剂; （v）加热上述（iii）和（iv）的混合物约树脂颗粒的Tg，得到由树脂和颜料组成的调色剂尺寸颗粒; （vi）用酸洗涤以溶解磷酸三钠; 和（vii）任选地用水洗涤，并任选地干燥获得的调色剂。

12. 发明授权

US07781138B2 Low melt toners and processes thereof 有权
标题翻译：低熔点调色剂及其工艺
公开(公告)号：US07781138B2
公开(公告)日：2010-08-24
申请号：US12574019
申请日：2009-10-06
申请人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allen K. Chen , Edward G. Zwartz , T. Hwee Ng
发明人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allen K. Chen , Edward G. Zwartz , T. Hwee Ng
IPC分类号： G03G5/00
CPC分类号： G03G9/0819 , G03G9/0804 , G03G9/0821 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要： A process for preparing toner particles and compositions adapted for use in preparing toners that comprise a blend of a first polyester resin with a second sharp melting polyester resin. The process includes forming an emulsion resin comprising a branched polyester resin, a crystalline polyester resin, a colorant, and optionally a wax. The resin mixture is aggregated using an aggregating agent, such as a zinc acetate solution, to form an aggregate mixture. The aggregate mixture is then coalesced at a temperature of from about 5 to about 20° C. above the Tg of the emulsion resin to produce the resultant toner particles.
摘要翻译：一种用于制备调色剂颗粒和组合物的方法，所述调色剂颗粒和组合物适用于制备调色剂，所述调色剂包括第一聚酯树脂与第二尖锐熔融聚酯树脂的共混物。该方法包括形成包含支链聚酯树脂，结晶聚酯树脂，着色剂和任选的蜡的乳液树脂。树脂混合物使用聚集剂如乙酸锌溶液聚集以形成骨料混合物。然后将聚集体混合物在高于乳液树脂的Tg约5至约20℃的温度下聚结，以产生所得到的调色剂颗粒。

13. 发明申请

US20090061349A1 LOW MELT TONERS AND PROCESSES THEREOF 失效
标题翻译：低熔体粉末及其工艺
公开(公告)号：US20090061349A1
公开(公告)日：2009-03-05
申请号：US12140738
申请日：2008-06-17
申请人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allan K. Chen , Edward G. Zwartz , T. Hwee Ng
发明人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allan K. Chen , Edward G. Zwartz , T. Hwee Ng
IPC分类号： G03G9/08
CPC分类号： G03G9/0819 , G03G9/0804 , G03G9/0821 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要： A process for preparing toner particles and compositions adapted for use in preparing toners that comprise a blend of a first polyester resin with a second sharp melting polyester resin. The process includes forming an emulsion resin comprising a branched polyester resin, a crystalline polyester resin, a colorant, and optionally a wax. The resin mixture is aggregated using an aggregating agent, such as a zinc acetate solution, to form an aggregate mixture. The aggregate mixture is then coalesced at a temperature of from about 5 to about 20° C. above the Tg of the emulsion resin to produce the resultant toner particles.
摘要翻译：一种用于制备调色剂颗粒和组合物的方法，所述调色剂颗粒和组合物适用于制备调色剂，所述调色剂包括第一聚酯树脂与第二尖锐熔融聚酯树脂的共混物。该方法包括形成包含支链聚酯树脂，结晶聚酯树脂，着色剂和任选的蜡的乳液树脂。树脂混合物使用聚集剂如乙酸锌溶液聚集以形成骨料混合物。然后将聚集体混合物在高于乳液树脂的Tg约5至约20℃的温度下聚结，以产生所得到的调色剂颗粒。

14. 发明授权

US07442740B2 Hybrid toner processes 有权
标题翻译：混合调色剂工艺
公开(公告)号：US07442740B2
公开(公告)日：2008-10-28
申请号：US12099430
申请日：2008-04-08
申请人： Raj D Patel , Guerino G Sacripante , Edward G Zwartz , Enno E Agur , Allan K Chen , T. Hwee Ng , Kimberly D Nosella , Cuong Vong , Karen A Moffat
发明人： Raj D Patel , Guerino G Sacripante , Edward G Zwartz , Enno E Agur , Allan K Chen , T. Hwee Ng , Kimberly D Nosella , Cuong Vong , Karen A Moffat
IPC分类号： C08J3/02 , G03G5/00 , C08K3/20
CPC分类号： G03G9/0806 , G03G9/0804 , G03G9/08711 , G03G9/08726 , G03G9/08755 , G03G9/08782 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要： A toner process that includes a first heating of a colorant dispersion, a first polyester resin free latex emulsion, a second polyester latex emulsion, and a wax dispersion in the presence of a coagulant containing a metal ion; adding a third polyester free latex; adding an organic sequestering compound or a silicate salt sequestering compound, followed by a second heating.
摘要翻译：在含有金属离子的凝结剂的存在下，包括着色剂分散体的第一次加热，第一聚酯树脂无胶乳乳液，第二聚酯胶乳乳液和蜡分散体的调色剂方法; 加入第三无聚酯胶乳; 加入有机螯合化合物或硅酸盐隔离化合物，然后进行第二次加热。

15. 发明申请

US20100021841A1 LOW MELT TONERS AND PROCESSES THEREOF 有权
标题翻译：低熔体粉末及其工艺
公开(公告)号：US20100021841A1
公开(公告)日：2010-01-28
申请号：US12574019
申请日：2009-10-06
申请人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allan K. Chen , Edward G. Zwartz , T. Hwee Ng
发明人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allan K. Chen , Edward G. Zwartz , T. Hwee Ng
IPC分类号： G03G9/08
CPC分类号： G03G9/0819 , G03G9/0804 , G03G9/0821 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要： A process for preparing toner particles and compositions adapted for use in preparing toners that comprise a blend of a first polyester resin with a second sharp melting polyester resin. The process includes forming an emulsion resin comprising a branched polyester resin, a crystalline polyester resin, a colorant, and optionally a wax. The resin mixture is aggregated using an aggregating agent, such as a zinc acetate solution, to form an aggregate mixture. The aggregate mixture is then coalesced at a temperature of from about 5 to about 20° C. above the Tg of the emulsion resin to produce the resultant toner particles.
摘要翻译：一种用于制备调色剂颗粒和组合物的方法，所述调色剂颗粒和组合物适用于制备调色剂，所述调色剂包括第一聚酯树脂与第二尖锐熔融聚酯树脂的共混物。该方法包括形成包含支链聚酯树脂，结晶聚酯树脂，着色剂和任选的蜡的乳液树脂。树脂混合物使用聚集剂如乙酸锌溶液聚集以形成骨料混合物。然后将聚集体混合物在高于乳液树脂的Tg约5至约20℃的温度下聚结，以产生所得到的调色剂颗粒。

16. 发明授权

US07615328B2 Low melt toners and processes thereof 失效
标题翻译：低熔点调色剂及其工艺
公开(公告)号：US07615328B2
公开(公告)日：2009-11-10
申请号：US12140738
申请日：2008-06-17
申请人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allen K. Chen , Edward G. Zwartz , T. Hwee Ng
发明人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allen K. Chen , Edward G. Zwartz , T. Hwee Ng
IPC分类号： G03G5/00
CPC分类号： G03G9/0819 , G03G9/0804 , G03G9/0821 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要： A process for preparing toner particles and compositions adapted for use in preparing toners that comprise a blend of a first polyester resin with a second sharp melting polyester resin. The process includes forming an emulsion resin comprising a branched polyester resin, a crystalline polyester resin, a colorant, and optionally a wax. The resin mixture is aggregated using an aggregating agent, such as a zinc acetate solution, to form an aggregate mixture. The aggregate mixture is then coalesced at a temperature of from about 5 to about 20° C. above the Tg of the emulsion resin to produce the resultant toner particles.
摘要翻译：一种用于制备调色剂颗粒和组合物的方法，所述调色剂颗粒和组合物适用于制备调色剂，所述调色剂包括第一聚酯树脂与第二尖锐熔融聚酯树脂的共混物。该方法包括形成包含支链聚酯树脂，结晶聚酯树脂，着色剂和任选的蜡的乳液树脂。树脂混合物使用聚集剂如乙酸锌溶液聚集以形成骨料混合物。然后将聚集体混合物在高于乳液树脂的Tg约5至约20℃的温度下聚结，以产生所得到的调色剂颗粒。

17. 发明授权

US07402371B2 Low melt toners and processes thereof 失效
标题翻译：低熔点调色剂及其工艺
公开(公告)号：US07402371B2
公开(公告)日：2008-07-22
申请号：US10948450
申请日：2004-09-23
申请人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allan K. Chen , Edward G. Zwartz , T. Hwee Ng
发明人： Guerino G. Sacripante , Fatima M. Mayer , Kimberly D. Nosella , Valerie M. Farrugia , Raj D. Patel , Milan Maric , Allan K. Chen , Edward G. Zwartz , T. Hwee Ng
IPC分类号： G03G9/087
CPC分类号： G03G9/0819 , G03G9/0804 , G03G9/0821 , G03G9/08755 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797
摘要： A process for preparing toner particles and compositions adapted for use in preparing toners that comprise a blend of a first polyester resin with a second sharp melting polyester resin. The process includes forming an emulsion resin comprising a branched polyester resin, a crystalline polyester resin, a colorant, and optionally a wax. The resin mixture is aggregated using an aggregating agent, such as a zinc acetate solution, to form an aggregate mixture. The aggregate mixture is then coalesced at a temperature of from about 5 to about 20° C. above the Tg of the emulsion resin to produce the resultant toner particles.
摘要翻译：一种用于制备调色剂颗粒和组合物的方法，所述调色剂颗粒和组合物适用于制备调色剂，所述调色剂包括第一聚酯树脂与第二尖锐熔融聚酯树脂的共混物。该方法包括形成包含支链聚酯树脂，结晶聚酯树脂，着色剂和任选的蜡的乳液树脂。树脂混合物使用聚集剂如乙酸锌溶液聚集以形成骨料混合物。然后将聚集体混合物在乳液树脂T T上方约5至约20℃的温度下聚结，以产生所得调色剂颗粒。

18. 发明授权

US08383309B2 Preparation of sublimation colorant dispersion 有权
标题翻译：升华着色剂分散体的制备
公开(公告)号：US08383309B2
公开(公告)日：2013-02-26
申请号：US12611336
申请日：2009-11-03
申请人： Yulin Wang , Ke Zhou , Edward G. Zwartz , T. Hwee Ng
发明人： Yulin Wang , Ke Zhou , Edward G. Zwartz , T. Hwee Ng
IPC分类号： G03G9/09
CPC分类号： G03G9/08795 , G03G9/08755 , G03G9/08764 , G03G9/08793 , G03G9/08797 , G03G9/091 , G03G9/0914 , G03G9/0918 , G03G9/092 , G03G9/0926 , G03G9/0928
摘要： A chemical toner composition that includes at least one curable amorphous resin and at least one sublimation colorant.
摘要翻译：一种化学调色剂组合物，其包括至少一种可固化无定形树脂和至少一种升华着色剂。

19. 发明授权

US6124409A Processes for preparing copolymers 失效
标题翻译：制备共聚物的方法
公开(公告)号：US6124409A
公开(公告)日：2000-09-26
申请号：US929457
申请日：1992-08-12
申请人： T. Hwee Ng , Hadi K. Mahabadi , Man C. Tam , Gregory J. Kovacs , Eric M. Peters , Rafik O. Loutfy
发明人： T. Hwee Ng , Hadi K. Mahabadi , Man C. Tam , Gregory J. Kovacs , Eric M. Peters , Rafik O. Loutfy
IPC分类号： C08F2/00 , C08F2/06 , C08F2/18 , C08F4/38
CPC分类号： C08F2/001 , C08F2/06 , Y10S526/921
摘要： Disclosed is a process for preparing copolymers which comprises, in the order stated: (1) adding monomers containing unsaturated carbon-to-carbon bonds, a first polymerization initiator, a second polymerization initiator, and a solvent to a reaction vessel; (2) purging the resulting solution with an inert gas; (3) sealing the reaction vessel and pressurizing it by addition of an inert gas to a pressure of from about 20 to about 600 kilopascals over ambient atmospheric pressure; (4) maintaining the temperature within the pressurized reaction vessel at a temperature of from about 50 to about 100.degree. C. for a period of from about 60 to about 300 minutes; (5) thereafter maintaining the temperature within the pressurized reaction vessel at a temperature of from about 80 to about 115.degree. C. for a period of from about 30 to about 300 minutes, wherein the temperature in step (5) is higher than the temperature in step (4); and (6) subsequently maintaining the temperature within the pressurized reaction vessel at a temperature of from about 115 to about 160.degree. C. for a period of from about 30 to about 180 minutes, wherein the temperature in step (6) is higher than the temperature in step (5). Polymers prepared according to the process of the present invention can be particularly useful in migration imaging members.
摘要翻译：公开了一种制备共聚物的方法，其顺序包括：（1）向反应容器中加入含有不饱和碳 - 碳键的单体，第一聚合引发剂，第二聚合引发剂和溶剂; （2）用惰性气体吹扫所得溶液; （3）密封反应容器并通过在环境大气压下加入约20至约600千帕斯卡的惰性气体对其加压; （4）将加压反应容器内的温度维持在约50至约100℃的温度下约60至约300分钟; （5）之后将加压反应容器内的温度保持在约80至约115℃的温度下约30至约300分钟的时间，其中步骤（5）中的温度高于温度在步骤（4）中; 和（6）随后将加压反应容器内的温度保持在约115至约160℃的温度下约30至约180分钟的时间，其中步骤（6）中的温度高于步骤（5）中的温度。根据本发明的方法制备的聚合物可以在迁移成像构件中特别有用。

20. 发明授权

US5928832A Toner adsorption processes 失效
标题翻译：调色剂吸附过程
公开(公告)号：US5928832A
公开(公告)日：1999-07-27
申请号：US219027
申请日：1998-12-23
申请人： Paul F. Smith , Beng S. Ong , T. Hwee Ng
发明人： Paul F. Smith , Beng S. Ong , T. Hwee Ng
IPC分类号： G03G9/08 , G03G9/097 , G03G9/087
CPC分类号： G03G9/0975 , G03G9/0804 , G03G9/0806
摘要： A process for the preparation of toner comprising mixing a colorant dispersion and a latex emulsion, and wherein there is accomplished a heating below about or equal to about the resin latex glass transition temperature to form aggregates followed by heating above about or equal to about the resin glass transition temperature to coalesce the aggregates; separating the toner formed, and subsequently adding to the toner in the form of a slurry a mixture of monomer and cleavable surfactant, cleaving the surfactant under basic conditions, and allowing the monomer to adsorb on the toner, then polymerizing and cooling, and wherein the cleavable surfactant is of the Formulas (I) or (II), or optionally mixtures thereof ##STR1## wherein R.sup.1 is a hydrophobic aliphatic, or hydrophobic aromatic group; R.sup.2 is selected from the group consisting of hydrogen, alkyl, aryl, alkylaryl, and alkylarylalkyl; R.sup.3 is hydrogen or alkyl; A is a hydrophilic polymer chain, and m represents the number of A segments
摘要翻译：一种制备调色剂的方法，包括混合着色剂分散体和胶乳乳液，并且其中完成低于大约或等于约树脂胶乳玻璃化转变温度的加热，以形成聚集体，然后加热至大约或等于约树脂玻璃化转变温度以聚集聚集体; 分离形成的调色剂，然后将浆料形式的调色剂加入到单体和可切割表面活性剂的混合物中，在碱性条件下裂解表面活性剂，并使单体吸附在调色剂上，然后聚合和冷却，其中可分解的表面活性剂是式（I）或（II）或其任选的其中R 1是疏水性脂族或疏水性芳族基团的混合物; R2选自氢，烷基，芳基，烷基芳基和烷基芳基烷基; R3是氢或烷基; A是亲水性聚合物链，m表示A链段的数目

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