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11. 发明授权

US4764493A Method for the production of mono-size powders of barium titanate 失效
标题翻译：生产钛酸钡单体粉末的方法
公开(公告)号：US4764493A
公开(公告)日：1988-08-16
申请号：US874460
申请日：1986-06-16
申请人： Edward Lilley , Raja R. Wusirika
发明人： Edward Lilley , Raja R. Wusirika
IPC分类号： C01G23/00 , C04B35/46
CPC分类号： B82Y30/00 , C01G23/006 , C01P2004/32 , C01P2004/52 , C01P2004/62 , C01P2004/64 , C01P2006/10 , C01P2006/12
摘要： Mono-sized barium titanate powders which have high density and substantially pure stoichiometry are provided. The powders can be produced by reacting barium hydroxide with titanium dioxide in a protic solvent at a temperature of at least 100.degree. C. for a period of at least 48 hours, or by reacting barium hydroxide with a titanium alkoxide in a protic solvent at a temperature of about the boiling point of the alkyl alcohol corresponding to the alkoxide for a period of at least about 240 hours.
摘要翻译：提供了具有高密度和基本上纯粹的化学计量的单体钛酸钡粉末。该粉末可以通过使氢氧化钡与二氧化钛在质子溶剂中在至少100℃的温度下反应至少48小时的时间，或通过使氢氧化钡与钛酸烷氧化物在质子溶剂中反应来制备约与醇盐相应的烷基醇的沸点的温度至少约240小时。

12. 发明授权

US4546089A Group 4b boride and VB.sub.2 /YB.sub.2 失效
标题翻译： 4b族硼化物和VB2 / YB2
公开(公告)号：US4546089A
公开(公告)日：1985-10-08
申请号：US454720
申请日：1982-12-30
申请人： Raja R. Wusirika
发明人： Raja R. Wusirika
IPC分类号： C04B35/58
CPC分类号： C04B35/58078 , C04B35/58 , C04B35/58071 , C04B35/645
摘要： A powder sinterable (without necessarily hot pressing) to a density approaching theoretical density of its composition and to 0-5 volume % open porosity, which powder has a particle size substantially less than 5 .mu.m and consisting of about 2 to 10 mole % of diboride of vanadium or yttrium, optionally very small amounts of oxygen and carbon, and the balance essentially diboride of Group 4b metal. The diborides can be in solid solution in the powder. The minor diborides are sintering aids.
摘要翻译：粉末可烧结（不需要热压）至接近其组成的理论密度的密度和0-5体积％的开孔率，该粉末的粒度基本上小于5微米，并且由约2至10摩尔％钒或钇的二硼化物，任选非常少量的氧和碳，余量基本上是第4b族金属的二硼化物。二硼化物可以是粉末中的固溶体。次要二硼化物是烧结助剂。

13. 发明授权

US4141739A Oxynitride glass-ceramics 失效
标题翻译：氧氮化物玻璃陶瓷
公开(公告)号：US4141739A
公开(公告)日：1979-02-27
申请号：US896355
申请日：1978-04-14
申请人： Kenneth Chyung , Raja R. Wusirika
发明人： Kenneth Chyung , Raja R. Wusirika
IPC分类号： C03C3/11 , C03C10/00 , C03C3/22
CPC分类号： C03C3/111 , C03C10/0009
摘要： The instant invention is directed to the production of glass-ceramic articles from thermally crystallizable glass compositions containing, by weight, about 40-85% SiO.sub.2 and 2.5-17% N as basic constituents and utilizing such modifiers as the alkali metals, the elements of Groups IIA and IIB of the Periodic Table, boron, and aluminum to obtain practical glass-forming compositions. In general, at N contents greater than about 3.5%, the predominant crystal phase developed in situ will customarily comprise "nitrogen mullite", silicon oxynitride (Si.sub.2 ON.sub.2), and/or .beta.'--Si.sub.3 N.sub.4 solid solution. The crystal phase which has been denominated in the literature as "nitrogen-mullite" has a lath-like morphology and, hence, is useful in reinforcing the crystalline body. Where the predominant crystal phase comprises a silicate, it is believed that nitrogen is present in some manner within the silicate crystal structure. The parent thermally crystallizable glasses appear to be self-nucleating, i.e., the addition of a conventional nucleating agent such as TiO.sub.2, ZrO.sub.2, or SnO.sub.2 is not required to cause crystallization in situ. It is postulated that N may function as a nucleating agent.
摘要翻译：本发明涉及从可热结晶的玻璃组合物中制备玻璃陶瓷制品，该玻璃组合物含有约40-85％的SiO 2和2.5-17％的N作为碱性组分，并且利用这种改性剂作为碱金属，元素周期表IIA和IIB族，硼和铝，以获得实用的玻璃形成组合物。通常，在大于约3.5％的N含量下，原位显影的主要结晶相通常包含“氮莫来石”，氮氧化硅（Si 2 ON 2）和/或β'-Si 3 N 4固溶体。在文献中称为“氮 - 莫来石”的结晶相具有板条形态，因此可用于增强结晶体。当主要结晶相包含硅酸盐时，认为氮以某种方式存在于硅酸盐晶体结构内。母体热可结晶玻璃似乎是自成核的，即不需要加入常规的成核剂如TiO 2，ZrO 2或SnO 2以引起原位结晶。假设N可以作为成核剂起作用。

14. 发明授权

US4097295A Silica-alumina-nitrogen containing glasses for production of glass-ceramics 失效
标题翻译：用于生产玻璃陶瓷的二氧化硅 - 氧化铝 - 含氮玻璃
公开(公告)号：US4097295A
公开(公告)日：1978-06-27
申请号：US843872
申请日：1977-10-20
申请人： Kenneth Chyung , Raja R. Wusirika
发明人： Kenneth Chyung , Raja R. Wusirika
IPC分类号： C03C3/11 , C03C10/00 , C03C3/04 , C03C3/08
CPC分类号： C03C3/111 , C03C10/0009
摘要： The instant invention is directed to the production of glass-ceramic articles from thermally crystallizable glass compositions containing, by weight, about 40-85% SiO.sub.2 and 2.5-17% N as basic constituents and utilizing such modifiers as the alkali metals, the elements of Groups IIA and IIB of the Periodic Table, boron, and aluminum to obtain practical glass-forming compositions. In general, at N contents greater than about 3.5%, the predominant crystal phase developed in situ will customarily comprise "nitrogen mullite," silicon oxynitride (Si.sub.2 ON.sub.2), and/or .beta.'-Si.sub.3 N.sub.4 solid solution. The crystal phase which has been denominated in the literature as "nitrogen-mullite" has a lath-like morphology and, hence, is useful in reinforcing the crystalline body. Where the predominant crystal phase comprises a silicate, it is believed that nitrogen is present in some manner within the silicate crystal structure. The parent thermally crystallizable glasses appear to be self-nucleating, i.e., the addition of a conventional nucleating agent such as TiO.sub.2, ZrO.sub.2, or SnO.sub.2 is not required to cause crystallization in situ. It is postulated that N may function as a nucleating agent.
摘要翻译：本发明涉及从可热结晶的玻璃组合物中制备玻璃陶瓷制品，该玻璃组合物含有约40-85％的SiO 2和2.5-17％的N作为碱性组分，并且利用这种改性剂作为碱金属，元素周期表IIA和IIB族，硼和铝，以获得实用的玻璃形成组合物。通常，在大于约3.5％的N含量下，原位显影的主要结晶相通常包含“氮富铝红柱石”，氮氧化硅（Si2ON2）和/或β'-Si3N4固溶体。在文献中称为“氮 - 莫来石”的结晶相具有板条形态，因此可用于增强结晶体。当主要结晶相包含硅酸盐时，认为氮以某种方式存在于硅酸盐晶体结构内。母体热可结晶玻璃似乎是自成核的，即不需要加入常规的成核剂如TiO 2，ZrO 2或SnO 2以引起原位结晶。假设N可以作为成核剂起作用。

15. 发明申请

US20080160376A1 Fuel cells with enhanced via fill compositions and/or enhanced via fill geometries 有权
公开(公告)号：US20080160376A1
公开(公告)日：2008-07-03
申请号：US12075497
申请日：2008-03-12
申请人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Susan L. Schiefelbein , Dell J. St. Julien , Raja R. Wusirika
发明人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Susan L. Schiefelbein , Dell J. St. Julien , Raja R. Wusirika
IPC分类号： H01M8/10
CPC分类号： H01M4/8621 , H01M4/9066 , H01M8/0206 , H01M8/0208 , H01M8/0247 , H01M8/0256 , H01M8/1226 , H01M8/1231 , H01M8/1246 , H01M8/2425 , H01M8/2432 , H01M8/2457 , Y02E60/525 , Y02P70/56
摘要： A fuel cell and method for manufacturing the fuel cell are described herein. Basically, the fuel cell is formed from an electrode/electrolyte structure including an array of anode electrodes and cathode electrodes disposed on opposing sides of an electrolyte sheet, the anode and cathode electrodes being electrically connected in series, parallel, or a combination thereof by electrical conductors that traverse via holes in the electrolyte sheet. Several different embodiments of electrical conductors which have a specific composition and/or a specific geometry are described herein.

16. 发明授权

US07132150B2 Porous ceramic filters with catalyst coatings 有权
标题翻译：具有催化剂涂层的多孔陶瓷过滤器
公开(公告)号：US07132150B2
公开(公告)日：2006-11-07
申请号：US10641638
申请日：2003-08-14
申请人： Steven B. Ogunwumi , Odessa N. Petzold , Yuxin Tang , Tinghong Tao , Jianguo Wang , Raja R. Wusirika
发明人： Steven B. Ogunwumi , Odessa N. Petzold , Yuxin Tang , Tinghong Tao , Jianguo Wang , Raja R. Wusirika
IPC分类号： B32B3/12 , B05D7/22 , B05D3/02
CPC分类号： B01J35/04 , B01J37/0217 , B01J37/0219 , Y10T428/12479 , Y10T428/24149 , Y10T428/24157 , Y10T428/24471 , Y10T428/24926 , Y10T428/249956 , Y10T428/249978 , Y10T428/249981
摘要： Porous ceramic catalyst supports or filters to be provided with catalyst coatings via oxide washcoating processes are pre-coated with polymer barrier layers to prevent washcoat nanoparticle intrusion into the microcracked and/or microporous surfaces of the ceramics, the barrier coatings being formed of hydrocarbon polymers that are soluble or dispersible in polar media, capable of forming neutral or hydrophilic surfaces on porous ceramic supports, and completely vaporizable at moderate washcoat stabilization or catalyst activation temperatures.
摘要翻译：通过氧化物涂布工艺提供催化剂涂层的多孔陶瓷催化剂载体或过滤器预先涂覆有聚合物阻挡层，以防止修补涂层纳米颗粒侵入陶瓷的微裂纹和/或微孔表面，阻挡涂层由烃聚合物形成，在极性介质中是可溶的或可分散的，能够在多孔陶瓷载体上形成中性或亲水表面，并在适中的修补基面涂层稳定或催化剂活化温度下完全可蒸发。

17. 发明授权

US06852436B2 High performance solid electrolyte fuel cells 有权
标题翻译：高性能固体电解质燃料电池
公开(公告)号：US06852436B2
公开(公告)日：2005-02-08
申请号：US10077301
申请日：2002-02-15
申请人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Dell J. St. Julien , Raja R. Wusirika
发明人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Dell J. St. Julien , Raja R. Wusirika
IPC分类号： H01M4/86 , H01M8/02 , H01M8/12 , H01M8/24
CPC分类号： H01M4/8621 , H01M4/9066 , H01M8/0206 , H01M8/0208 , H01M8/0247 , H01M8/0256 , H01M8/1226 , H01M8/1231 , H01M8/1246 , H01M8/2425 , H01M8/2432 , H01M8/2457 , Y02E60/525 , Y02P70/56
摘要： The present invention relates to a fuel cell apparatus which includes arrays of positive air electrodes and negative fuel electrodes with via interconnections disposed on an electrolyte sheet; optional electrode designs include symmetric electrodes comprising a conductive silver alloy metal phase and a thermally stabilizing ceramic phase, the latter providing low interface resistance and matching thermal properties.
摘要翻译：燃料电池装置技术领域本发明涉及一种燃料电池装置，其包括正空气电极阵列和负极燃料电极，通孔互连设置在电解质片上; 可选的电极设计包括包括导电银合金金属相和热稳定陶瓷相的对称电极，后者提供低界面电阻和匹配的热性能。

18. 发明授权

US06623881B2 High performance solid electrolyte fuel cells 有权
标题翻译：高性能固体电解质燃料电池
公开(公告)号：US06623881B2
公开(公告)日：2003-09-23
申请号：US09858124
申请日：2001-05-15
申请人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Dell J. St. Julien , Raja R. Wusirika
发明人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Dell J. St. Julien , Raja R. Wusirika
IPC分类号： H01M400
CPC分类号： H01M8/0247 , H01M4/8621 , H01M4/9066 , H01M8/0206 , H01M8/0208 , H01M8/0256 , H01M8/1226 , H01M8/1231 , H01M8/1246 , H01M8/2425 , H01M8/2432 , Y02E60/525 , Y02P70/56
摘要： The present invention relates to a compliant fuel cell apparatus which includes arrays of positive air electrodes and negative fuel electrodes with via interconnections disposed on a thin compliant electrolyte sheet; optional electrode designs include symmetric electrodes comprising a conductive silver alloy metal phase and a thermally stabilizing ceramic phase, the latter providing low interface resistance and matching thermal properties, with the resulting fuel cells remaining sufficiently compliant to demonstrate good resistance to thermal shock damage.
摘要翻译：本发明涉及一种兼容的燃料电池装置，其包括正空气电极和负极燃料电极的阵列，其中通孔互连设置在薄柔顺电解质片上; 可选的电极设计包括包括导电银合金金属相和热稳定陶瓷相的对称电极，后者提供低界面电阻和匹配的热性能，所得到的燃料电池保持足够的柔顺性以显示出良好的耐热冲击损伤性。

19. 发明授权

US5449541A Electrically heatable honeycomb structures 失效
标题翻译：电加热蜂窝结构
公开(公告)号：US5449541A
公开(公告)日：1995-09-12
申请号：US119833
申请日：1993-09-13
申请人： G. Daniel Lipp , Srinivas H. Swaroop , Donald M. Trotter , Raja R. Wusirika
发明人： G. Daniel Lipp , Srinivas H. Swaroop , Donald M. Trotter , Raja R. Wusirika
IPC分类号： B01D29/31 , B01D46/00 , B01D46/24 , F01N3/022 , F01N3/027 , F01N3/20 , F01N3/28 , B32B3/12
CPC分类号： B01D46/2418 , B01D29/31 , B01D46/0032 , F01N3/0222 , F01N3/027 , F01N3/2026 , F01N3/2807 , B01D2046/2481 , B01D2046/2492 , B01D46/2459 , Y02T10/26 , Y10T428/24149
摘要： Electrically conductive honeycomb structures are provided for use as catalytic converters, pre-heaters for catalytic converters, or particulate filters. The honeycomb structures are composed of subunits which are arranged to produce a serpentine conductive path through the honeycomb. The serpentine path gives the honeycomb an increased electrical resistance so that elevated temperatures can be achieved with less current. The subunits allow the serpentine current path to be produced without any slitting or cutting of the honeycomb.
摘要翻译：提供导电蜂窝结构用作催化转化器，用于催化转化器的预热器或微粒过滤器。蜂窝结构由被设置成产生通过蜂窝的蛇形导电路径的子单元组成。蛇纹路径使蜂窝体具有增加的电阻，从而可以以更少的电流实现升高的温度。子单元允许在没有任何切割或切割蜂窝体的情况下产生蛇形电流路径。

20. 发明授权

US5334570A Pore impregnated catalyst device 失效
标题翻译：孔浸渍催化剂装置
公开(公告)号：US5334570A
公开(公告)日：1994-08-02
申请号：US914473
申请日：1992-07-21
申请人： Patricia A. Beauseigneur , Irwin M. Lachman , Mallanagouda D. Patil , Srinivas H. Swaroop , Raja R. Wusirika
发明人： Patricia A. Beauseigneur , Irwin M. Lachman , Mallanagouda D. Patil , Srinivas H. Swaroop , Raja R. Wusirika
IPC分类号： B01J23/40 , B01J23/63 , B01J35/10 , B01J37/02 , B01J21/04 , B01J21/06
CPC分类号： B01J35/10 , B01J23/40 , B01J23/63 , B01J35/04 , B01J35/1019 , B01J37/024 , B01J35/023
摘要： A porous catalyst support which may be used in a catalytic converter for treating automotive exhaust gases. The support comprises a substrate having a multichannel structure of generally thin walls and washcoat particles of colloidal particle size mainly or wholly within the pores of the walls so as to increase open frontal area and reduce back pressure. Substrate is either ceramic or metal. In a ceramic substrate with microcracks in the walls, the washcoat colloidal dispersion is free of soluble inorganic constituents and the particles do not fill the microcracks so as to prevent undesirable increase in thermal expansion and corresponding decrease in thermal shock resistance.
摘要翻译：可用于处理汽车废气的催化转化器中的多孔催化剂载体。支撑体包括具有大体薄壁的多通道结构的基底和主要或完全在壁的孔内的胶体粒度的修补基面涂层颗粒，以增加开放的正面面积并降低背压。基材是陶瓷或金属。在壁中具有微裂纹的陶瓷基体中，修补基面涂层胶体分散体不含可溶性无机成分，并且颗粒不会填充微裂纹，以防止热膨胀的不期望的增加和耐热冲击性的相应降低。

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