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11. 发明申请

US20100137670A1 PROCESS AND APPARATUS FOR INJECTING OXYGEN INTO A REACTION GAS FLOWING THROUGH A SYNTHESIS REACTOR 审中-公开
标题翻译：将氧气注入通过合成反应器流动的反应气体的方法和装置
公开(公告)号：US20100137670A1
公开(公告)日：2010-06-03
申请号：US12312502
申请日：2007-11-05
申请人： Max Heinritz-Adrian , Stefan Hamel , Lothar Semrau
发明人： Max Heinritz-Adrian , Stefan Hamel , Lothar Semrau
IPC分类号： C07B41/00 , B01J19/00
CPC分类号： B01F5/0453 , B01F3/02 , B01F5/0256 , B01J8/025 , B01J8/0278 , B01J2208/00221 , B01J2208/00707
摘要： Synthesis reactor comprising an apparatus for injecting oxygen, which can be initially charged in pure form, as air, or mixed with inert gas or water vapor, into a reaction gas which can flow through the synthesis reactor which finds use, for example, in an oxydehydrogenation plant, wherein oxygen and reaction gas have different temperatures, wherein a distribution element is provided upstream of the device for accommodating a catalyst charge in flow direction of the reaction gas, said distributor element comprising a distributor body, two tube plates and a multitude of gas guide tubes for passing the reaction gas through, and the oxygen can be supplied to the chamber between the gas guide tubes, wherein at least one baffle plate is arranged orthogonally to the gas guide tubes and divides the intermediate space into at least two distributor chambers, wherein the distributor chambers are connected to one another or merge into one another fluidically through one or more orifices, at least one gas line leads into the first distributor space in flow direction, through which the oxygen can be supplied, and the lower tube plate is provided in flow direction with a multitude of orifices in the form of nozzles, bores or the like, through which the oxygen can leave the intermediate space, wherein a solids-free gas mixing zone is provided below the lower tube plate.
摘要翻译：合成反应器包括用于注入氧气的装置，其可以最初以纯的形式装入空气中，或者与惰性气体或水蒸气混合到可流过合成反应器的反应气体中，所述反应气体可用于例如氧化脱氢设备，其中氧和反应气体具有不同的温度，其中分配元件设置在装置的上游，用于在反应气体的流动方向上容纳催化剂装料，所述分配器元件包括分配器主体，两个管板和多个用于使反应气体通过的气体引导管，并且可以将氧气供应到气体引导管之间的室，其中至少一个挡板布置成与气体引导管正交，并将中间空间分成至少两个分配器室，其中分配器室彼此连接或者通过一个或多个孔在流体流动地彼此并入一条气体管线在流动方向上引入第一分配器空间，通过该空气可以供应氧气，并且下部管板沿流动方向设置有多个喷嘴，孔等形式的孔口，通过该管道氧气可以离开中间空间，其中在下管板下方设置无固体的气体混合区。

12. 发明申请

US20080300440A1 Method For Catalytically Dehydrating Propane To Form Propylene 失效
标题翻译：催化脱水丙烷形成丙烯的方法
公开(公告)号：US20080300440A1
公开(公告)日：2008-12-04
申请号：US11667518
申请日：2005-11-10
申请人： Max Heinritz-Adrian
发明人： Max Heinritz-Adrian
IPC分类号： C07C5/32
CPC分类号： C07C5/333 , C07C11/06
摘要： The invention relates to a method for producing propylene during which a first gas mixture, which is technically free of oxygen but contains propane, water vapor and hydrogen, and which has a temperature of at least 400° C., is led into a reaction device having at least one catalyst bed as well as usual dehydration conditions. Another gas mixture, which contains propane and oxygen and which can also contain ammonia, the propane content exceeding the oxygen content, is led into the same reaction device in which it reacts with the first gas mixture while forming propylene, water vapor and hydrogen, and the formed gas mixture containing propylene, water vapor and hydrogen is drawn out of the reaction device.
摘要翻译：本发明涉及一种生产丙烯的方法，其中在技术上不含氧但包含丙烷，水蒸气和氢气并且具有至少400℃的温度的第一气体混合物被引入反应装置具有至少一个催化剂床以及通常的脱水条件。包含丙烷和氧气并且还可以含有氨的另外的气体混合物被引入到与第一气体混合物反应而形成丙烯，水蒸气和氢气的相同的反应装置中，含有丙烯，水蒸汽和氢气的形成的气体混合物从反应装置中抽出。

13. 发明授权

US09290709B2 Gasification reactor and process for entrained-flow gasification 有权
标题翻译：气化反应器和夹带气化过程
公开(公告)号：US09290709B2
公开(公告)日：2016-03-22
申请号：US12733720
申请日：2008-09-18
申请人： Johannes Kowoll , Eberhard Kuske , Ralf Abraham , Max Heinritz-Adrian
发明人： Johannes Kowoll , Eberhard Kuske , Ralf Abraham , Max Heinritz-Adrian
IPC分类号： C10J3/82 , C10J3/78 , C10J3/48 , C10J3/84
CPC分类号： C10J3/82 , C01B3/02 , C10J3/20 , C10J3/485 , C10J3/78 , C10J3/845 , C10J2200/09 , C10J2300/0916 , C10J2300/093 , C10J2300/0943 , C10J2300/1223 , Y02P20/145
摘要： A process and device for the gasification of liquid or fine-grain solid fuel materials with the aid of oxygenous, gaseous gasification agents in a reactor is described. Liquid slag is separated on the walls of the reactor. The synthesis gas is generated in a first reaction chamber arranged in the upper part of the reactor and the feedstock is fed to the upper part. Liquid slag precipitates on its lateral walls, with free downflow and no solidification of the slag surface. The lower side has a hole with a slag drop-off edge, from which the generated synthesis gas can be withdrawn in downward direction and the liquid slag can drop off the edge. A second chamber which is delimited by a water film is located under the opening and used to keep the synthesis gas dry and cool. A third chamber is adjacent to the bottom of the second and fed with water to cool the synthesis gas. A water bath is adjacent the bottom of the third chamber and collects the slag particles already solidified and dropped off or those particles still in the liquid phase. The synthesis gas is withdrawn from the pressure vessel in an area below or on the side of the third chamber but in any case located above the water bath.
摘要翻译：描述了在反应器中借助于氧气气化气化剂气化液体或细粒固体燃料材料的方法和装置。液体渣在反应器的壁上分离。在布置在反应器上部的第一反应室中产生合成气，并将原料送入上部。液体渣在其侧壁上沉淀，具有自由下流并且没有熔渣表面的固化。下侧具有具有熔渣落下边缘的孔，所产生的合成气可从该孔向下拉出并且液体渣可以从边缘脱落。由水膜界定的第二个室位于开口下方，用于保持合成气干燥和冷却。第三室与第二室的底部相邻并且供给水以冷却合成气。水浴与第三室的底部相邻，并收集已经凝固并脱落的渣粒，或者仍然处于液相的颗粒。合成气体在第三室的下方或侧面的区域内从压力容器中取出，但是无论如何位于水浴上方。

14. 发明授权

US08932375B2 Method for supplying an entrained-flow gasification reactor with carbonaceous fuels 有权
标题翻译：向夹带气化反应器供应碳质燃料的方法
公开(公告)号：US08932375B2
公开(公告)日：2015-01-13
申请号：US13389870
申请日：2010-08-10
申请人： Max Heinritz-Adrian , Johannes Kowoll , Stefan Hamel
发明人： Max Heinritz-Adrian , Johannes Kowoll , Stefan Hamel
IPC分类号： C01B3/36 , C10J3/50 , C10G2/00 , C10J3/46 , C10K3/04 , C10K1/00
CPC分类号： C10J3/506 , C10G2/32 , C10G2300/207 , C10G2300/4081 , C10G2400/02 , C10J3/466 , C10J2200/15 , C10J2200/156 , C10J2300/0933 , C10J2300/0936 , C10J2300/1659 , C10J2300/1665 , C10J2300/1807 , C10J2300/1815 , C10K1/004 , C10K1/005 , C10K3/04 , Y02P30/20
摘要： With a method for supplying an entrained-flow gasification reactor with carbonaceous fuel for the production of a gas that contains CO and H2 and flue ash under pressure and at a temperature above the melting point of the ash, wherein the resulting gas is passed to further treatment stages, particularly at least one synthesis stage, the waste gas that is derived from the subsequent treatment stage and still contains hydrocarbons and/or hydrogen is used for pneumatic conveying of the fuel into the entrained-flow gasification reactor.
摘要翻译：用于在夹带气化反应器中提供含碳燃料的方法，用于在压力和高于灰分熔点的温度下产生含有CO和H 2的气体和烟灰，其中所得气体进一步传递处理阶段，特别是至少一个合成阶段，源自后续处理阶段并仍然含有烃和/或氢的废气用于将燃料气动输送到夹带气化反应器中。

15. 发明申请

US20100263278A1 GASIFICATION REACTOR AND PROCESS FOR ENTRAINED-FLOW GASIFICATION 有权
标题翻译：气化反应器和进气流化过程
公开(公告)号：US20100263278A1
公开(公告)日：2010-10-21
申请号：US12733720
申请日：2008-09-18
申请人： Johannes Kowoll , Eberhard Kuske , Ralf Abraham , Max Heinritz-Adrian
发明人： Johannes Kowoll , Eberhard Kuske , Ralf Abraham , Max Heinritz-Adrian
IPC分类号： C10J3/46 , C10J3/48
CPC分类号： C10J3/82 , C01B3/02 , C10J3/20 , C10J3/485 , C10J3/78 , C10J3/845 , C10J2200/09 , C10J2300/0916 , C10J2300/093 , C10J2300/0943 , C10J2300/1223 , Y02P20/145
摘要： A process and device for the gasification of liquid or fine-grain solid fuel materials with the aid of oxygenous, gaseous gasification agents in a reactor is described. Liquid slag is separated on the walls of the reactor. The synthesis gas is generated in a first reaction chamber arranged in the upper part of the reactor and the feedstock is fed to the upper part. Liquid slag precipitates on its lateral walls, with free downflow and no solidification of the slag surface. The lower side has a hole with a slag drop-off edge, from which the generated synthesis gas can be withdrawn in downward direction and the liquid slag can drop off the edge. A second chamber which is delimited by a water film is located under the opening and used to keep the synthesis gas dry and cool. A third chamber is adjacent to the bottom of the second and fed with water to cool the synthesis gas. A water bath is adjacent the bottom of the third chamber and collects the slag particles already solidified and dropped off or those particles still in the liquid phase. The synthesis gas is withdrawn from the pressure vessel in an area below or on the side of the third chamber but in any case located above the water bath.
摘要翻译：描述了在反应器中借助于氧气气化气化剂气化液体或细粒固体燃料材料的方法和装置。液体渣在反应器的壁上分离。在布置在反应器上部的第一反应室中产生合成气，并将原料送入上部。液体渣在其侧壁上沉淀，具有自由下流并且没有熔渣表面的固化。下侧具有具有熔渣落下边缘的孔，所产生的合成气可从该孔向下拉出并且液体渣可以从边缘脱落。由水膜界定的第二个室位于开口下方，用于保持合成气干燥和冷却。第三室与第二室的底部相邻并且供给水以冷却合成气。水浴与第三室的底部相邻，并收集已经凝固并脱落的渣粒，或者仍然处于液相的颗粒。合成气体在第三室的下方或侧面的区域内从压力容器中取出，但是无论如何位于水浴上方。

16. 发明申请

US20070100191A1 Method and device for nozzle-jetting oxygen into a synthesis reactor 有权
标题翻译：将氧气喷射到合成反应器中的方法和装置
公开(公告)号：US20070100191A1
公开(公告)日：2007-05-03
申请号：US10583572
申请日：2004-12-10
申请人： Johannes Kowoll , Max Heinritz-Adrian , Lothar Semrau
发明人： Johannes Kowoll , Max Heinritz-Adrian , Lothar Semrau
IPC分类号： B01J8/02 , C07C5/327
CPC分类号： B01F5/0466 , B01F5/0453 , B01J8/025 , B01J8/0278 , C01B3/386 , C01B2203/0261
摘要： With the help of a method and device for nozzle-jetting oxygen into a synthesis reactor, e.g. for oxy-dehydration, with largely axial flow of the gas mixture through a catalyst bed, it is intended to vastly improve the mixing-in and mixing-through of oxygen above the catalyst especially for oxy-dehydration process. This is achieved by feeding the oxygen to a ring distributor system arranged above the catalyst bed in pure form, as air or mixed with inert gas or water vapour and jetting the oxygen onto the catalyst surface through several exit openings in the ring distributor at an inclined angle deviating from the vertical.
摘要翻译：借助于将氧气喷射到合成反应器中的方法和装置，例如，对于氧脱水，气体混合物的大量轴向流动通过催化剂床，旨在极大地改善催化剂上方的氧气的混合和混合，特别是用于氧脱水过程。这通过将氧气供给到布置在催化剂床上方的环形分配器系统中，以纯的形式，作为空气或与惰性气体或水蒸气混合并通过环形分配器中的多个出口开口将氧气喷射到催化剂表面上，角度偏离垂直方向。

17. 发明申请

US20140374661A1 METHOD FOR PRODUCING SYNTHESIS GAS BY GASIFYING A BIOMASS IN A FLUIDIZED BED 审中-公开
标题翻译：通过在流化床中生物质生产合成气的方法
公开(公告)号：US20140374661A1
公开(公告)日：2014-12-25
申请号：US14345583
申请日：2012-09-05
申请人： Max Heinritz-Adrian , Ralf Abraham , Domenico Pavone
发明人： Max Heinritz-Adrian , Ralf Abraham , Domenico Pavone
IPC分类号： C01B3/02 , B01J8/32
CPC分类号： C01B3/02 , B01J8/32 , B01J2219/30416 , B01J2219/3086 , C01B2203/0272 , C01B2203/1211 , C10J3/503 , C10J2200/15 , C10J2300/0906 , C10J2300/0916 , C10J2300/0976 , C10J2300/0993 , C10J2300/1807 , C10K1/008 , C10K1/101 , Y02P20/145
摘要： A method for producing synthesis gas by gasifying a biomass in a fluidized bed is disclosed wherein the biomass is fed to a fluidized bed gasifier. In order to eliminate vapor-forming alkalis produced during the gasification, the method brings the synthesis gas into contact with getter ceramics.
摘要翻译：公开了一种通过在流化床中气化生物质来生产合成气的方法，其中生物质被供给流化床气化器。为了消除在气化期间产生的蒸气形成碱，该方法使合成气与吸气剂陶瓷接触。

18. 发明授权

US08043577B2 Method and device for nozzle-jetting oxygen into a synthesis reactor 有权
标题翻译：将氧气喷射到合成反应器中的方法和装置
公开(公告)号：US08043577B2
公开(公告)日：2011-10-25
申请号：US10583572
申请日：2004-12-10
申请人： Johannes Kowoll , Max Heinritz-Adrian , Lothar Semrau
发明人： Johannes Kowoll , Max Heinritz-Adrian , Lothar Semrau
IPC分类号： B01J8/02 , C07C5/48
CPC分类号： B01F5/0466 , B01F5/0453 , B01J8/025 , B01J8/0278 , C01B3/386 , C01B2203/0261
摘要： With the help of a method and device for nozzle-jetting oxygen into a synthesis reactor, e.g. for oxy-dehydration, with largely axial flow of the gas mixture through a catalyst bed, it is intended to vastly improve the mixing-in and mixing-through of oxygen above the catalyst especially for oxy-dehydration process.This is achieved by feeding the oxygen to a ring distributor system arranged above the catalyst bed in pure form, as air or mixed with inert gas or water vapor and jetting the oxygen onto the catalyst surface through several exit openings in the ring distributor at an inclined angle deviating from the vertical.
摘要翻译：借助于将氧气喷射到合成反应器中的方法和装置，例如，对于氧脱水，气体混合物的大量轴向流动通过催化剂床，旨在极大地改善催化剂上方的氧气的混合和混合，特别是用于氧脱水过程。这通过将氧气供给到布置在催化剂床上方的环形分配器系统中，以纯的形式，作为空气或与惰性气体或水蒸气混合并通过环形分配器中的多个出口开口将氧气喷射到催化剂表面上，角度偏离垂直方向。

19. 发明授权

US07678956B2 Method for catalytically dehydrating propane to form propylene 失效
标题翻译：催化脱水丙烷以形成丙烯的方法
公开(公告)号：US07678956B2
公开(公告)日：2010-03-16
申请号：US11667518
申请日：2005-11-10
申请人： Max Heinritz-Adrian
发明人： Max Heinritz-Adrian
IPC分类号： C07C5/333
CPC分类号： C07C5/333 , C07C11/06
摘要： The invention relates to a method for producing propylene during which a first gas mixture, which is technically free of oxygen but contains propane, water vapor and hydrogen, and which has a temperature of at least 400° C., is led into a reaction device having at least one catalyst bed as well as usual dehydration conditions. Another gas mixture, which contains propane and oxygen and which can also contain ammonia, the propane content exceeding the oxygen content, is led into the same reaction device in which it reacts with the first gas mixture while forming propylene, water vapor and hydrogen, and the formed gas mixture containing propylene, water vapor and hydrogen is drawn out of the reaction device.
摘要翻译：本发明涉及一种生产丙烯的方法，其中在技术上不含氧但包含丙烷，水蒸气和氢气并且具有至少400℃的温度的第一气体混合物被引入反应装置具有至少一个催化剂床以及通常的脱水条件。包含丙烷和氧气并且还可以含有氨的另外的气体混合物被引入到与第一气体混合物反应而形成丙烯，水蒸气和氢气的相同的反应装置中，含有丙烯，水蒸汽和氢气的形成的气体混合物从反应装置中抽出。

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