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11. 发明授权

US08153062B2 Analyte detection via electrochemically transported and generated reagent 有权
标题翻译：通过电化学传输和产生的试剂进行分析物检测
公开(公告)号：US08153062B2
公开(公告)日：2012-04-10
申请号：US11731138
申请日：2007-03-30
申请人： Martin W. Kendig , Chuan-Hua Chen , D. Morgan Tench , Jeffrey F. DeNatale , Frederick M. Discenzo
发明人： Martin W. Kendig , Chuan-Hua Chen , D. Morgan Tench , Jeffrey F. DeNatale , Frederick M. Discenzo
IPC分类号： G01N15/06
CPC分类号： G01N33/02 , G01N21/272 , G01N33/1826 , Y02A20/206
摘要： Electrochemical devices, methods, and systems for detecting and quantifying analytes are disclosed. A chemical detection reagent is locally generated in a test solution by electrochemical reaction of a precursor compound caused to migrate into the test solution from a precursor solution separated from the test solution by a cell separator. This approach provides precise metering of the reagent, via the charge passed, and avoids the need to store a reagent solution that may be chemically unstable. In one embodiment, the starch concentration in a colloidal solution can be measured via spectroscopic detection of a blue complex formed by the interaction of starch with iodine produced, on demand, by electrochemical oxidation of iodide ion. The approach may also be used to characterize certain types of analytes. The invention is amenable to automation and is particularly useful for on-line monitoring of production processes, including the inclusion of feed back loop mechanisms for process control.
摘要翻译：公开了用于检测和定量分析物的电化学装置，方法和系统。化学检测试剂在测试溶液中通过电化学反应局部产生，所述前体化合物通过细胞分离器从与测试溶液分离的前体溶液迁移到测试溶液中。该方法通过经过的电荷提供了试剂的精确计量，并且避免了存储可能化学不稳定的试剂溶液的需要。在一个实施方案中，胶体溶液中的淀粉浓度可以通过光谱检测通过淀粉与产生的碘的相互作用形成的蓝色络合物，根据需要通过碘化物离子的电化学氧化来测量。该方法也可用于表征某些类型的分析物。本发明适用于自动化，并且特别适用于生产过程的在线监测，包括包括用于过程控制的反馈循环机制。

12. 发明授权

US08016987B2 Evaluation of the corrosion inhibiting activity of a coating 有权
标题翻译：评估涂层的腐蚀抑制活性
公开(公告)号：US08016987B2
公开(公告)日：2011-09-13
申请号：US12218148
申请日：2008-07-11
申请人： Martin W. Kendig , Melitta M. Hon
发明人： Martin W. Kendig , Melitta M. Hon
IPC分类号： G01N27/403
CPC分类号： G01N17/02
摘要： The corrosion inhibiting activity of a coating is determined from the effect of corrosion inhibiting species released by the coating on the oxygen reduction current for a cathode placed very close to the coating. A rotating disk electrode or pumped solution flow is used to sweep the corrosion inhibiting species from the coating surface to the cathode. The oxygen reduction current is measured under conditions of oxygen diffusion control.
摘要翻译：由涂层释放的腐蚀抑制物质对非常接近涂层的阴极的氧还原电流的影响确定涂层的腐蚀抑制活性。旋转圆盘电极或泵送溶液流被用于将腐蚀抑制物质从涂层表面扫除至阴极。在氧扩散控制的条件下测量氧还原电流。

13. 发明授权

US07970559B2 Identifying damage to a wire 有权
标题翻译：识别电线损坏
公开(公告)号：US07970559B2
公开(公告)日：2011-06-28
申请号：US12210178
申请日：2008-09-12
申请人： Daniel N. Rogovin , Martin W. Kendig
发明人： Daniel N. Rogovin , Martin W. Kendig
IPC分类号： G01R31/00 , G01R31/08 , G01R31/02
CPC分类号： H04B5/00 , G01R31/025 , G01R31/088
摘要： Methods, systems, and articles of manufacture consistent with the present invention determine the type of damage to a wire, the amount of damage, and the location of the damage based on the wire's broadband impedance measured from a single measurement point. The type of damage is determined by comparing the wire's calculated dielectric function, resistance and inductance to known values that correspond to types of wire damage. The amount of damage is determined by comparing the wire's low-frequency impedance phase to known low-frequency impedance phase information that corresponds to a known amount of wire damage. The location of damage is determined by comparing the wire's high-frequency impedance phase to known high-frequency impedance phase information that corresponds to a known location of wire damage.
摘要翻译：根据本发明的方法，系统和制品根据从单个测量点测量的线的宽带阻抗来确定线的损坏类型，损伤量和损坏的位置。通过将导线的计算介电函数，电阻和电感与对应于导线损坏类型的已知值进行比较来确定损坏类型。通过将电线的低频阻抗相位与对应于已知的电线损伤量的已知低频阻抗相位信息进行比较来确定损坏量。损坏的位置是通过将电线的高频阻抗相位与对应于已知位置的电线损伤的已知高频阻抗相位信息进行比较来确定的。

14. 发明申请

US20100066384A1 IDENTIFYING DAMAGE TO A WIRE 有权
标题翻译：识别线损坏
公开(公告)号：US20100066384A1
公开(公告)日：2010-03-18
申请号：US12210178
申请日：2008-09-12
申请人： Daniel N. Rogovin , Martin W. Kendig
发明人： Daniel N. Rogovin , Martin W. Kendig
IPC分类号： G01R31/08
CPC分类号： H04B5/00 , G01R31/025 , G01R31/088
摘要： Methods, systems, and articles of manufacture consistent with the present invention determine the type of damage to a wire, the amount of damage, and the location of the damage based on the wire's broadband impedance measured from a single measurement point. The type of damage is determined by comparing the wire's calculated dielectric function, resistance and inductance to known values that correspond to types of wire damage. The amount of damage is determined by comparing the wire's low-frequency impedance phase to known low-frequency impedance phase information that corresponds to a known amount of wire damage. The location of damage is determined by comparing the wire's high-frequency impedance phase to known high-frequency impedance phase information that corresponds to a known location of wire damage.
摘要翻译：根据本发明的方法，系统和制品根据从单个测量点测量的线的宽带阻抗来确定线的损坏类型，损伤量和损坏的位置。通过将导线的计算介电函数，电阻和电感与对应于导线损坏类型的已知值进行比较来确定损坏类型。通过将电线的低频阻抗相位与对应于已知的电线损伤量的已知低频阻抗相位信息进行比较来确定损坏量。损坏的位置是通过将电线的高频阻抗相位与对应于已知位置的电线损伤的已知高频阻抗相位信息进行比较来确定的。

15. 发明授权

US07662312B2 Pigment grade corrosion inhibitor host-guest compositions and procedure 失效
标题翻译：颜料级缓蚀剂主体 - 客体组合物和程序
公开(公告)号：US07662312B2
公开(公告)日：2010-02-16
申请号：US11982011
申请日：2007-11-01
申请人： John Sinko , Martin W. Kendig
发明人： John Sinko , Martin W. Kendig
IPC分类号： C09K3/00 , C23F11/00 , B05D3/02
CPC分类号： C23C22/74 , C01P2002/22 , C01P2002/82 , C09C1/02 , C09C1/40 , C09D5/084 , C23C22/66 , C23C22/67 , C23C26/00
摘要： A pigment grade corrosion inhibitor and a method of applying the inhibitor is disclosed. The inhibitor is comprised of a host species comprised of an inorganic compound having a layered structure and a guest species comprised an anionic species of a weak acid. The host species is preferably a double hydroxide having a structure of: [M(II)1−x M(III)x (OH−)2] [An−x/n.y H2O], where M(II) is a divalent metal cationic species, M(III) is a trivalent metal cationic species, and An− is an anionic species, preferably with the species present in a range of: 0.2≦M(III)/(M(II)+M(III))≦0.4. The guest species include: various phosphoric acids and derivatives thereof; boric acid; cyanamidic acid; nitrous acid; derivatives of thio- and dithiocarbonic acid; thio-organic compounds functionalized with at least one —SH group of acidic character, including: 2,5-dimercapto-1,3,4-thiadiazole (DMTD), 2,4-dimercapto-s-triazolo-[4,3-b]-1,3-4 thiadiazole, trithiocyanuric acid (TMT), and dithiocyanuric acid.
摘要翻译：公开了一种颜料级缓蚀剂及其应用抑制剂的方法。抑制剂包括由具有层状结构的无机化合物和包含弱酸的阴离子种类的客体物质组成的宿主物质。主要物质优选是具有以下结构的双氢氧化物：[M（II）1-x M（III）x（OH-）2] [An-x / nYH 2 O]，其中M（II）是二价金属阳离子种类，M（III）是三价金属阳离子物质，An-是阴离子物质，优选物质存在于：0.2≤M（III）/（M（II）+ M（III））<= 0.4。客体物种包括：各种磷酸及其衍生物; 硼酸氰amid酸亚硝酸; 硫代和二硫代碳酸的衍生物; 具有至少一个酸性特征的-SH基官能化的硫代有机化合物，包括：2,5-二巯基-1,3,4-噻二唑（DMTD），2,4-二巯基-s-三唑并[4,3- b] -1,3,4-噻二唑，三硫代氰尿酸（TMT）和二硫氰尿酸。

16. 发明授权

US08691028B2 Article having a hexavalent-chromium-free, corrosion-inhibiting organic conversion coating thereon, and its preparation 有权
标题翻译：具有六价铬无腐蚀性的有机转化膜的制品及其制备方法
公开(公告)号：US08691028B2
公开(公告)日：2014-04-08
申请号：US11382499
申请日：2006-05-10
申请人： Martin W. Kendig , Melitta M. Hon , Leslie F. Warren, Jr.
发明人： Martin W. Kendig , Melitta M. Hon , Leslie F. Warren, Jr.
IPC分类号： C23C22/48 , C23C22/56 , C23C22/02
CPC分类号： B05D7/16 , B05D3/107 , B05D7/142 , C23C22/68 , C23C22/73 , C23C22/83
摘要： A method for protecting a surface of an article includes preparing or otherwise providing a reactive solution of a form of polyaniline and an acid, thereafter applying the reactive solution to the surface of the article to form an adherent conversion coating on the surface, thereafter oxidizing the adherent conversion coating to form an oxidized coating, and thereafter contacting a chromate-free, corrosion inhibiting organic compound such as a salt of a dithiocarbamate or a salt of a dimercaptothiadiazole to the oxidized coating to form a fixed conversion coating on the surface of the article. The resulting article has the fixed conversion coating adhered to the surface of the article. The fixed conversion coating has a mixture of a reduced polyaniline salt, and a fixed disulfur-linked dithiocarbamate polymer or dimer.
摘要翻译：用于保护制品表面的方法包括制备或以其它方式提供聚苯胺和酸形式的反应性溶液，然后将反应性溶液施加到制品的表面以在表面上形成粘附转化膜，然后将粘附转化涂层以形成氧化涂层，然后使无铬酸盐，腐蚀抑制性有机化合物如二硫代氨基甲酸盐或二巯基噻二唑的盐与氧化涂层接触，以在物品的表面上形成固定的转化涂层。所得到的制品具有粘附到制品表面的固定转化涂层。固定转化涂层具有还原的聚苯胺盐和固定的脱硫连接的二硫代氨基甲酸酯聚合物或二聚体的混合物。

17. 发明授权

US08292092B2 Macrocyclic pore-apertured carbon nanotube apparatus 有权
标题翻译：大孔孔径碳纳米管装置
公开(公告)号：US08292092B2
公开(公告)日：2012-10-23
申请号：US12555670
申请日：2009-09-08
申请人： Dennis R. Strauss , Martin W. Kendig
发明人： Dennis R. Strauss , Martin W. Kendig
IPC分类号： B01D63/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/174 , C01B2202/34 , C01B2202/36 , Y10T428/2918
摘要： A macrocyclic pore-apertured carbon nanotube apparatus is disclosed. The carbon nanotube apparatus can be used to filter or exclude ions, solutes in solution, as well as particles suspended in a colloidal mixture. The nanotube apparatus includes a carbon nanotube having a carboxylated portion at least one pore entrance and at least one molecular aperture adapted to be bonded to the carboxylated portion of the carbon nanotube. The molecular aperture is further adapted to prevent dissolved ions in a solution from entering the pore entrance. Methods for preparing and using the apparatus are also disclosed. The apparatus can also be incorporated into to filtration media for conducting reverse osmosis filtration.
摘要翻译：公开了一种大环孔径碳纳米管装置。碳纳米管装置可用于过滤或排除溶液中的离子，溶质以及悬浮在胶态混合物中的颗粒。纳米管装置包括碳纳米管，其具有羧化部分，至少一个孔入口和至少一个适于与碳纳米管的羧化部分结合的分子孔。分子孔径还适于防止溶液中溶解的离子进入孔入口。还公开了制备和使用该装置的方法。该装置也可以并入到用于进行反渗透过滤的过滤介质中。

18. 发明申请

US20110056892A1 MACROCYCLIC PORE-APERTURED CARBON NANOTUBE APPARATUS 有权
标题翻译：大理石核心碳纳米管装置
公开(公告)号：US20110056892A1
公开(公告)日：2011-03-10
申请号：US12555670
申请日：2009-09-08
申请人： Dennis R. Strauss , Martin W. Kendig
发明人： Dennis R. Strauss , Martin W. Kendig
IPC分类号： B01D37/00 , B01J19/10 , B32B9/00 , B01D24/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/174 , C01B2202/34 , C01B2202/36 , Y10T428/2918
摘要： A macrocyclic pore-apertured carbon nanotube apparatus is disclosed. The carbon nanotube apparatus can be used to filter or exclude ions, solutes in solution, as well as particles suspended in a colloidal mixture. The nanotube apparatus includes a carbon nanotube having a carboxylated portion at least one pore entrance and at least one molecular aperture adapted to be bonded to the carboxylated portion of the carbon nanotube. The molecular aperture is further adapted to prevent dissolved ions in a solution from entering the pore entrance. Methods for preparing and using the apparatus are also disclosed. The apparatus can also be incorporated into to filtration media for conducting reverse osmosis filtration.
摘要翻译：公开了一种大环孔径碳纳米管装置。碳纳米管装置可用于过滤或排除溶液中的离子，溶质以及悬浮在胶态混合物中的颗粒。纳米管装置包括碳纳米管，其具有羧化部分，至少一个孔入口和至少一个适于与碳纳米管的羧化部分结合的分子孔。分子孔径还适于防止溶液中溶解的离子进入孔入口。还公开了制备和使用该装置的方法。该装置也可以并入到用于进行反渗透过滤的过滤介质中。

19. 发明授权

US07735362B2 Thermomechanical sensor for fluid diagnostics 有权
标题翻译：用于流体诊断的热机械传感器
公开(公告)号：US07735362B2
公开(公告)日：2010-06-15
申请号：US11395022
申请日：2006-03-31
申请人： Jeffrey F. DeNatale , Robert L. Borwick, III , Philip A. Stupar , Martin W. Kendig
发明人： Jeffrey F. DeNatale , Robert L. Borwick, III , Philip A. Stupar , Martin W. Kendig
IPC分类号： G01N33/30
CPC分类号： G01N33/2888 , G01N11/16 , G01N33/26 , G01N2011/002
摘要： A method for diagnosing a fluid includes sensing a property of the fluid and the temperature of the fluid at the time the property is sensed, then determining the status of the fluid from the sensing. The sample volume may be small in comparison to the total fluid volume.
摘要翻译：用于诊断流体的方法包括在感测特性时感测流体的特性和流体的温度，然后从感测确定流体的状态。与总流体体积相比，样品体积可能较小。

20. 发明申请

US20090192251A1 NANO-STRUCTURED INORGANIC ZINC PHOSPHATE CORROSION PROTECTIVE COATING FOR METAL ALLOYS 有权
标题翻译：金属合金纳米结构无机锌磷酸盐防腐涂料
公开(公告)号：US20090192251A1
公开(公告)日：2009-07-30
申请号：US10885197
申请日：2004-07-06
申请人： Young J. Chung , Melitta M. Hon , Martin W. Kendig
发明人： Young J. Chung , Melitta M. Hon , Martin W. Kendig
IPC分类号： C09D5/08
CPC分类号： C23C18/1216 , C09D5/084 , C23C18/122 , C23C18/1241 , C23C18/1254 , Y02T50/67
摘要： A method is provided for enhancing corrosion resistance of a metal surface that includes the step of forming a sol-gel coating in which nanostructured zinc phosphate (Zn3(PO4)2) and zinc oxide (ZnO) phases are present in the mixture. The method may include the steps of mixing an organosilane, organometallic, organic acid, water, and alcohol and allowing the components of the mixture to partially hydrolyze, followed by adding at least one component having zinc functionality and at least one component having phosphate functionality to the partially hydrolyzed mixture, wherein the zinc component and phosphate component are added in a molar ratio of from about 1.5:1 to about 5:1 (Zn:PO4). The resulting mixture can be applied as a coating to a metal surface to improve the corrosion resistance of the metal and to enhance the adhesion of resinous materials to the metal surface.
摘要翻译：提供一种用于提高金属表面的耐腐蚀性的方法，包括形成溶胶 - 凝胶涂层的步骤，其中纳米结构化磷酸锌（Zn 3（PO 4）2）和氧化锌（ZnO）相存在于混合物中。该方法可以包括以下步骤：将有机硅烷，有机金属，有机酸，水和醇混合并使混合物的组分部分水解，然后将至少一种具有锌官能团的组分和至少一种具有磷酸酯官能团的组分加入到部分水解的混合物，其中以约1.5:1至约5:1（Zn：PO4）的摩尔比加入锌组分和磷酸盐组分。所得到的混合物可以作为涂层施加到金属表面以改善金属的耐腐蚀性并增强树脂材料对金属表面的粘合性。

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